• 열처리공학회지
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• 제29권3호
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• pp.103-108
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• 2016

In recent years, TRIP steels which are composed of ferrite, bainite, and retained austenite have drawn much attention for automotive sheets due to excellent combination of strength and ductility. The effect of two-step isothermal heat treatment of bainitic transformation on microstructures, especially retained austenites and tensile properties in the conventional TRIP steel was investigated. A two-step isothermal heat treatment, in which 50% bainitic transformation occurred at high temperature, followed by bainitic transformation at low temperature, improves tensile properties, resulting from enhanced mechanical stability of retained austenite against external plastic deformation due to refinement of retained austenites, compared to single-step isothermal heat treatment.

• Progress in Superconductivity
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• 제4권1호
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• pp.90-93
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• 2002

The sintering process of BSCCO 2223 tapes is a complex process that is very sensitive to parameters, such as temperature, oxygen partial pressure, heating and cooling rate and holding time. During the first heat treatment, 2212 phase of precursor powder is partially transformed into 2223 phase and some residual secondary phases, such as $(Bi,Pb)_2$$Sr_2$CuO／sub y／(2201), $(Ca,Sr)_2$CuO／sub y／(2/1AEC), (Ca,Sr)／sub 14／Cu／sub 24／O／sub 41／(14／24 AEC) etc. The secondary phases are difficult to be removed from the BSCCO 2223 matrix on the heat treatment. These secondary phases degrade the critical current density. In order to minimize the amount and size of alkaline earth cuprate(AEC) particles step heat treatment is applied during the first heat treatment under the varying atmosphere. Experimental results showed that by adapting the step heat treatment process, the amount and particle size of the secondary phases in the final tapes are decreased. Consequently, the BSCCO 2223grain texture and Jc properties are improved.

• 한국분말재료학회지
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• 제28권4호
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• pp.301-309
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• 2021

In this study, an AISI 316 L alloy was manufactured using a selective laser melting (SLM) process. The tensile and impact toughness properties of the SLM AISI 316 L alloy were examined. In addition, stress relieving heat treatment (650℃ / 2 h) was performed on the as-built SLM alloy to investigate the effects of heat treatment on the mechanical properties. In the as-built SLM AISI 316 L alloy, cellular dendrite and molten pool structures were observed. Although the molten pool did not disappear following heat treatment, EBSD KAM analytical results confirmed that the fractions of the low- and high-angle boundaries decreased and increased, respectively. As the heat treatment was performed, the yield strength decreased, but the tensile strength and elongation increased only slightly. Impact toughness results revealed that the impact energy increased by 33.5% when heat treatment was applied. The deformation behavior of the SLM AISI 316 L alloy was also examined in relation to the microstructure through analyses of the tensile and impact fracture surfaces.

• 한국분말재료학회지
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• 제18권6호
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• pp.552-561
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• 2011

This study attempted to manufacture a Cu-15 at.%Ga coating layer via the cold spray process and investigated the effect of heat treatment environment on the properties of cold sprayed coating material. Three kinds of heat treatment environments, $5%H_2$+argon, pure argon, and vacuum were used in this study. Annealing treatments were conducted at $200{\sim}800^{\circ}C$/1 hr. With the cold sprayed coating layer, pure ${\alpha}$-Cu and small amounts of $Ga_2O_3$ were detected in the XRD, EDS, EPMA analyses. Porosity significantly decreased and hardness also decreased with increasing annealing temperature. The inhomogeneous dendritic microstructure of cold sprayed coating material changed to the homogeneous and dense one (microstructural evolution) with annealing heat treatment. Oxides near the interface of particles could be reduced by heat treatment especially in vacuum and argon environments. Vacuum environment during heat treatment was suggested to be most effective one to improve the densification and purification properties of cold sprayed Cu-15 at.%Ga coating material.

• 열처리공학회지
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• 제23권6호
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• pp.344-349
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• 2010

Silicon carbide nanowires were grown by heat treatment of the films at $1200^{\circ}C$ after amorphous SiC thin films were deposited on graphite substrate by radio frequency magnetron sputtering at $600^{\circ}C$. It was confirmed that SiC nanowires with the diameter of 20-60 nm and length of about 50nm were grown from Field Emission Scanning Election Microscope (FE-SEM) and Transmission Election Microscope (TEM) observation. The diameter of nanowires was increased as heat treatment time is increased. The nanowires were identified to ${\beta}$-SiC single crystalline from X-Ray Diffraction(XRD) analysis. It was observed from this study that deposition temperature of samples was critical to the crystallization of nanowires. On the other hand, the effect of deposition time was insignificant.

