• Journal of the Korean Society for Precision Engineering
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• v.20 no.5
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• pp.140-147
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• 2003

As the huge energy transfer systems like as nuclear power plant and steam power plant are operated for a long time at a high temperature, mechanical properties are changed and ductile-brittle transition temperature is raised by degradation. So it is required to estimate degradation in order to assess the safety, remaining life and further operation parameters. The sub-sized specimen test method using surveillance specimen was developed for evaluating the integrity of metallic components. In this study, we would like to present the evaluation technique of the ductile-brittle transition temperature by the sub-sized specimen test. The four classes of the thermally aged 1Cr-1Mo-0.25V specimens were prepared using an artificially accelerated aging method. The tensile test and fracture toughness test were performed. The results of the fracture toughness tests using the sub-sized specimens were compared with the evaluation technique of the ductile-brittle transition temperature.

• Journal of the Korean Society for Heat Treatment
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• v.28 no.1
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• pp.1-6
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• 2015

The ductile-to-brittle transition behavior of two austenitic Fe-18Cr-10Mn alloys with the combined addition of nitrogen and carbon was investigated in this study. The alloys exhibited a ductile-to-brittle transition behavior because of unusual brittle fracture at low temperatures unlike conventional austenitic alloys. The alloy with higher carbon content had higher yield and tensile strengths than that with lower carbon content due to the solid solution strengthening effect resulting from carbon addition. However, the increase in carbon content promoted the occurrence of intergranular fracture, and thus deteriorated the impact toughness. In order to develop successfully the austenitic Fe-18Cr-10Mn alloys with the excellent combination of strength and toughness in the future, therefore, more systematic studies are required to find the appropriate amount and ratio of nitrogen and carbon.

• Korean Journal of Materials Research
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• v.23 no.7
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• pp.385-391
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• 2013

The influence of Cu and Ni on the ductile-brittle transition behavior of metastable austenitic Fe-18Cr-10Mn-N alloys with N contents below 0.5 wt.% was investigated in terms of austenite stability and microstructure. All the metastable austenitic Fe-18Cr-10Mn-N alloys exhibited a ductile-brittle transition behavior by unusual low-temperature brittle fracture, irrespective of Cu and/or Ni addition, and deformation-induced martensitic transformation occasionally occurred during Charpy impact testing at lower temperatures due to reduced austenite stability resulting from insufficient N content. The formation of deformation-induced martensite substantially increased the ductile-brittle transition temperature(DBTT) by deteriorating low-temperature toughness because the martensite was more brittle than the parent austenite phase beyond the energy absorbed during transformation, and its volume fraction was too small. On the other hand, the Cu addition to the metastable austenitic Fe-18Cr-10Mn-N alloy increased DBTT because the presence of ${\delta}$-ferrite had a negative effect on low-temperature toughness. However, the combined addition of Cu and Ni to the metastable austenitic Fe-18Cr-10Mn-N alloy decreased DBTT, compared to the sole addtion of Ni or Cu. This could be explained by the fact that the combined addition of Cu and Ni largely enhanced austenite stability, and suppressed the formation of deformation-induced martensite and ${\delta}$-ferrite in conjunction with the beneficial effect of Cu which may increase stacking fault energy, so that it allows cross-slip to occur and thus reduces the planarity of the deformation mechanism.

• Korean Journal of Materials Research
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• v.25 no.10
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• pp.559-565
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• 2015

The ductile-brittle transition behavior of two austenitic Fe-18Cr-10Mn-N-C alloys with different grain sizes was investigated in this study. The alloys exhibited a ductile-brittle transition behavior because of an unusual brittle fracture at low temperatures unlike conventional austenitic alloys. The alloy specimens with a smaller grain size had a higher yield and tensile strengths than those with a larger grain size due to grain refinement strengthening. However, a decrease in the grain size deteriorated the low-temperature toughness by increasing the ductile-brittle transition temperature because nitrogen or carbon could enhance the effectiveness of the grain boundaries to overcome the thermal energy. It could be explained by the temperature dependence of the yield stress based on low-temperature tensile tests. In order to improve both the strength and toughness of austenitic Fe-Cr-Mn-N-C alloys with different chemical compositions and grain sizes, more systematic studies are required to understand the effect of the grain size on the mechanical properties in relation to the temperature sensitivity of yield and fracture stresses.

