• 열처리공학회지
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• 제35권2호
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• pp.88-95
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• 2022

Titanium alloy for bio-medical applications have been developed to reduce the toxicity of alloying elements and avoid the stress-shielding effect which is caused by relatively high elastic modulus compared to bone. Ti-39Nb-6Zr (TNZ40) alloy of elastic modulus exhibits around 40 GPa in the case of beta single phase. However, the strength of this alloy is lower than the other types of titanium alloys. Many research found that adding oxygen to beta-titanium alloys is beneficial for improving the strength through solid solution strengthening. In this study, TNZ40 ingots with addition of O were prepared by an arc remelting process (Ti-39Nb-6Zr-0.16O (wt.%), Ti-39Nb-6Zr-0.26O (wt.%)). Thermo-mechanical processing (i.e., heat treatment, cold swaging and aging heat treatment) has been performed under various conditions. Therefore, the aim of this study is to investigate the effect of oxygen content and ω phase formation on microstructure and mechanical properties.

• 한국가금학회지
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• 제16권1호
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• pp.23-28
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• 1989

난백단백질의 농도와 당류의 첨가 수준이 난백의 열감수성에 미치는 영향을 검토하기 위하며 가열처리.($60^{\circ}C$, 5분간) 전후 난백의 기능성을 측정하였으며 그 결과는 다음과 같다. 난백단백질의 농도 8.3%까지는 가열처리 전후 난백의 탁도가 감소하였으나 희석됨에 따라 증가하다가 3.32% 이하에서는 다시 감소하였다. 가열처리 전후 난백의 기포력은 단백질 농도 8.3%에서 가장 높았으며 희석됨에 따라 점차 감소하였고 기포안정성은 단백질 농도가 희석됨에 따라 점차 저하하였다. 난백에 sucrose를 첨가할 경우 탁도의 변화가 없었으나 가열처리의 경우에는 sucrose의 첨가량에 따라 점차 감소하였다. 기포력은 sucrose 5%이상 첨가 시 감소하였으며 가열처리의 경우에는 sucrose 2.5%이상 첨가 시 점차 감소하였다. 기포안정성은 sucrose를 5%이상 진가할 경우 점차 증가하였으나 가열처리한 경우에는 sucrose의 첨가량에 따라 증가하였다. Glucose의 첨가량에 따라서는 탁도가 높아졌으며 가열처리 시에는 변화가 없었다. 기포력은 Glucose의 첨가량에 따라 점차 감소하였으며 가열처리의 경우에는 5%이상 첨가 시 다소 감소하였다. 기포안정성은 가열처리 전후 glucose의 첨가량에 따라 증가되었으며 sucrose의 첨가시 보다 크게 증가되었다.

• 동력기계공학회지
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• 제15권6호
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• pp.67-72
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• 2011

In the present study, crack healing effect and residual stress of $Al_2O_3$ ceramics were investigated by changing the sintering temperature and heat treatment conditions. And also it was investigated that the influence of different filler loadings of nano-sized SiC particles on the crack healing behavior of $Al_2O_3$ ceramics. The test samples were characterized by three point bend flexural tests to evaluate their mechanical properties. The morphological changes were studied by FE-SEM and EDS. The test results indicated that the $Al_2O_3$ with nano-sized SiC ceramics sintered at $1800^{\circ}C$ were showed highest density. Sintering temperature at $1800^{\circ}C$, the bending strength of heat treatment in air atmosphere specimens showed about 42 % increment in comparison to the un-heat treated specimens. The cracked specimens can be healed by heat treatment in vacuum atmosphere but the crack healing effect of $Al_2O_3$ ceramics, which is heat treated in air atmosphere was higher than that of heat treated in vacuum atmosphere. $Al_2O_3$ with 30 wt% of SiC ceramics indicated higher crack healing ability than that with 15 wt% of SiC ceramics. The FE-SEM images showed that the median cracks and pores were disappeared after heat treatment in air.

• 대한기계학회논문집
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• 제15권6호
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• pp.1982-1989
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• 1991

본 연구에서는 AISI 강은 대부분 열처리후에 사용되는 고강도강으로 용접시 발생하는 높은 잔류응력 분포를 제거 또는 감소시키기 위해서 여러가지 방법이 사용된 다. 잔류응력 제거는 용접후 풀림처리를 하면 잔류응역이 제거된다. 그러나 풀림 처리 하기전에 용접부에 높은 잔류응력 제거는 용접후 풀림처리를 하면 잔류응력이 제 거된다. 그러나 풀림처리 하기전에 용접부에 높은 잔류응력에 의해 균열이 생성될 수 있으므로 용접시 높은 잔류응력이 생성되지 않도록 예열 및 후열처리를 필요로한 다. 그러므로 본 연구에서는 예열 및 후열이 잔류응력 분포에 어떠한 영향을 주는가 를 실험적인 방법에 의해 연구하였다.

