• Title/Summary/Keyword: direct heat method

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Purification of Antioxidant substance from the stem bark of Rhus verniciflua

  • Kim, Jung-Bae
    • Proceedings of the Korean Journal of Food and Nutrition Conference
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    • 2001.12a
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    • pp.126-126
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    • 2001
  • The Rhus verniciflua contains alkly(en)-catechol type allergens with a saiurated or unsaturated alkly chain of 15 or 17 carbon atoms. It has been recognized as an extremely active allergen causing skin reactions similar In poison ivy. The allergic contact dermatitis induced by the urushiol is known to be mediated be T lymphocytes whicht specifically recognize the hepten urushiol. Therefore. direct use of this plant as a medicinal purpose might imply a considerable hazard in Korea. In this study, using the established method for the detoxification from the stem bark of Rhus verniciflua, an strong antioxidant substance was isolated and characterized DPPH (diphenypricryl hydrazyl) assay measures hydrogen atom-donating activity and hence provides a measure of free radical scavenging antioxidant activity. DPPH, a purple-colored stable free radical, is reduced to yellow-colored diphenylpicryl hydrazine by antioxidants to deducing agents. Antioxidative effects of the water extract from RV were measured by DPPH assay. Twenty microliters of the extract was added to 1ml of 100mM DPPH solution in ethanol The mixture was shaken and left to stand for 10min at room temperature. The crude water extracts was purified by using HPLC method with a DEAE (anionic type), CN, ODS column. The purified compound remained stable at pH 3.0-6,0, but unstable above pH 6.5. It was stable heat at 10$0^{\circ}C$ for 4 hours, but still had about 80% of residual activity after treatment at 10$0^{\circ}C$ for 5 hours. The elemental composition of the HR-EI mass spectrum at m/z 170.02 was estimated the empirical formula as $C_{7}$ $H_{6}$ $O_{5}$. $C_{10}$ $H_4$ $O_2$N$_1$, $C_{5}$ $H_4$ $O_4$N$_3$, $C_{8}$$H_2O$$_1$N$_4$. In antimicrobial test, no inhibition was observed against Gram-positive and negative bacteria. This compound was stronger than that of commercial antioxidant by DPPH test, such as BHT, BHC at the same concentration (20$\mu$g/ml).ml).

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Development of Remote Field Eddy Current Pipeline Inspection System (원격장 와전류 배관 탐상 시스템 개발)

  • Jeong, Jin-Oh;Yi, Jae-Kyung;Kim, Hyoung-Jean
    • Journal of the Korean Society for Nondestructive Testing
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    • v.21 no.5
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    • pp.556-560
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    • 2001
  • Remote field eddy current testing (RFECT) with through-wall transmission characteristic is being applied to pipes ranging from small tubes of heat exchanger to natural gas supply pipelines. Cast iron pipes with nominal diameter of 100mm are used primarily as the waterline pipes. The leakage of water occurs due to defects in the pipes caused by vibration of automobiles and corrosion. But, the use of direct inspection methods such as insertion of inspection equipment inside the pipelines has been limited due to its lack of economical efficiency. Economical development of inspection equipments is possible since RFECT method can be easily employed for system integration and quantitative evaluation of both inside and outside defects. In this study, the development of underground pipeline inspection system was tarried out by using RFECT method in consideration of the characteristics of waterline network. This paper specifically describes the design and production of RFECT pipeline inspection pig using centralizer mechanism, development of remote field eddy current signal acquisition and processing software, and review of RFECT system operation procedures.

