• Title/Summary/Keyword: distillation technique

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A study for cyclic Process technique of mineral base engine used oil resource (Engine 폐유 자원순환 기술에 관한 연구)

  • 김주항
    • Journal of the Korean Professional Engineers Association
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    • v.18 no.2
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    • pp.6-15
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    • 1985
  • A new process disregraded the H$_2$SO$_4$ treatment process heretofore in use, was developed and substituted for mineral base engine used oil of homemade SAE-30 grade H.V.I., which was used covering 4,500km, as samples, and the following results in research, was obtained. (1) A good quality of rerefinded base oil was obtained through roughly a course of developed processes of vacuum distillation process, solvent extraction process, neutralization treatment process and clay treatment process. (2) Through vacuum distillation process, the size of fine grains of insoluble colloid carbon that is, colloid carbon which was produced by burning of internal combustion engine oil and fuel, could be brought up and precipitated (3) The insoluble matters and admixtures could be easily dispersed and dissolved by mixing and extracting solvent disregarded the H$_2$SO$_4$ treatment process heretofore in use (4) waste matter heretofore called acid sludge in consequence of the process, did not appear at all. accordingly, the environmental pollution could be removed. (5) The troubles of corrosion to copper strip which was faults of the usual used oil refined products and peculiar offensive odor of the rerefined oil, could be solved through the neutralization process. (6) The yield of rerefined oil obtained through a course of processes was over 86 percent, and it is of practical use, not to speak of commercial value.

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In-Service Identification of the Heterogeneous Zone in Petrochemical Pipelines by Using Sealed Gamma-Ray Sources $(^{60}Co,\;^{137}Cs)$

  • Kim, Jin-Seop;Jung, Sung-Hee;Kim, Jong-Bum
    • Journal of the Korean Society for Nondestructive Testing
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    • v.26 no.3
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    • pp.169-173
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    • 2006
  • In-service diagnoses of pipeline facilities are important for a systematic maintenance of them. Field applications by using sealed gamma-ray sources $(^{60}Co,\;^{137}Cs)$ were performed to identify the heterogeneous zone in the pipelines of a distillation tower and a flare stack respectively. From the results, the heterogeneous zones in the pipelines were successfully identified. In the case of the pipeline connected to the distillation tower, a vapor pocket was detected in the fluid under hydrodynamic conditions, which could explain the reason for a decrease of the flow rate. In another case, an area with some amount of catalyst deposits was found at the bottom of the gas pipeline which was connected to the flare stack. And these findings provided important information for the process operators. Diagnosis technique by using gamma radiation sources has been proven to be an effective and reliable method for providing information on a media distribution in a facility.

Utilizing Mean Teacher Semi-Supervised Learning for Robust Pothole Image Classification

  • Inki Kim;Beomjun Kim;Jeonghwan Gwak
    • Journal of the Korea Society of Computer and Information
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    • v.28 no.5
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    • pp.17-28
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    • 2023
  • Potholes that occur on paved roads can have fatal consequences for vehicles traveling at high speeds and may even lead to fatalities. While manual detection of potholes using human labor is commonly used to prevent pothole-related accidents, it is economically and temporally inefficient due to the exposure of workers on the road and the difficulty in predicting potholes in certain categories. Therefore, completely preventing potholes is nearly impossible, and even preventing their formation is limited due to the influence of ground conditions closely related to road environments. Additionally, labeling work guided by experts is required for dataset construction. Thus, in this paper, we utilized the Mean Teacher technique, one of the semi-supervised learning-based knowledge distillation methods, to achieve robust performance in pothole image classification even with limited labeled data. We demonstrated this using performance metrics and GradCAM, showing that when using semi-supervised learning, 15 pre-trained CNN models achieved an average accuracy of 90.41%, with a minimum of 2% and a maximum of 9% performance difference compared to supervised learning.