• 청정기술
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• 제28권2호
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• pp.110-116
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• 2022

본 연구에서는 NdFeB 영구자석 스크랩으로부터 회수한 철(Fe) 부산물을 이용하여 산화철(FeO_x) 나노입자를 합성하였고, 열처리 온도가 FeO_x 나노입자의 물성에 미치는 영향을 관찰하였다. 이를 위해 D.I. water에 약 10 wt%로 희석한 철 부산물 용액에 2.0 M 암모니아(NH₄OH) 용액을 투여하여 산화철 전구체를 석출하였고, 이를 300 ℃, 400 ℃, 500 ℃ 및 600 ℃로 각각 열처리하여 FeO_x 나노 입자를 합성, 열처리 온도에 따른 FeO_x 나노 입자의 물성을 관찰하였다. X-ray diffraction (XRD) 분석 결과 열처리 온도가 증가할수록 <104> 회절 피크가 성장하여 500 ℃ 이상에서 α-Fe₂O₃ 결정구조와 일치하는 회절 피크가 검출되었다. BET (Brunauer-Emmett-Teller) 비표면적 분석 결과 400 ℃ 이상에서 열처리 온도가 증가할수록 비표면적이 감소하는 경향을 나타내었다. HRTEM (high resolution transmission electron microscope) 관찰 결과 rod 형 나노입자가 관찰되었고, 열처리 온도 증가에 따라 나노입자의 크기가 증가하는 경향을 나타내었다.

• Journal of the Korean Wood Science and Technology
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• 제23권4호
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• pp.67-73
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• 1995

This study was undertaken to investigate the effect of heat treatment on the dynamic viscoelasticity of three species of Phyllostachys bambusoides, Phyllostachys nigra var. henonis and Phyllostachys pubescens, grown in southern Korea. The bamboo was treated for 3~24 hours at $60{\sim}180^{\circ}C$, and then was treated in a climatic chamber for 3~48 hours at $40^{\circ}C$ and 95% relative humidity. The results obtained are summarized as follows : 1. Dynamic Young's modulus decreased with increasing temperature and duration of the heat treatment. 2. Internal friction decreased with increasing treatment duration. 3. Moisture absorption decreased with increasing temperature and duration of the heat treatment. 4. Dynamic viscoelasticity decreased, whereas internal friction slowly increased, with increasing moisture content.

• 한국전기전자재료학회논문지
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• 제11권7호
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• pp.502-507
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• 1998

The purpose of this study is to investigate the breakdown properties in joint interface of power cables with heat treatment. The specimens have the structure of XLPE/EPDM interface like the joint of distribution power cable. The breakdown characteristics of the SLPE/EPDM joint were studied with crosslinking by=products. AC breakdown voltages were measured with heat treatment time and interfacial materials and crosslinking by-products as testing factors. This study has shown that crosslinking by-product gases play an important role at the insulation properties of cable joints by heating. The dielectric strength shows the lowest values at 4 hours heat treatment. The AC breakdown strength in the untreated sample was increased with heat treatment time.

• Journal of Welding and Joining
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• 제4권2호
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• pp.21-29
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• 1986

The influence of welding heat input variation(600-900J/cm) and heat-treatment condition after welding on tensile strength of butt welded joint in $175Kg/mm^2$ strength level Maraging steel(Co-free and Co-containing) sheets was investigated on the basis of hardness distribution, microstructure of weld metal and fracture surface. The obtained main results are as follows; 1. The strength of weldment (UTS, NTS), joint efficiency showed a little decreasing tendency with the increase in welding heat input, and the elongation showed a little increasing tendency with the increase in the width of weld metal. It was considered because of the plastic constraint of the high strength base metal. 2. The strength of weldment was better in the solution treatment and aging than the aging only after welding due to the disappearance of almost denverite in weld metal. 3. The hardness distribution in weldment after welding and heat-treatment was almost similar to both Co containing and Co free Maraging steel with change in welding heat input. 4. The fracture was occurred at weld metal, and the fracture surface showed a relatively shallow dimples in both Co containing and Co free Maraging steel.

• Journal of Welding and Joining
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• 제14권4호
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• pp.89-98
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• 1996

This study was performed to establish the characteristics of the heat affected zones from view point of the repair weldability for a damaged CrMoV steam turbine rotor steel. Characterization of the heat affected zones of the weldment was conducted with respect to various of postweld heat treatment temperatures, $566^{\circ}C$, $621^{\circ}C$ and $677^{\circ}C$. The evaluations of the heat affected zones were carried out in terms of microstructural characterization, microhardness measurements, Charpy v-notch impact, tensile and stress-rupture tests. The results indicated that the effect of the postweld heat treatment at $677^{\circ}C$ exhibited the favorable microstructure and mechanical properties for the stability of the heat affected zones. While the heat affected zone of the weldment, produced without postweld heat treatment, displayed the inferior toughness and microstructure indicating localized carbide precipitations on the grain boundary. It was also indicated that the stability of the heat affected zones were deteriorated by the formation of the cavitation on the grain boundaries.