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Combustion Characteristics Study using Hyper-mixer in Low-enthalpy Supersonic Flow (하이퍼 혼합기를 사용한 저엔탈피 초음속 유동장 내연소 특성 연구)

  • Kim, Chae-Hyoung;Jeung, In-Seuck
    • Journal of the Korean Society of Propulsion Engineers
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    • v.17 no.6
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    • pp.75-80
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    • 2013
  • In this study, a forced ignition method with a plasma jet torch is studied in Mach 2 laboratory scaled wind-tunnel. The hyper-mixer is used as a mixer. For two normal injection cases, the one is collided against a wedge plate of the hyper-mixer and the other is directly injected into the cold main flow. For the first case, the hyper-mixer disperses the injected fuel, leading to the mixing enhancement. Furthermore, the fuel-air mixture is provided into the plasma hot gas, which enhances the combustion performance. However, the direct injection into the main flow method spends amount of fuel without ignition in the cold supersonic flow. In the end, for the forced combustion, it is important to supply the fuel-air mixture into the heat source.

Characteristics of Plasma Sprayed TiO2-NiCr Conductive Heating Roll Coatings (가열 롤에서 플라즈마 TiO2-NiCr 용사피막의 특성)

  • Kang, Tae-Gu;Jin, Min-Seok;Ko, Young-Bong;Kim, Tae-Hyung;Cho, Sang-Hum;Park, Jung-Sik;Kim, Jong-Chul;Park, Kyeung-Chae
    • Journal of Welding and Joining
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    • v.25 no.4
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    • pp.28-34
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    • 2007
  • The heating unit of direct heating method manufactured as the plasma spray coating of $TiO_2/NiCr$ conductive heating material on the surface of heating unit in order to improve the disadvantages of indirect heating method. $TiO_2$ and NiCr (80wt.%Ni-20wt.%Cr) that had the properties of conduction and heating was chosen for the conductive heating material. The compositions of the composite powders were studied $TiO_2-30wt.%NiCr\;and\;TiO_2-10wt.%NiCr$. As the heating temperature was increased, the hardness of heating layer was increased because of the fine microstructure and the decrease of porosity. The adhesion strength was decreased for coarsening and connection of voids in the insulation layer, and the electrical resistivity of heating layer was increased for fine crack formation and growth. In this study, the best efficient sprayed coatings with heating unit was concluded as the plasma sprayed $TiO_2-10wt.%NiCr$ coatings that was heat treated at $300^{\circ}C$.

Clinical considerations for complete denture relining (의치상 첨상재의 종류와 임상적 고려사항)

  • Young-Eun Cho
    • Journal of Dental Rehabilitation and Applied Science
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    • v.40 no.2
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    • pp.39-45
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    • 2024
  • The residual alveolar ridge below the denture base undergoes physiologic changes over time, which results in the existing dentures becoming less accurate with the residual alveolar ridge. In addition, changes of the occlusal plane, decreasing in vertical dimension and loss of denture retention and facial support can occur. Consequently, denture relining may be required to accommodate these changes and ensure an ongoing close fit. Relining a denture can be performed directly on the chairside using autopolymerizing relining materials or indirectly in the laboratory using heat-cured relining materials. A direct relining method is not only simple but also time and cost effective. However, irritation or burning sensation of the mucosa can occur, and poor bonding of the relining material to the denture base can be cited as disadvantages. The indirect relining method exhibits relatively high bonding strength between the relining material and the denture base, but the patient might experience discomfort during relining process period. This report will examine the characteristics of relining materials, including those used in the relining of CAD-CAM dentures, and explore the clinical considerations for relining procedures.

The Enhancement of Recycling Processes Efficiency of Lithium Ion Batteries; A Review (리튬이온전지 재활용공정 효율 향상을 위한 공정개선 연구동향)

  • Kyoungkeun Yoo;Wonhwa Heo;Bumchoong Kim
    • Resources Recycling
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    • v.33 no.2
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    • pp.24-36
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    • 2024
  • The lithium-ion battery recycling process has been classified into direct recycling, hydrometallurgical process, and pyrometallurgical process. The commercial process based on the hydrometallurgical process produces black mass through pretreatment processes consisting of dismantling, crushing and grinding, heat treatment, and beneficiation, and then each metal is recovered by hydrometallurgical processes. Since all lithium-ion battery recycling processes under development conducts hydrometallurgical processes such as leaching, after the pretreatment process, to produce precursor raw materials, this article suggests a classification method according to the pretreatment method of the recycling process. The processes contain sulfation roasting, carbothermic reduction roasting, and alloy manufacturing, and the economic feasibility of the lithium-ion battery recycling process can be enhanced using unused by-products in the pretreatment process.

