• Title/Summary/Keyword: dry heat sterilization

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The Effect of Heat Sterilization on the Surface Topography and the Tensile Properties in Various Nickel Titanium Wires Including a Korean Product (열멸균과정이 nickel titanium호선의 기계적 성질과 표면상태에 미치는 영향)

  • Kim, Byoung-Ho;Nahm, Dong-Seok;Yang, Won-Sik
    • The korean journal of orthodontics
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    • v.28 no.6 s.71
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    • pp.927-935
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    • 1998
  • The purpose of this study is to investigate the changes of mechanical properties and surface topography of various nickel titanium wires after heat sterilization for recycling with quantitative method. The materials used were four kinds of nickel titanium orthodontic wires including a Korean product. Experimental specimens were treated with two kinds of heat sterilization methods ; dry heat ($180^{\circ}C$, 60min) and autoclave ($121^{\circ}C$, 15-20psi, 30min). Mechanical properties were evaluated by tensile test with Instron 4466 (load cell capacity:.1000 kg, cross head speed:5mm/min, grip distince:40mm in room temperature). Surface topography of various wires was compared with each other qualitatively by using scanning electron microscopy and quantitatively by using profilometer. The findings were analyzed statistically with student t-tests. The results were as follows; 1. Neither method of heat sterilization had any effects on tensile properties of the nickel-titanium wires used in this experiment. 2. Before heat sterilization, the surface smoothness was highest in Optimalloy, followed by Align and Sentalloy, with NiTi showing the lowest smoothness value. 3. In surface topography, Align and Optimalloy were not influenced by heat sterilization. NiTi, on the other hand, had increased roughness after dry heat sterilization and Sentalloy showed the same tendency after each of the two heat sterilization procedures.

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Effects of Sterilizing Methods on the Content of Index .Constituents of Herbal Medicines (품질 보증을 위한 멸균법이 수종 생약의 지표성분 함량에 미치는 영향)

  • Jeong, Choon-Sik;Cho, So-Yean;Lee, Yong-Soo
    • YAKHAK HOEJI
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    • v.50 no.6
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    • pp.415-420
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    • 2006
  • The purpose of this study was to develop the best methods to sterilize herbal medicines which is frequently used and known to have high susceptibility to microbial contamination. We used dry heat, gamma irradiation and alcohol gas treatment for sterilization, and evaluated these methods in terms of the followings; i) the efficacy of sterilization, and ii) the chemical alteration of index constituents of herbal medicines. Treatment with dry heat effectively eliminated the contaminated microorganisms, and did not significantly alter the content of berberine chloride, paeoniflorin and amygdalin in Phellodendron Bark, Peony Root and Apricot Kernel, respectively: However it seriously changed the color and morphology which are essential criteria to estimate a measure of quality of herbal medicines. Treatment with gamma irradiation showed a strong sterilizing effect, and no alteration of the content of index constituents, color and morphology: Alcohol gas treatment resulted in similar effects as those in gamma irradiation. Collectively; these results suggest that treatment with gamma irradiation or alcohol gas may be useful methods for sterilizing herbal medicines without a decrease in their microbial quality.

Quality Characteristics and Functionality of Low Alcohol Wines after Heat Sterilization and Non-Thermal Sterilization (저알코올 와인의 가열 및 비가열 살균 후 품질 특성 및 기능성)

