• 제목/요약/키워드: dipping temperature

검색결과 160건 처리시간 0.022초

침액 코오팅 방법에 의한 $TiO_2$ 박막의 제조와 광전기 화학전극의 응용에 관한 연구 (Preparation of $TiO_2$ Film by the Dip-Coating Method and its Application to Photo electrochemical Electrodes)

  • 정현채;안병두;김기선
    • 태양에너지
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    • 제9권1호
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    • pp.14-21
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    • 1989
  • Preparation of $TiO_2$ Film by the Dip-coating Method and its Application to photo-electrochemical Electrodes. $TiO_2$ film of n-type semiconductor has been of great interest as a material for solar energy conversion. For its practical application, the dip-coating method has been applied to prepare $TiO_2$ (anatase) film on the nesa glass substrate. Films up to about $1.8{\mu}m$ in thickness can be obtained by repeating the operation, dipping $\to$ pulling up $\to$ drying $\to$ heating at $500^{\circ}C$ for 10 minute. Heating temperature at $500^{\circ}C$ was adopted to convert $TiO_2$ gels into $TiO_2$ crystalline films. The $TiO_2$ films showed the maximum photocurrent ($14mA/cm^2$) at the film thickness of about $1.8{\mu}m$. It was also found that the additional heating at $500^{\circ}C$ for about 20 minutes improved remarkably the photo current of the $TiO_2$ films.

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Verticillium Wilt of Potato Caused by Verticillium albo-atrum in Daegwallyong Area in Korea

  • Kim, Jong-Tae;Ryu, Kyoung-Yul;Kim, Jeom-Soon;Hahm, Young-Il;Yu, Seung-Hun
    • The Plant Pathology Journal
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    • 제19권3호
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    • pp.184-187
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    • 2003
  • Verticillium wilt was first observed in 2001 on potatoes (Solanum tuberosum) cv. Superior at Daegwallyong area, one of the major seed potato producing areas in Korea. The wilted potato plants showed typical symptoms including gradual yellowing and interveinal necrosis. There was discoloration in the vascular tissues of the infected stems which turned light brown. Fungal isolates from discolored vascular tissues were whitish to creamy with folding on potato dextrose agar medium, where they used to produce resting dark mycelia but no micro-sclerotia. Conidiophores were septate with side branches, swelled at the base, and arranged in a whorl. Conidia were 2.5-11.2$\times$2.0-4.5 $\mu\textrm{m}$ um in size and were borne in small clusters at the tips of phialides. Optimal temperature range for mycelial growth was $25-30^{\circ}C$. Based on these cultural and morphological characteristics, the fungus was identified as Verticillium albo-atrum Reink & Berth. Pathogenicity tests by root dipping method revealed that the fungus caused the same symptoms as observed in naturally infected potato plants. This is the first report of Verticillium wilt on potato caused by Verticillium albo-atrum in Korea.

도자기 소지와 유약의 잔류 응력이 기계적 강도에 미치는 영향에 관한 연구 (A Study on the Effect of Residual Stress between Body and Glaze of Pottery on the Mechanical Strength)

  • 이진하;나은상;최성철
    • 한국재료학회지
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    • 제9권2호
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    • pp.181-187
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    • 1999
  • In this study, the effect of residual stress on mechanical strength was investigated with 1 kind of whiteware body and 4 kinds of glazes which are produced in succeeding ceramic art place. Using dipping method, the body was coated for different times in order to manipulate the coating thickness and sintered in the different temperatures ($1200^{\circ}C$, $1250^{\circ}C$, $1300^{\circ}C$, $1350^{\circ}C$) for two thus hours. The sintered bodies were characterized by XRD, EPMA, FEM and UTM in order to study the forming of reaction layer between body and glazes, residual stresses and the effects of residual stresses on mechanical strength of pottery. At $1300{\circ}C$, we obtained maximum density and mechanical strength. By the finite element method, the residual stresses in surface of body were minimum in specific thickness of glazes and the mechanical strength of body in that thickness of glazes showed maximum when the firing temperature was settled.