Evaluation of Amino Acid and Energy Utilization in Feedstuff for Swine and Poultry Diets

  • Kong, C.;Adeola, O.
    • Asian-Australasian Journal of Animal Sciences
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    • v.27 no.7
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    • pp.917-925
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    • 2014
  • An accurate feed formulation is essential for optimizing feed efficiency and minimizing feed cost for swine and poultry production. Because energy and amino acid (AA) account for the major cost of swine and poultry diets, a precise determination of the availability of energy and AA in feedstuffs is essential for accurate diet formulations. Therefore, the methodology for determining the availability of energy and AA should be carefully selected. The total collection and index methods are 2 major procedures for estimating the availability of energy and AA in feedstuffs for swine and poultry diets. The total collection method is based on the laborious production of quantitative records of feed intake and output, whereas the index method can avoid the laborious work, but greatly relies on accurate chemical analysis of index compound. The direct method, in which the test feedstuff in a diet is the sole source of the component of interest, is widely used to determine the digestibility of nutritional components in feedstuffs. In some cases, however, it may be necessary to formulate a basal diet and a test diet in which a portion of the basal diet is replaced by the feed ingredient to be tested because of poor palatability and low level of the interested component in the test ingredients. For the digestibility of AA, due to the confounding effect on AA composition of protein in feces by microorganisms in the hind gut, ileal digestibility rather than fecal digestibility has been preferred as the reliable method for estimating AA digestibility. Depending on the contribution of ileal endogenous AA losses in the ileal digestibility calculation, ileal digestibility estimates can be expressed as apparent, standardized, and true ileal digestibility, and are usually determined using the ileal cannulation method for pigs and the slaughter method for poultry. Among these digestibility estimates, the standardized ileal AA digestibility that corrects apparent ileal digestibility for basal endogenous AA losses, provides appropriate information for the formulation of swine and poultry diets. The total quantity of energy in feedstuffs can be partitioned into different components including gross energy (GE), digestible energy (DE), metabolizable energy (ME), and net energy based on the consideration of sequential energy losses during digestion and metabolism from GE in feeds. For swine, the total collection method is suggested for determining DE and ME in feedstuffs whereas for poultry the classical ME assay and the precision-fed method are applicable. Further investigation for the utilization of ME may be conducted by measuring either heat production or energy retention using indirect calorimetry or comparative slaughter method, respectively. This review provides information on the methodology used to determine accurate estimates of AA and energy availability for formulating swine and poultry diets.

Study of Elementary and Middle School Students' Consumption of Foods Cooked at High Heat (초등학생과 중학생의 고온가열조리식품 섭취실태조사 연구)