Development of Machine Learning-Based Platform for Distillation Column (증류탑을 위한 머신러닝 기반 플랫폼 개발)

  • Oh, Kwang Cheol;Kwon, Hyukwon;Roh, Jiwon;Choi, Yeongryeol;Park, Hyundo;Cho, Hyungtae;Kim, Junghwan
    • Korean Chemical Engineering Research
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    • v.58 no.4
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    • pp.565-572
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    • 2020
  • This study developed a software platform using machine learning of artificial intelligence to optimize the distillation column system. The distillation column is representative and core process in the petrochemical industry. Process stabilization is difficult due to various operating conditions and continuous process characteristics, and differences in process efficiency occur depending on operator skill. The process control based on the theoretical simulation was used to overcome this problem, but it has a limitation which it can't apply to complex processes and real-time systems. This study aims to develop an empirical simulation model based on machine learning and to suggest an optimal process operation method. The development of empirical simulations involves collecting big data from the actual process, feature extraction through data mining, and representative algorithm for the chemical process. Finally, the platform for the distillation column was developed with verification through a developed model and field tests. Through the developed platform, it is possible to predict the operating parameters and provided optimal operating conditions to achieve efficient process control. This study is the basic study applying the artificial intelligence machine learning technique for the chemical process. After application on a wide variety of processes and it can be utilized to the cornerstone of the smart factory of the industry 4.0.

A Study on the Temperature Control of Vapor System Using Induction Heating (유도가열 증기발생장치의 온도제어)

  • Shin, Dae-Chul;Yoo, Jae-Hoon
    • Journal of the Korean Institute of Illuminating and Electrical Installation Engineers
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    • v.24 no.1
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    • pp.117-123
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    • 2010
  • Proposed induction-heated system is innovative system which applied special high-frequency power circuit technique for thermal converse technique and IH(Induction-Heating) magnetic induction heating generated from induction-heated metallic package that is for distillation unit. This electromagnetic induction heating technique is used high frequency inverter. By using high frequency inverter high frequency alternative current in the range of [kHz] can be made with conventional alternative current. In this contribution IGBT module is used for high frequency inverter. Resonant high frequency inverter make system of high capacity and high efficiency. This paper describes the temperature control of induction heating system hot air producer using the voltage-fed series resonant high-frequency inverter which can operate in the frequency range from 20 to 44[kHz].

Isolation of Sorbic Acid from the Mountain Ash Berries (I) (국산(國産) 건조(乾燥)마가목 열매로 부터 Sorbic Acid의 분리(分離)에 관한 연구(硏究) (I))

  • Lee, S.M.;Kim, C.E.;Joe, Y.I.;Tahk, H.K.
    • Korean Journal of Food Science and Technology
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    • v.4 no.1
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    • pp.1-5
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    • 1972
  • This investigation was primarily carried out to establish the optimum conditions for the separation of sorbic acid, as an enzyme inhibitor, from dry mountain ash berries. The berries were crushed to $35{\sim}40\;mesh$, and leached with water to produce a reddish juice, which was concentrated to syrup after evaporation. Parasorbic acid was separated from the syrup by steam distillation in the presence of acid. In this study, the optimum experimental results for separation of parasorbic acid were obtained as follows : (1) the most applicable leaching time of the dry ash berries was about 6 hours at room temperature and less than 4 hours at $40^{\circ}C$ and (2) in steam distillation, after removal of malic acid, addition of 30 ml of sulfuric acid per 50 ml of syrup extracted from 100 g of the ash berries was very adequate. The purity of sorbic acid obtained experimentally through the isomerization technique was qualitatively examined by spectrophotometeric, paper chromatographic, and melting point measurements.

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Study on Fishy Off-flavor in Porcine Liver by GC-O (GC-olfactometry를 이용한 돼지간의 비린내불쾌취 성분 연구)

  • Im, Sung-Im;Choi, Sung-Hee
    • Korean Journal of Food Science and Technology
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    • v.35 no.3
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    • pp.353-358
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    • 2003
  • Volatile compounds of porcine liver were collected by simultaneous steam distillation and extraction and steam distillation under reduced pressure. Volatiles were analyzed by gas chromatography (GC) and GC-mass spectrometry. Key aroma compounds of off-flavor in porcine liver were characterized using GC-olfactometry technique. Concentrates of cooked porcine liver had odor of a typical liver, fishy, and metallic off-flavor. Aroma concentrates showed over 90 peaks, of which 69 compounds were positively and/or tentatively identified. 1-Octen-3-one, 1-hexanol, (E)-2-nonenal, (Z)-4-decenal, (E,E)-2,4-heptadienal and (E,E)-2,4-decadienal were newly identified in this study. These compounds seem to be produced from unsaturated fatty acids of porcine liver by oxidation. 1-Octen-3-one (metallic), 1-hexanol (metallic) and (E,E)-2,4-heptadienal(fishy) have been implicated in fishy and metallic off-flavor in cooked porcine liver.

