• 한국재료학회지
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• 제31권8호
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• pp.433-438
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• 2021

In this study, microstructural characteristics and constituent elements of fiberglass splint and cast are examined using a scanning electron microscope and an energy dispersive X-ray spectrometer. As observed by the scanning electron microscope, fiberglass splint and cast had a porous structure with many bundles of fiberglass textures well assembled. Spaces between bundles of the fiberglass splint are triangular or elliptical shaped and the long-axis diameter is measured at about 1 mm. The thickness of fiber bundles covered with plaster is measured at 600 ㎛ and the diameter of a single strand of fiberglass is up to 10 ㎛. The thickness of the fiberglass bundle of the fiberglass splint is measured at about 700 ㎛. Spaces between bundles are formed in the shape of triangles with gentle edges and long-axis diameter of up to 1.4 mm, which is larger than that of the splint. The thickness of a single strand of fiberglass of the plaster-coated cast is 11.5 ㎛, which is thicker than that of fiberglass of the splint. As a result of analyzing constituent elements of the fiberglass cast and the splint with an energy dispersive X-ray spectrometer, Ca, Si, and Al components are identically detected. This result shows that the fiberglass cast has a smoother surface with hardened plaster than the fiberglass splint. The thickness of the fiberglass bundle and the thickness of a single strand of the fiberglass are also larger than those of the fiberglass splint.

• 공학기술논문지
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• 제6권2호
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• pp.121-124
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• 2013

This paper proposed a new concept of estimating method for LED(light-emitting diode) delamination with high accuracy. Usually, The LED is composed several materials which are LED chips, gold wire, phosphor, epoxy resin, adhesive, reflector and lead frame. These different materials are usually delaminated in a trouble conditions which are huge temperature difference, hot and humid or mechanical shocked. When the components are delaminated, a luminance will be lost, moisture be absorbed easily and a thermal resistance be increased attendantly. As a conventional method to estimate a delamination of LEDs, a solution immersing method is usually used in a field of LED manufacturing companies or researching institutes. This method has an advantage of simplicity but it is only shown that the existence of delamination or not. In this paper, we have proposed an estimating method for LEDs delamination using the polishing and the electron microscope. New proposed method has shown the result of confirming delamination without destruction and enabled quantitative analysis for LED delamination.

• 한국건축시공학회:학술대회논문집
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• 한국건축시공학회 2022년도 가을 학술논문 발표대회
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• pp.149-150
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• 2022

In Korea, there is no clearly established technology for diagnosing and evaluating the damage depth of concrete structures created by fire. There have been cases of repairing, reinforcing, and demolishing degraded structures without diagnosing the damage depth. The commonly used phenolphthalein-based carbonate thickness measurement does not satisfy the complete disappearance condition of Ca(OH)₂ in the interval where the relatively stationary flow declines after exposure to high temperatures. Even a small amount of Portlandite[Ca(OH)₂] reacts with a red color, and the damage depth is misjudged. It was confirmed by X-ray diffraction and scanning electron microscope that Ca(OH)₂ existed from 300℃ to 500℃ where the residual compressive strength decreased.

• 보존과학회지
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• 제37권4호
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• pp.402-410
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• 2021

Woolen tapestry curtains possessed by the Seoul Museum of Craft Art were used to hung on the wall or used for carpets in the winter season in the late Joseon dynasty. Since similar artifacts were only used for the curtain as functional aspects, woolen tapestry curtains were a rare case. In this study, scientific analysis on the accessory ornament of woolen tapestry curtains such as components of metal accessories and frame bar were conducted with the microscope, p-XRF, and SEM. Result of frame bar pigments, organic pigments such as ink stick were likely been used in woolen tapestry curtain 1. In woolen tapestry 2, lead red (Minium) was used in the frame bar. The result of metal parts, copper, and zinc were analyzed by p-XRF. This suggests that metal accessories were crafted using brass. Frame bar of woolen tapestry curtain 2 was made of soft pine (Pinus spp.) analyzed with the scanning electron microscope. Artifacts like woolen tapestry curtains are rare in Korea and scientific analysis databases were scarce, so it is important to construct components analysis data of woolen tapestry curtains. It is expected that additional scientific analysis and interpretation on the artifact's crafting technique can be merged with the analytical data gathered in this study to be utilized on the conservation and restoration of not only woolen curtains but curtain artifacts of the late Joseon dynasty in general.