  • Lee, Joon-Kyoung;Yoon, Ki-Sun
    • Korean journal of food and cookery science
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    • v.26 no.6
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    • pp.685-698
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    • 2010
  • Acrolein is a highly toxic, reactive mutagenic aldehyde. Humans are exposed to acrolein vapors from overheated cooking oil, cigarette smoke, and combustion of organic products. In this study, we investigated elementary and middle school students' consumption of foods cooked at high heat, such as fried, direct fire, and indirect fire cooked foods. The subjects of this survey study were 265 fifth grade students and 396 middle school students nationwide. According to the results of the frequency test, broiled fish was the most frequently consumed, followed by fried fish, indirect cooked samgyebsal, and other fried foods, which were eaten more than three times per month. The total intake of foods cooked at high heat per child over 1 year was in the following order: Fried chicken(7.50 kg) > Samgeybsal(6.57 kg) > Broiled pork ribs(4.18 kg) > Broiled fish(4.12 kg) > Bulgogi(3.31 kg) > Fried dish(3.18 kg) > Pork cuttlet(3.17 kg) > Jeyukbockeum(3.13 kg) > Charcoal-broiled beef ribs(2.74 kg) > Roasted whole chicken(2.05 kg) > Dackochi(1.87 kg) > Tangsuyuk(1.87 kg) > Fried fish(1.83 kg) > Hamburger patties(1.21 kg) > Fried potato(1.01 kg) > Barbecue(0.95 kg) > Doughnut(0.80 kg) > Corn dog(0.66 kg) > Croquette(0.51 kg). The favorite cooking method was indirect fire cooking for beef, pork, and fish, whereas frying was preferred for chicken. The results of this study provide important data for assessment of acrolein exposure via foods cooked at high heat temperature. The results also indicate that children might be exposed to acrolein through consumption of foods cooked at high heat temperature, suggesting the need to promote education of proper food consumption behavior.

Electrode bonding method and characteristic of high density rechargeable battery using induction heating system (유도 가열 접합 시스템을 이용한 대용량 이차전지 전극의 접합 방법 및 특성)

  • Kim, Eun-Min;Kim, Shin-Hyo;Hong, Won-Hee;Cho, Dae-Kweon
    • Journal of Advanced Marine Engineering and Technology
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    • v.38 no.6
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    • pp.688-697
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    • 2014
  • In this study, electrode bonding technology needed for high density of rechargeable battery is studied, which is recently researched for electric vehicle, the small leisure vessel. For the alternative overcoming the limit of stacking amount able to be stacked by conventional ultrasonic welding, the low temperature bonding method, eligible for minimum of degeneration of chemical activator on the electrode surface which is generated by thermal effect as well as the increase of conductivity and tension strength caused by electrode bonding using filler metal, not using conventional direct heating on the electrode material method, is studied. Specifically to say, recently used more generally the ultrasonic welding and spot welding method are not usable for satisfying stable electric conductivity and bonding strength when much electrode is stacking bonded. If the electrical power is unreasonably increased for the welding, due to the effect of welding temperature, deformation of electrode and activating material degeneration are caused, and after the last packaging, decline of electrical output and generating heat cause to reduce stability of battery. Therefore, in this study, induction heating system bonding method using high frequency heating and differentiated electrode method using filler metal pre-treatment of hot dipping are introduced.

SOOT YIELD OF TURBULENT PREMIXED PROPANE-OXYGEN-INERT GAS FLAMES IN A CONSTANT-VOLUME COMBUSTOR AT HIGH PRESSURES

  • Bae, M.W.;Bae, C.W.;Lee, S.K.;Ahn, S.W.
    • International Journal of Automotive Technology
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    • v.7 no.4
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    • pp.391-397
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    • 2006
  • The soot yield has been studied by a premixed propane-oxygen-inert gas combustion in a specially designed disk-type constant-volume combustion chamber to investigate the effect of pressure, temperature and turbulence on soot formation. Premixtures are simultaneously ignited by eight spark plugs located on the circumference of chamber at 45 degrees intervals in order to observe the soot formation under high temperature and high pressure. The eight converged flames compress the end gases to a high pressure. The laser schlieren and direct flame photographs with observation area of 10 mm in diameter are taken to examine the behaviors of flame front and gas flow in laminar and turbulent combustion. The soot volume fraction in the chamber center during the final stage of combustion at the highest pressure is measured by the in-situ laser extinction technique and simultaneously the corresponding burnt gas temperature by the two-color pyrometry method. The changes of pressure and temperature during soot formation are controlled by varying the initial charging pressure and the volume fraction of inert gas compositions, respectively. It is found that the soot yield increases with dropping the temperature and raising the pressure at a constant equivalence ratio, and the soot yield in turbulent combustion decreases as compared with that in laminar combustion because the burnt gas temperature increases with the drop of heat loss for laminar combustion.