• Korean Journal of Materials Research
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• v.23 no.11
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• pp.649-654
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• 2013

The effect of interstitial elements on the ductile-brittle transition behavior of austenitic Fe-18Cr-10Mn-2Ni alloys with different nitrogen and carbon contents was investigated in this study. All the alloys exhibited ductile-brittle transition behavior because of unusual low-temperature brittle fracture, even though they have a faced-centered cubic structure. With the same interstitial content, the combined addition of nitrogen and carbon, compared to the sole addition of nitrogen, improved the low-temperature toughness and thus decreased the ductile-brittle transition temperature (DBTT) because this combined addition effectively enhances the metallic component of the interatomic bonds and is accompanied by good plasticity and toughness due to the increased free electron concentration. The increase in carbon content or of the carbon-to-nitrogen ratio, however, could increase the DBTT since either of these causes the occurrence of intergranular fracture that lead to the deterioration of the toughness at low temperatures. The secondary ion mass spectroscopy analysis results for the observation of carbon and nitrogen distributions confirms that the carbon and nitrogen atoms were significantly segregated to the austenite grain boundaries and then caused grain boundary embrittlement. In order to successfully develop austenitic Fe-Cr-Mn alloys for low-temperature application, therefore, more systematic study is required to determine the optimum content and ratio of carbon and nitrogen in terms of free electron concentration and grain boundary embrittlement.

• Korean Journal of Materials Research
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• v.24 no.1
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• pp.13-18
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• 2014

In order to clarify the effect of Nb addition on the ductile-brittle transition property of sintered TiC, TiC-10 mol% Nb composites were researched using a three-point bending test at temperatures from room temperature to 2020 K, and the fracture surface was observed by scanning electron microscopy. It was found that the Nb addition decreases the ductile-brittle transition temperature of sintered TiC by 300 K and increases the ductility. The room temperature bending strength was maintained at up to 1800 K, but drastically dropped at higher temperatures in pure TiC. The strength increased moderately to a value of 320MPa at 1600 K in TiC-10 mol% Nb composites, which is 40% of the room temperature strength. Pores were observed in both the grains and the grain boundaries. It can be seen that, as Nb was added, the size of the grain decreased. The ductile-brittle transition temperature in TiC-10 mol% Nb composites was determined to be 1550 K. Above 1970 K, yieldpoint behavior was observed. When the grain boundary and cleavage strengths exceed the yield strength, plastic deformation is observed at about the same stress level in bending as in compression. The effect of Nb addition is discussed from the viewpoint of ability for plastic deformation.

• Journal of the Korean Institute of Gas
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• v.19 no.6
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• pp.62-66
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• 2015

Considering for plants and structure under extreme conditions is required for the successful design, especially temperature and pressure. The ductile-brittle transition temperature (DBTT) for the materials under extreme condition needs to be considered. In this study, A-grade mild steel for the LNG carrier and offshore plant was examined by performing low-temperature Charpy V-notch (CVN) impact tests to investigate DBTT and the fracture toughness. The absorbed energy decreased gradually with the experimental temperature, which showed an upper-shelf energy region, lower shelf energy region, and transition temperature indicating DBTT. In addition, the fracture surface morphologies of the mild steels indicated ductile fractures at the upper-shelf energy level, with wide and large-sized dimples, whereas a brittle fracture surface, where was observed at the lower-shelf energy level, with both large and small cleavage facets. Based on the experimental results, ductile brittle transition temperature was estimated in about $-60^{\circ}C$.

• Journal of Welding and Joining
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• v.21 no.6
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• pp.55-63
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• 2003

Welded joint generally has heterogeneity of strength, material, and fracture toughness and it is important to understand the characteristics of material strength and fracture of welded joint considering heterogeneous effect. Characteristics of strength and fracture of an undermatched joint under dynamic loading was studied by round-bar tension tests and thermal elastic-plastic analyses in this paper. The strength and fracture of the undermatched joints should be evaluated based on the effects of the strain rate and the temperature including temperature rise during the dynamic loading. The differences of fracture characteristics like such as ductile-to-brittle transition behavior are well precisely explained from the stress-strain distribution obtained by numerical analysis.

• Proceedings of the Korean Society of Machine Tool Engineers Conference
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• 1999.05a
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• pp.51-55
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• 1999

Recently, manufacturing work has been transformed to advanced technology intensive form from mass production with a little items required in the past. It was demanded that superior workpiece surface integrity. However, the study of ductile mode machining was proceeded actively.In this paper, it is developed Ultra-Micro Indentation Device using the PZT actuator. Experimentally, by using theUltra-Micro Indentation device, the micro fracture behavior of the silicon wafer was invesgated. It was possible that ductile-brittle transition point in ultimate surface of brittle material can be detected by adding an acoustic emission sensor system to the Ultra-Micro Indentation apparatus.

• Journal of the Korean Society of Manufacturing Technology Engineers
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• v.9 no.1
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• pp.38-44
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• 2000

The background of this study lies in he investigation of the formation mechanism of ductile mode(nkanometer-size) chips of brittle materials such as fine ceramics glass and silicon. As the first step to achieve this purpose this paper intends to observe the micro-deformation behavior of these materials in sub${\mu}{\textrm}{m}$ depth indentation tests using a diamond indentor. In this study it was developed Ultra-Micro Indentation. Device using the PZT actuator. Experimentally by using the Ultra-Micro Indentation device the micro fracture behavior of the silicon wafer was investigated. It was possible that ductile-brittle transition point in ultimate surface of brittle material can be detected by adding an acoustic emission sensor system to the Ultra-Micro Indentation appartus.