• Applied Microscopy
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• 제38권4호
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• pp.285-291
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• 2008

Electron tomography의 정량적 분석을 위해서 대물렌즈 조리개가 투과빔의 강도에 미치는 영향을 평가하였다. Electron tomography에 도입되는 Beer's law의 올바른 적용을 위해서는 투과빔은 시료의 기울기에 따른 mass thickness의 변화에 의한 효과만을 반영해야 한다. 그러므로 빔 경로상의 대물렌즈 조리개, 홀더 등에 의한 다른 효과는 제거되어야 한다. 본 연구에서는 대물렌즈 조리개의 cut-off 효과를 120 kV TEM과 Quantifoil holey 카본 시료를 이용하여 상세히 평가하였다. 대물렌즈 조리개를 사용하지 않은 경우와 비교할 때, $30{\mu}m$ 크기의 대물렌즈 조리개를 통과한 투과전자빔의 강도는 약 16.7%의 감소가 일어난다. 또한 $55^{\circ}$ 이상의 고경사각 기울기에서는 대물렌즈 조리개의 cut-off 효과에 의해 14.2%의 강도 감소가 추가적으로 발생함을 알 수 있었다. Electron tomography에서 정량 분석을 위해서는 이러한 대물렌즈 조리개의 영향을 고려해야만 한다. 또한 Beer's law의 올바른 적용을 위해서는 일련의 기울기에 따른 2차원적 영상은 가능하면 대물렌즈 조리개를 사용하지 않은 상태에서 획득하는 것이 바람직하다.

• 대한기계학회논문집A
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• 제37권3호
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• pp.429-436
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• 2013

본 논문에서는 고주파 열처리된 SAE1055 베어링강의 경도에 따른 피로 거동 및 이의 확률론적 평가를 수행하였다. 이를 위하여 경도 수준에 따른 5 종류의 시험편(A : 원재료, B : HV390-전경화, C : HV510-전경화, D : HV700-전경화 및 E : HV-700 표면경화)를 준비하였다. 피로시험은 4 점 회전굽힘 피로시험기를 이용하여 응력비 R=-1 의 조건하에서 수행하였다. 그 결과, SAE1055 강의 피로 거동은 경도에 따라 크게 변화하였으나 HV510 수준이상에서는 피로한도의 증가는 관찰되지 않았다. 또한 피로 파손기구에 대한 경도의 영향을 평가하기 위하여 SEM(scanning electron microscope)을 이용한 파면 관찰을 수행하였다. 피로수명의 통계적 특성은 P-S-N(probabilistic S-N) 곡선을 이용하여 평가되었으며 이에 대한 경도의 영향은 잔류치 해석(residue analysis)을 통하여 수행하였다.

• 대한치과기공학회지
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• 제43권4호
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• pp.145-152
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• 2021

Purpose: This study aimed to produce resin prosthetics using a dental barrel finishing machine. For dental resin grinding, the ingredients of the barrel finishing media were analyzed, and surface residues of the resin were observed. Methods: Two types of barrel finishing media for dental resin grinding were tested. Specimens were made from thermal polymerized, auto polymerized, and photopolymerized resins. Finishing media were analyzed through energy-dispersive X-ray spectroscopy (EDS) component analysis and inductively coupled plasma-optical emission spectrometry (ICP-OES) component analysis. Then, the prepared specimen was barrel finished for 25 minutes using two types of barrel finishing media, and scanning electron microscope was photographed to observe the surface residues. Results: As a result of EDS component analysis, both types of finishing media were analyzed for the components of C, O, Zr and Al elements, and industry media (IM) was further analyzed for the components of Si and Mg elements. In the ICP-OES component analysis, Cd and As, which are harmful elements, were detected in IM, and no harmful elements were detected in manufacturing media (MM). Because of observation of surface residues, no residues were observed in the three types of resin specimens that were barrel finished with two types of finishing media. Conclusion: Surface residue wasn't observed on the specimens polished using two types of finishing media. However, in IM, Cd and As, which are harmful elements, were detected, making it inappropriate for clinical use. In MM, harmful elements were not detected; therefore, clinical use will be possible.

