• 한국전자현미경학회:학술대회논문집
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• 한국현미경학회 2004년도 제35차 춘계학술대회
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• pp.74-77
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• 2004

• 한국전자현미경학회:학술대회논문집
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• 한국현미경학회 1993년도 제24회 학술대회 연제 초록
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• pp.33-33
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• 1993

• 한국세라믹학회지
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• 제40권6호
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• pp.513-518
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• 2003

La/sub 2/3-x/Li/sub 3x/□/sub 1/3-2x/TiO₃ compounds with x=0.13 and 0.12 were prepared by slow cooling (x=0.13) and rapid quenching (x=0.12) into the liquid nitrogen after sintering at 1350℃ for 6 h. Their crystal structure has been determined by Rietveld refinement of both the powder neutron and X-ray diffraction data. From neutron diffraction data, we found that the main phase was not tetragonal (P4/mmm), but trigonal (R3cH). The refinement of neutron diffraction for the slow cooled samples were in a good agreement with a new model; a mixture of trigonal (R3cH, 45.7 wt％), tetragonal (p4/mmm, 37.0 wt％), and Li/sub 0.57/Ti/sub 0.86/O₂(pbnm, 17.2 wt%), but the quenched sample was found not to contain tetragonal (p4/mmm). X-ray diffraction data couldn't be well fitted because of the Poor scattering factor of lithium ions and the similar reflection patterns among trigonal (R3cH), tetragonal (p4/mmm), and cubic (Pm3m). We also knew that one transport bottlenecks is destroyed by one La vacancy in the case of trigonal (R3cH).

• Carbon letters
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• 제16권3호
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• pp.215-218
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• 2015

Carbon micro particles with dimple patterns were produced by electro-spraying a solution of pitch in tetrahydrofuran. Particle formation depended on separation in an electrical field and volatilization of the solvent. More than 80% of the obtained carbon exhibited an average particle size of less than 50 μm. X-ray diffraction analysis suggests that the carbon with dimple patterns has increased crystallinity after heat treatment.

• Molecules and Cells
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• 제43권3호
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• pp.298-303
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• 2020

Cryo-electron microscopy (cryo-EM) is now the first choice to determine the high-resolution structures of huge protein complexes. Grids with two-dimensional arrays of holes covered with a carbon film are typically used in cryo-EM. Although semi-automatic plungers are available, notable trial-and-error is still required to obtain a suitable grid specimen. Herein, we introduce a new method to obtain thin ice specimens using real-time measurement of the liquid amounts in cryo-EM grids. The grids for cryo-EM strongly diffracted laser light, and the diffraction intensity of each spot was measurable in real-time. The measured diffraction patterns represented the states of the liquid in the holes due to the curvature of the liquid around them. Using the diffraction patterns, the optimal time point for freezing the grids for cryo-EM was obtained in real-time. This development will help researchers rapidly determine high-resolution protein structures using the limited resource of cryo-EM instrument access.

• 한국결정성장학회지
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• 제27권5호
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• pp.223-228
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• 2017

Aluminum nitride (AlN) powder was successfully synthesized at low temperature via carbothermal reduction and nitridation (CRN) assisted by microwave heating. The synthesis processes of AlN powder were investigated with X-ray diffraction, FE-SEM, FT-IR and TGA/DSC. Aluminum nitrate was used as an oxidizer and aluminum source, urea as fuel, and glucose as carbon source. These starting materials were mixed with D.I water and reacted in a flask at $100^{\circ}C$ for 20 minutes. After the reaction was finished, black foamy intermediate product was formed, which was considered to be an amorphous $Al_2O_3$ particles through intermediate product obtained by solution combustion synthesis (SCS) at the results of X-ray diffraction patterns and FT-IR. This intermediate product was nitridated at temperatures of $1300^{\circ}C$ and $1400^{\circ}C$ in $N_2$ atmosphere by a microwave heating furnace and then decarbonated at $600^{\circ}C$ for 2 hours in air. It should be noticed from FE-SEM images that as nitridated particles, identified as AlN from X-ray diffraction patterns, are covered with carbon residues. After decarbonating the nitridated powders, the spherical pure AlN powders were obtained without alumina and their particle sizes were dependent on the nitridating temperature with high temperature of $1400^{\circ}C$ giving large particles of around 70~100 nm.