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면사의 효소가공 및 실켓 가공 (Bio-polishing and Silket Treatment of Cotton Yarns)

  • 배영환;이지완;손영아;김주혜;권미연;김의화;이승구
    • 한국염색가공학회지
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    • 제20권4호
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    • pp.15-20
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    • 2008
  • The cotton yarn was subjected to bio-polishing treatment with three commercial enzymes(Cellusoft L, Denimax-991L and Denimax-acid) to remove the fuzz on the cotton yarn. Also, enzyme treated cotton yarns were compared with singeing cotton yarns. Experimental variables of enzyme treated cotton yarn were as follow: concentration of enzyme solution and NaOH, dipping time, and processing temperature. The enzymatic treatments were evaluated by analyzing the effect on yarn count, twist contraction, evenness and tenacity. As the results, enzymatic treatment on cotton yarn induced same effects as the traditional singeing treatment. Also, silket treatment of cotton yarn after bio-polishing enhanced the tensile properties of the cotton yarn.

옥돔 건제품의 산화방지에 관한 연구 (INHIBITION OF OXIDATION IN DRIED YELLOW SEA BREAM BRANCHIOSTEGUS JAPONICUS JAPONICUS (HOUTTUYN))

  • 신필현;허종화;하봉석
    • 한국수산과학회지
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    • 제8권4호
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    • pp.213-216
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    • 1975
  • 항산화제 및 약제처리가 옥돔 건제품의 품질에 미치는 영향을 실험한 결과 Tenox-II가 가장 산패방지 효과가 좋았고, 다음이 BHA, sustane, NDGA였으며, EDTA, 솔빈산 칼리움, CTC, $\alpha-naphylamine$은 효과가 없었다. 옥돔은 $0.1\%$ Tenox-II용액에 침지처리하여 건조한 다음 PVC 필름에 포장하여 저장하면 4개월간 품질을 안정하게 유지할 수 있었다.

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연속성장법에 의한 Silicon 단결정 연속성장 (Silicon Single Crystal Growth by Continuous Crystal Growth Method)

  • 인서환;최성철
    • 한국결정성장학회지
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    • 제3권2호
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    • pp.117-124
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    • 1993
  • 연속성장법은 crystal growth chamber의 상부에 있는 reservoir에서 원료 분말을 연속적으로 공급하면서 도가니 하부에 용융대를 형성시킨 후, 종자결정을 용융대에 dipping하여 회전시키면서 아래로 끌어내려 단결정을 성장시키는 방법이다. 본 연구에서는 연속 성장법을 이용하여 silicon 단결정을 육성시켰으며 연속성장에 영향을 미치는 인자는 critical melt level, 원료공급속도, 성장속도, graphite crucible과 gruphite susceptor의 형태, work coil의 위치에 따른 graphite susceptor의 수직온도구배, 중력과 종자결정의 회전에 의한 원심력이 용융대의 안정화에 미치는 영향과 용융액 표면에서 일어나는 소결현상에 관해 고찰하였다.

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현장 도금 공정에서 PVC 여과지에 채취된 6가 크롬의 환원 (Reduction of Hexavalent Chromium Collected on PVC Filters in Field Electroplating Process)

  • 신용철;백남원;이광용;이병규;이지태
    • 한국환경보건학회지
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    • 제28권1호
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    • pp.41-49
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    • 2002
  • Recently, pilot studies showed an evidence of reduction of airborne hexavalent chromium, Cr(VI), on PVC filter during air sampling and storage. However, the information on this in the field was limited. Thus, we studied the reduction behaviors of airborne Cr(VI) on PVC filters during sampling and storage at three field electroplating operations. Regression between sampling time and the reduction (ratio of Cr(VI) to total Cr concentrations) was not statistically significant (p>0.05). However, the reductions in samples collected for 240 ~ 340 minutes were significantly higher than those for 30 - 60 minutes. On the other hand, another experiment showed a good correlation (r=0.96) between sampling time and the reduction without an exceptional value. Storage temperature was not a factor affecting the reduction of Cr(VI) collected on PVC filter. The loss of Cr(VI) samples stored in alkali solution (2% NaOH/3% Na$_2$CO$_3$) was significantly lower than that stored in vial according to NIOSH method (p<0.05). Thus, dipping Cr(VI) samples into alkali solution was a storage method to minimize tile reduction.