• Applied Microscopy
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• 제45권1호
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• pp.1-8
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• 2015

We have developed a new HD-2700 (Hitachi High-Technologies Corp., Japan) scanning transmission electron microscope (STEM) that includes an automatic aberration correction function, and a large-solid-angle energy-dispersive X-ray spectroscopy detector that enables high-resolution and sensitive analysis. For observation with atomic resolution, using spherical-aberration-corrected STEM, in order that satisfactory performance of the device can be achieved readily, and within a short time, irrespective of the operator's skill level, a spherical-aberration-correction device with an automatic aberration-correction function was developed. This automatic aberration-correction function carries out the entire correction-related process (aberration measurement, selection and correction) automatically, with automatic selection of the aberrations that require correction, and automatic measurement of the appropriate corrections.

• Journal of Welding and Joining
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• 제31권1호
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• pp.43-50
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• 2013

The spot welds of Transformation Induced Plasticity (TRIP) steels are prone to interfacial failure and narrow welding current range. Hard microstructures in weld metal and heat affected zone arenormally considered as one of the main reason to accelerate the interfacial failure mode. There fore, detailed observation of weld microstructure for TRIP steels should be made to ensure better weld quality. However, it is difficult to characterize the microstructure, which has similar color, size, and shape using the optical or electron microscopy. The atomic force microscope (AFM) can help to analyze microstructure by using different energy levels for different surface roughness. In this study, the microstructures of resistance spot welds for AHSS are analyzed by using AFM with measuring the differences in average surface roughness. It has been possible to identify the different phases and their topographic characteristics and to study their morphology using atomic force microscopy in resistance spot weld TRIP steels. The systematic topographic study for each region of weldments confirmed the presence of different microstructures with height of 350nm for martensite, 250nm for bainite, and 150nm for ferrite, respectively.

• 전기전자학회논문지
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• 제23권3호
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• pp.904-909
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• 2019

$100^{\circ}C$에 소성한 인듐 아연 산화막 (IZO)을 이온빔 처리하여, 균일할 수평 액정 배향을 구현하였다. 유리 기판 위에 코팅된 IZO 박막을 $100^{\circ}C$에 소성하고 액정 배향 기술로 이온빔을 사용하였다. 이것을 이용하여 얻어진 액정 배향의 특성을 분석하기 위해서, 편광 현미경과 결정 회전법을 사용하였다. 또한 이온빔 처리된 IZO 박막을 이용하여 만든 액정 셀이 높은 품질의 액정 소자에 충분한 열적 안정성을 가진다는 것을 확인할 수 있었다. 그리고 전계방출 주사 전자 현미경을 이용하여 이온빔의 IZO 박막의 표면에 미치는 영향을 분석하였다. 이것을 통하여 이온빔이 IZO 박막 표면의 거칠기를 변화시키고, 액정 배향에 영향을 준다는 것을 확인할 수 있었다. 마지막으로 IZO 박막으로 제작한 액정 셀의 전기-광학 특성을 측정하였다. 그리고 이것이 기존에 사용되는 러빙법 처리된 폴리이미드 박막으로 제작한 액정 셀보다 뛰어난 특성을 가진다는 것을 확인하였다. 또한 액정 고정 에너지를 측정하여 이것이 균일한 액정 배향을 구현하기 위한 적합한 특성을 가진다는 것을 확인하였다.