• 한국분말재료학회지
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• 제13권5호
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• pp.360-365
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• 2006

The phase stability of tetragonal phase in Y-TZP was investigated in terms of the distribution of grain sizes and heat-treating atmosphere. Y-TZP with various grain sizes were prepared using duration time at $1600^{\circ}C$ as experimental parameter. Accumulated grain size distributions were built from the SEM micrographs and the amount of tetragonal phase were measured using XRD. Both results were compared to determine the critical grain size before and after heat-treatment in vacuum. The critical grain size drastically decreased compared with the small increase of average grain size due to the autocatalytic effect which critically affects the tetragonal to monoclinic phase transformation. After heat-treatment in reductive atmosphere critical grain size relatively increased due to the stabilization of tetragonal phase. The formation of oxygen vacancies during heat-treatment was ascribed to the increase of stability.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2003년도 하계학술대회 논문집 Vol.4 No.1
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• pp.526-528
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• 2003

The effect of heat treatment on torsion characteristics of high nitrogen steel wire has been studied by using torsion test, micro vickers hardness and scanning electron microscopy. After heat treatment at $600{\sim}700^{\circ}C$, the torsion cycle was increased with increasing temperature. Especially, in case of high nitrogen steel wire heat treated at $600^{\circ}C$, the torsion cycle was sharply increased. It is estimated that the cold-worked high nitrogen steel wire started to recrystallize around at $650^{\circ}C$ in air atmosphere.

• 대한전기학회:학술대회논문집
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• 대한전기학회 2003년도 하계학술대회 논문집 C
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• pp.1469-1471
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• 2003

The effect of heat treatment on torsion characteristics of high nitrogen steel wire has been studied by using torsion test, micro vickers hardness and scanning electron microscopy. After heat treatment at $600{\sim}700^{\circ}C$, torsion cycle was increased with increasing temperature. Especially, in case of high nitrogen steel wire heat treated at $650^{\circ}C$, torsion cycle was sharply increased. It is estimated that the cold-worked high nitrogen steel wire started to recrystallize around at $640^{\circ}C$ in air atmosphere.

• Journal of Advanced Marine Engineering and Technology
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• 제8권2호
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• pp.81-87
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• 1984

The effect of heat treatment and mechanical stress on the dielectic strength of epoxy resin film is studied. The film with 30-210 .mu.m thickness are casted at room temperature for 8 hours and post cured at the range of temperature 60-180 .deg. C, and the heat setting time are two kind, ie, 2 and 10 hours. The samples are made with Stycast 1266 that the primary compound is diglycidyl ether of bisphenol A, and the hardner is denaturated polyamines. Under no mechanical stresses, the maximum dielectric strength of the sample is obtained for the sample heat treated for 2 hours at 150 .deg. C. However, the best dielectric strength characteristics under compressive stress is obtained for the sample heat treated at 90 .deg. C and 120 .deg. C. The dielectric strength of the sample are also affected significantly by the cooling velocity of the sample after post heat setting at given temperature.

• 대한용접접합학회:학술대회논문집
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• 대한용접접합학회 2002년도 Proceedings of the International Welding/Joining Conference-Korea
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• pp.273-275
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• 2002

The effect of post-weld heat treatment (PWHT) of marine structures steel was investigated at electrochemical viewpoint. In addition, slow strain rate test (SSRT) was carried out to investigate both electrochemical and mechanical properties by PWHT effect during impressed current cathodic protection. The optimum cathodic protection potential by SSRT was -770 mV(SCE). At the applied cathodic protection potential of -770 mV -850 mV(SCE), the fracture morphology was dimple pattern with ductile fracture, while it was transgranular pattern (Q.C: quasi cleavage) under -875 mV(SCE).

• Journal of Advanced Marine Engineering and Technology
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• 제27권3호
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• pp.453-459
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• 2003

In this study, the effect of heat treatment to the electrochemical polarization resistance for the Ti-6Al-4V alloy was measured. The solution heat treatments were carried out at $1066^{circ}E, 966^{\circ}$E$, followed by aging heat treated $550^{circ}E, 600^{circ}E, and 650^{circ}E$. The electrochemical polarization resistance behavior was measured by potentio-dynamic polarization in the 1N $HNO_3$ + 15ppm HF solution. The obtained results were as follows. 1. As solution heat temperature increased. the corrosion potential was increased, whereas passive current density and critical current density were decreased. 2. As aging heat temperature increased, the corrosion potential was almost constant, but passive current density was decreased 3. The results of composition test measured by EDS at grain boundary and near $\gamma'$ precipitates indicated that S, Cl. and Si which originated from base metal were segregated at the grain boundaries Al and Ti which were the main alloying element in $\gamma'$ were depleted at the $\gamma'$ precipitated. The depletion of Al and Ti in $\gamma'$ was caused to early breakdown of passive film.