소취 섬유의 제조에 관한 연구 (IV) - 산화티탄(IV)을 이용한 소취 섬유의 제조 및 calcination 온도가 소취율에 미치는 영향 - (Study for the Preparation of Deodorizing Fiber (IV) - Preparations of Deodorizing Fibers using $TiO_2$ and Effects of Calcination Temperature on the Deodorant Activity -)

  • 박수민;오선화
    • 한국염색가공학회지
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    • 제15권3호
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    • pp.161-167
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    • 2003
  • The preparations of deodorizing fibers using $TiO_2$ have been investigated. The fibers were coated with $TiO_2$ for the purpose of deodorizing by dipping fibers into the $TiO_2$ sol solutions and calcined at $450^\circ{C}$, $500^\circ{C}$ and $750^\circ{C}$ for 1 h after coating. The surface structure of the coated fibers was studied with XRD on the different preparation conditions of calcination temperatures. The deodorizing function of the prepared fibers was studied by the determination of the decomposing capability for $NH_3,\;CH_3SH\;and\;CH_3CHO$. The deodorant activity(D.A.) of these deodoriBing fibers was measured by chromogenic gas detector tubes. The deodorizing effect of the prepared fibers were shown to be similar for the three model compounds; 5wt% $TiO_2$ sol solution calcined at $450^\circ{C}$ < 5 wt% $TiO_2$ sol solution calcined at $500^\circ{C}$< 5 wt% TiO$_2$ sol solution calcined at $750^\circ{C}$.

유기 트랜지스터를 위한 자가조립단층을 이용한 ITO의 습식 표면개질 (Wet Chemical Surface Modification of ITO by Self Assembled Monolayer for Organic Thin Film Transistor)

  • 지승현;김수호;고재환;박훈;이광훈;윤영수
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2007년도 하계학술대회 논문집 Vol.8
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    • pp.450-450
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    • 2007
  • Indium tin oxide (ITO), which is used as an electrode in organic thin film transistors (OTFT), was modified with a self-assembled monolayer (SAM) by wet chemical surface modification. The surface of the ITO was treated by dipping method in a solution of 2-chloroethane phosphonic acid (2-CEPA) at room temperature. The work function in the ITO which was modified with the SAM in the 2-CEPA had 5.43eV. A surface energy and a transmittance were unchanged in an error range. On this study, therefore, possibility of ohmic contact is showed in the interface between the ITO and the organic semiconductors. These results suggest that the treatment of the ITO with the SAM can greatly enhance the performance of the OTFT.

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스테인레스 강 안정화 YBCO 초전도선재의 접합 특성에 관한 연구 (A study on the bonding properties of YBCO coated conductors with stainless steel stabilizer)

  • 김태형;오상수;송규정;김호섭;고락길;신형섭
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2005년도 하계학술대회 논문집 Vol.6
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    • pp.262-263
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    • 2005
  • For mechanical and electrical stability and environment protection, Cu and stainless steel stabilizer is laminated to Ag layer to produce a composite neutral-axis(N-A) architecture in which the YBCO layer is centered between the oxide buffered metallic substrate and stabilizer strip lamination. this architecture allows the wire to meet operational requirements including stresses at cryogenic temperature, winding tensions, mechanical bending requirements thermal and electrical stability under fault conditions. we have experimentally studied mechanical properties of laminated stainless steel stabilizer on YBCO coated conductors. we have laminated YBCO coated conductors by continuous dipping soldering process. we have investigated lamination interface between solder and stabilizer, YBCO coated conductor. we evaluated bonding properties tensile / shear bonding strength, peeling strength laminated YBCO coated conductors.

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