• 한국식품영양과학회지
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• 제21권6호
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• pp.672-676
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• 1992

동부와 녹두 전분 gel의 텍스쳐 비교에 관한 연구의 일환으로 저장중의 노화 특성을 노화속도, 결정화도의 변화 및 이장량을 측정하여 비교하였다. 두 시료 전분 gel(30%)을 $20^{\circ}C$에서 저장하여 Avrami방정식으로 계산한 시간 상수는 동부 전분 gel이 1.9215일, 녹두 전분 gel이 1.984일로 거의 비슷하였으며 노화된 시료 전분 gel(10%)의 X-선 회절도는 모두 2${\theta}$ ; $17.2^{\circ},$ $22^{\circ},$ $24.0^{\circ}$ 에서 peak를 보여 B도형을 나타냈다. 한편 이장량은 두 전분 gel(6~10%) 모두 농도가 낮을수록 많았고, 저장 1, 2일째에 가장 많았으며 그 이후로 이장량의 증가율은 서서히 둔화되어 저장 6일째에 농도와 시료에 따라 17~34.9%에 이르렀다.

• 한국통신학회논문지
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• 제16권10호
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• pp.934-940
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• 1991

본 논문에서는 새로운 양자화 방법을 도입하여 학습을 수행하는 단층 신경망을 광학적으로 구현하였다 본 논문의 시스템은 입력 마스크 위상형 홀로그램 회절격자. LCD, CCD 카메라 등으로 구성된다. 입력단의 뉴런과 출력단의 뉴런간의 연결은 홀로그램 회절격자를 이용하여 2차원 연결을 이루었으며, 회절광들의 세기를 같게 하기 위하여 진폭형 회절격자를 위상형 회절격자로 변환시켰다. 뉴런간의 가중치는 2진 양자화되어 LCD를 이용하여 나타내었고, 출력값은 CCD를 통하여 컴퓨터에 입력되어 가중치를 보정하며, 이 과정은 학습이 완료될 때가지 반복 수행된다. 실험은 학습도 (learning rate) 0.5, 0.9에 대하여 실행하였으며, 제안된 방식으로 학습을 무리없이 수행할 수 있음을 확인할 수 있었다.

• 한국전기전자재료학회논문지
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• 제27권12호
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• pp.797-802
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• 2014

In this study, in order to develop the capacitor composition ceramics with the good dielectric properties, $(Ba_{1-x}Ca_x)(Ti_{0.85}Zr_{0.12}Sn_{0.03})O_3$ (abbreviated as BCTZ) ceramics were prepared by the conventional solid-state reaction method. The effects of Ca substitution on the microstructure and dielectric properties was investigated. The X-ray diffraction patterns demonstrated that all the specimens showed perovskite phase, and secondary phases are indicated in the measurement range of X-ray diffraction. Also, all the specimens indicated an rhombohedron phase structure. It was identified from the X-ray diffraction patterns that the secondary phase formed in grain boundaries and then decreased the dielectric properties. For all the specimens, observed one peak was tetragonal cubic phase transition temperature($T_c$), which is located in the vicinity of room temperature.

• Current Optics and Photonics
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• 제2권2호
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• pp.140-146
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• 2018

In this paper, mesoscale optical surface structures are found to possess both geometric and wave optics features. The study reveals that geometric optic analysis cannot correctly predict the experimental results of light transmission or reflection by mesoscale optical structures, and that, for reliable analyses, a hybrid approach incorporating both geometric and wave optic theories should be employed. By analyzing the transmission patterns generated by the mesoscale periodic pyramid prism plates, we show that the wave optic feature is mainly ascribed to the edge diffraction effect and we estimate the relative contributions of the wave optic diffraction effect and the geometric refraction effect to the total scattering field distribution with respect to the relative dimension of the structures.