  • Shin, Hyerim;Park, Hyejin;Hwang, On Bit;Choi, Sungyeol;Park, Eui Kwang;Yoon, Dong Kyu;Yoon, Hyang-Sik
    • The Korean Journal of Food And Nutrition
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    • v.35 no.5
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    • pp.343-352
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    • 2022
  • Low alcohol (6%) wines were manufactured using Campbell Early. To develop the sterilization process of low alcohol wines, red wines were heat sterilized, and rose wines were nonthermal sterilized by concentration using potassium metasulfite and potassium sorbate. Samples were stored at 25℃ and quality characteristics were investigated by period. Results of this study revealed the pH of the samples after sterilization ranged from 3.15 to 3.19, and the total acidity of wines ranged from 0.011 to 0.024%. The free SO2 contents of wines ranged from 13.00 to 29.678 mg/L, and the total SO2 contents of wines ranged from 47.50 to 121.00 mg/L. L (lightness) of wines decreased whereas a (redness) and b(yellowness) increased. The hue value of wines ranged from 0.52 to 1.03, and decreased significantly(not including rose sweet wines). The color intensity of red and rose dry wines after sterilization increased, whereas red and rose sweet wines decreased. The DPPH radical scavenging activity of red wines and rose wines ranged between 75.50 to 89.23%, and 36.60 to 56.54%, respectively. The total polyphenol contents were 57.51~182.63 mg%. Results of this study provide scientific information to establish the sterilization process of low alcohol wines.

Effects of Sterilization for Quality Control and Content of baicalin in Scutellariae Radix (멸균법에 따른 황금의 미생물학적 품질보증과 바이칼린 함량에 미치는 영향)

  • Jeong, Choon-Sik
    • Korean Journal of Pharmacognosy
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    • v.36 no.3 s.142
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    • pp.220-223
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    • 2005
  • The purposes of this study was to develop the best one among the methods using dry heat, gamma irradiation and alcohol gas, to sterilize Scutellariae Radix selected based on high frequency of circulation between merchants and high susceptibility to microbial contamination, through comparing these methods in terms of the followings; ⅰ) the efficacy of sterilization in comparison with cost, and ⅱ)the alteration of chemical components of these herbal medicines. The results of this study will be taken advantage of establishment of the maximum limit of microorganism contaminated in herbal medicines. From the results of this study we conclude the followings: ⅰ) The sterilizing method using dry heat may be inappropriate, because it seriously changed their color and morphology which is an essential criterion to estimate a measure of quality between merchants and consumers, although it effectively got rid of contaminated microorganism and did not alter major components, baicalin; ⅱ) The sterilizing method using gamma irradiation may be appropriate, because it showed a strong sterilizing effect, and no alteration of chemical components, color and morphology; ⅲ)The sterilizing method using alcohol gas may also be appropriate, because it had a similar effects as in the case of gamma irradiation. Collectively, we suggest that appropriate sterilizing methods to guarantee the microbial quality of this herbal medicine may be those using gamma irradiation and alcohol gas.

Effects of Sterilization for Quality Control on the Content of Paeonol in Moutan Radicies Bark (품질 보증을 위한 멸균법이 목단피의 패오놀 함량에 미치는 영향)

  • Lee, Yong-Soo;Shin, Woon-Seob;Cho, So-Yean;Ze, Keum-Ryon;Lee, Hyo-Min;Jeong, Choon-Sik
    • YAKHAK HOEJI
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    • v.49 no.2
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    • pp.180-184
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    • 2005
  • The purpose of this study was to develop the best methods to sterilize Moutan Root Bark which is frequently used as a herbal medicine, and known to have high susceptibility to m icrobial contamination. We used dry heat, gamma irradiation and alcohol gas treatment for sterilization, and evaluated these methods in terms of the followings; I) the efficacy of sterilization, and ii) the chemical alteration of a major component of the harbal medicines. Treatment with dry heat effectively got rid of contaminated microorganisms, and did not significantly alter the content of paeonol. However it seriously changed the color and morphology which are an essential criterion to estimate a measure of quality of medicinal herbs. Treatment with gamma irradiation showed a strong sterilizing effect, and no alteration of the content of paeonol, color and morphology. Alcohol gas treatment resulted in similar effects as those in gamma irradiation. Collectively, these results suggest that appropriate sterilizing methods to guarantee the microbial quality of this herbal medicine may be those using gamma irradiation or alcohol gas.