Analysis of Essential Oils from Korean Aromatic Tobacco Varieties by GC/MS and data system. (GC/MS와 data system을 이용한 한국산 향끽미종 잎담배의 정유성분 분석)

  • Park, Jeen-Woo;Lee, Un-Chul;Kim, Yong-Tae;Heu, Il
    • Journal of the Korean Society of Tobacco Science
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    • v.4 no.1
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    • pp.61-66
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    • 1982
  • Essential oil components were isolated from Korean aromatic tobaccos by using a simultaneous distillation and extraction apparatus. The essential oils were analyzed by GC/M S and date system. Forty-two volatile components were identified on the basis of their mass spectra. Determination of contents of essential oil components from Hyangcho and Sohyang was achieved by pseudo-multiple ion selection (Ml S) technique. Varietal differences were detected from the quantitative comparison of the MIS data.

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Operation of dry distillation process on the production of radionuclide 131I at Puspiptek area Serpong Indonesia, 2021 to 2022

  • Chaidir Pratama;Daya Agung Sarwono;Ahid Nurmanjaya;Abidin Abidin;Triyatna Fani;Moch Subechi;Endang Sarmini;Enny Lestari;Yanto Yanto;Kukuh Eka Prasetya;Maskur Maskur;Fernanto Rindiyantono;Indra Saptiama;Anung Pujiyanto;Herlan Setiawan;Tita Puspitasari;Marlina Marlina;Hasnel Sofyan;Budi Setiawan;Miftakul Munir;Heny Suseno
    • Nuclear Engineering and Technology
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    • v.56 no.4
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    • pp.1526-1531
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    • 2024
  • 131I is a fission product produced in a nuclear reactor by irradiating tellurium dioxide, with a half-life of 8.02 day. The most important and widely used method for making 131I is irradiation using a nuclear reactor and post-irradiation followed by dry distillation. The advantage of the dry distillation process is that the process and the equipment are relatively simple, namely TeO2 (m.p. 750 ℃), which can withstand heating during reactor irradiation. Based on TeO2 irradiation by neutron following the technique of dry distillation was explained for production of 131I on a large scale. A dry distillation followed the radioisotope production operation using the 30 MW GA Siwabessy nuclear reactor to meet national demand. TeO2 targets are 25 and 50 g irradiated for 87-100 h. The resulting 131I activity is 20.29339-368.50335GBq. According to the requirements imposed on the radionuclide purity of the preparation, the contribution of 131I training in the resulting preparation was not less than 99.9 %

Development a Two Step Heater Using Induction Heating Based on o High Frequency Resonant Inverter (고주파 공진형 인버터를 이용한 유도가열형 2단 히터)

  • Shin, Dae-Cheul;Kwon, Hyuk-Min
    • Journal of the Korean Institute of Illuminating and Electrical Installation Engineers
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    • v.19 no.7
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    • pp.81-86
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    • 2005
  • Proposed induction-heated system is innovative system which applied special high-frequency power circuit technique for thermal converse technique and IH(Induction-Heating) magnetic induction heating generated from induction-heated metallic package that is for distillation unit. In this occurs not burning, so that the working environment can be improved. This electromagnetic induction heating technique is used high frequency inverter. By using high frequency inverter high frequency alternative current (HFAC) in the range of [kHz] can be made with conventional alternative current In this contribution IGBT module is used for high frequency inverter. In this paper are discussed action analysis and characteristics analysis of 1.5[kW]-Class half-bridge resonant inverter system and resonant metallic packaged. In addition, by using this system,t how two step heating superheated steam generator is developed and application of system are also discussed.