Establishment of some Conditions for the Development of Legume Inoculant (근류균 접종제 개발을 위한 우수 증량제의 선발 및 생산 최적조건)

  • Kim, Chang-Jin;Rhee, Yoon;Yoo, Ick-Dong
    • Korean Journal of Soil Science and Fertilizer
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    • v.23 no.2
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    • pp.146-151
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    • 1990
  • The viability of rhizobia according to various kinds of carrier materials, inoculum size, storage temperature and sterilization methods was investigated for the development of legume inoculat. The results were followings. 1. Peat and perlite were favorable as a carrier material. 2. Rhizobia counts were reached to $5{\times}10^8cells/g$ carrier 1-2 weeks after inoculation with inoculum size below $10^4cells/g$ carrier. 3. $10^9cells/g$ carrier was maintained 12 weeks after storage at room temperature. 4. Steam heat sterilization was the best method for carrier sterilization among methods used in this study. Dry heat and ${\gamma}$-ray sterilization were also applicable.

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Biocontrol of Isolated Cronobacter spp. (Enterobacter sakazakii) by Heat, Sanitizer, and Antibiotic (열, 살균소독제, 항생제에 의한 분리 Cronobacter spp. (Enterobacter sakazakii) 제어)

  • Lee, Eun-Jin;Park, Jong-Hyun
    • Food Science of Animal Resources
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    • v.30 no.3
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    • pp.479-486
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    • 2010
  • Tolerance against heat, sanitizers, and antibiotics of 112 Cronobacter isolates classified by desiccation was determined to permit effective biocontrol in powdered foods. The isolates were classified into three groups: dry-tolerant (n=37), dry-sensitive (n=7), and dry-intermediate (n=68). The strains that were highly tolerant to drying also showed high heat tolerance that they seemed to have high tolerance to heat after dry stress in powdered foods like infant formula. Sodium hypochlorite and benzalkonium chloride concentrations necessary to achieve a 5-log reduction in viable counts (CFU/mL) were 15-25 ppm and 5-15 ppm, respectively. However, there was little difference of the efficacy of these sanitizers between dry-sensitive and -tolerant strains for planktonic cells suspended in 3% albumin. The minimal inhibition concentration (MIC) of $\beta$-lactam ampicillin was 64-128 ppm for 90% of the strains. The isolates were consistently sensitive to kanamycin and naldixic acid (MIC=4 ppm). Dry-tolerant strains displayed more antibiotic resistance than dry-sensitive strains. The results indicate that dry-tolerant Cronobacter isolates often possess heat and antibiotic resistance, indicated the need for potent sterilization treatments of powdered foods.

Estimation of Heat Sterilization Time of Chinese Laminae Species Used in The Production of Glue-laminated Board (집성재 제조용 중국산 층재 수종의 적정 열처리 시간 평가)

  • Kim, Min-Ji;Shin, Hyun-Kyeong;Kim, Gyu-Hyeok
    • Journal of the Korean Wood Science and Technology
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    • v.44 no.5
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    • pp.760-766
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    • 2016
  • This study explored the effects of heating temperature and laminae thicknesses on the time required to heat the center of air-dried Paulownia tomentosa, Pinus sp., Abies sp., and Larix sp. laminae to $56^{\circ}C$, which is a minimum core temperature of wood packaging materials defined by ISPM 15 standard, and maintain for 30 minutes in dry heat treatment schedule. Heating times were different among wood species and were Pinus sp. ${\geq}$ Abies sp. > Paulownia tomentosa > Larix sp. in decreasing order. The differences in heating times of some species were significantly different statistically, but were not different enough in practical terms to warrant heating four species separately. Heating times decreased as heating temperature increased and followed approximately power-function relationship. Also, heating times increased linearly with increasing laminae thickness. These relationships make it possible to calculate intermediate heating times relative to experimentally observed heating times. The results of this study will serve as a guideline for heat sterilization of Chinese laminae species to meet heat treatment requirements for protection against invasive pests.

Effect of supplementary glycerin on milk composition and heat stability in dairy goats

  • Thoh, Deela;Pakdeechanuan, Patcharin;Chanjula, Pin
    • Asian-Australasian Journal of Animal Sciences
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    • v.30 no.12
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    • pp.1711-1717
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    • 2017
  • Objective: This experiment was studied the effects of various levels of crude glycerin (CG) in dairy goat diet on daily intake, milk yield, milk composition, some physical properties and some quality changes of goat milk after sterilization. Methods: Twelve 75% Saanen dairy goats (body weight = $49{\pm}3kg$; days in milk = $60{\pm}12d$) were randomly assigned in a completely randomized design to evaluate the effects of three experimental diets consisting of 0%, 5%, and 10% CG (dry matter basis) which were formulated to meet or exceed the nutrient requirements of goats. Experimental dairy goats were evaluated for feed and milk yield. Milk samples were analyzed for their composition, including fatty acids, casein profile, fat globule size, and color, and were sterilized to evaluate milk heat stability. Results: There were no significant differences between 0% and 5% CG treatments infeed. Increasing CG supplementation from 0% to 5% increased milk yield from $2.38{\pm}0.12$ to $2.64{\pm}0.23kg/goat/d$. In addition, milk samples from 5% CG treatment had the highest total solids, fat content and lactose content, and largest fat globule size. Increasing CG to 10% resulted in a decrease in milk fat. After sterilizing at $116^{\circ}C$, $F_0=3min$, goat milk samples from 5% CG treatment had slightly higher sediment content and comparatively higher degree of browning. Conclusion: Considering milk yield, milk fat content and quality of sterilized milk, 5% CG supplementation in a total mixed ration has a potential for implementation in dairy goats.

Effects of heat treatments on the microbial reduction and germination rates of red radish sprout seeds (Raphanus sativus) (열처리 방법이 적무 새싹종자(Raphanus sativus)의 미생물 저감화 및 발아율에 미치는 영향)

  • Jun, So-Yun;Lee, Yeon-Kyung
    • Food Science and Preservation
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    • v.21 no.4
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    • pp.544-548
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    • 2014
  • This study was conducted to investigate the effects of various heat treatments on the microbial reduction and germination of red radish seeds for the development of effective and economical sterilization methods of improving microbial safety without reducting the germination rate. Hydrothermal treatment was conducted at 60, 65, 70, 75, 80, and $90^{\circ}C$ for 30 and 60 seconds, and dry heat treatment was performed at 70, 80, 90, and $100^{\circ}C$ for 5 minutes. In the seeds that underwent the hydrothermal treatment, time had little effect on the microbial reduction. There was no significant microbial reduction over time. However, there was significant microbial reduction as temperatures increased (p<0.001). The total plate count (TPC) was reduced by more than 3 logs, and Listeria monocytogenes was not detected at temperatures above $70^{\circ}C$. In the seeds that were subjected to the dry heat treatment, the TPC and the population of the L. monocytogenes were significantly reduced as the temperatures increased (p<0.001). After treatment at $100^{\circ}C$ for 5 minutes, the TPC and the L. monocytogenes were reduced by 3 logs. As with the microbial reduction, time had little effect on the germination. There were no significant changes in the germination after the hydrothermal treatment over time; but at the temperatures above $75^{\circ}C$, the germination rate significantly decreased as the temperature increased (p<0.001). When the seeds were soaked after the hydrothermal treatment, their germination was stimulated. The dry heat treatment at temperatures of $80^{\circ}C$ and higher significantly decreased the germination rate as the temperature increased (p<0.001). Dry heat treatment before the germination of the seeds soaked in distilled water for three hours significantly decreased the germination at temperatures greater than $90^{\circ}C$ (p<0.05). This study showed that appropriate heat treatments can increase the microbiological safety and germination of red radish seeds.