• Title/Summary/Keyword: degassing

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Effects of Additional Bubbling on RH Vacuum Degassing Process with Water Model Experiment (수모델을 사용한 RH 진공 탈가스장치에서의 추가 버블링 효과)

  • Jang, Young-Hwan;Kim, Young-Tae;Yi, Kyung-Woo
    • Korean Journal of Metals and Materials
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    • v.48 no.5
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    • pp.424-429
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    • 2010
  • In the RH process, it is possible to obtain quicker processing times by enhancing the decarburization rates at a low carbon range of steel melt through Ar gas injection into the vacuum vessel. The RH decarburization reaction was simulated through a dissolved oxygen removal reaction by injecting nitrogen into a 1/8 scale RH water model system. The gas nozzles for the N$_{2}$ injection into the vacuum vessel were located at the lowest level of the vessel's outer wall. The nitrogen bubbling in the vacuum vessel resulted in an increase in the reaction rate constant, which rose in accordance with an increase in the bubbling flow rate and number of nozzles used. However, there was almost no variation in the reaction rate constant, which depended on the horizontal positions of the bubbling nozzles.

Fabrication of $YBa_2Cu_3O_{7-{\delta}}$ Superconducting Coils with Polymer Binder (유기물 바인더를 사용한 $YBa_2Cu_3O_{7-{\delta}}$ 초전도 Coil의 제조)

  • 정해원;박승만;김재묵;김성수
    • Journal of the Korean Ceramic Society
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    • v.27 no.3
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    • pp.355-360
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    • 1990
  • One of the possible ways to make a flexible wire of high-Tc superconductiong ceramics is the extrusion of a mixture slurry of superconducting powder with an appropriate polymer binder. The fabrication procedure for $YBa_2Cu_3O_{7-{\delta}}$ superconducting coils with this plastic mass is described. The major factors limiting the formation of extruded wire are the binder content, powder size, and entrapped gas in the mixture slurries. The optimum content of binder for both good flexbility and strength of wire was estimated to be 30wt%. The finer the powder size is, the more homogeneous structure the extruded wire has. The vacuum degassing before extrusion was necessary to remove the entrapped gas in as-extruded wire. The formability of wire depends greatly on the wire radius and binder content. After burning out the binder and the successive sintering, the contacts between the superconducting grains could be made. The resistivity vs. temperature behavior measured in the final wire showed the transition temperature of 90K with narrow transition width. However, the critical current densities of these wires are much lower in comparison to those of conventional bulk specimens.

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PCL Infiltration into a BCP Scaffold Strut to Improve the Mechanical Strength while Retaining Other Properties

  • Kim, Min-Sung;Kim, Yang-Hee;Park, Ih-Ho;Min, Young-Ki;Seo, Hyung-Seok;Lee, Byong-Taek
    • Korean Journal of Materials Research
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    • v.20 no.6
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    • pp.331-337
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    • 2010
  • A highly porous Biphasic Calcium Phosphate (BCP) scaffold was fabricated by the sponge replica method with a microwave sintering technique. The BCP scaffold had interconnected pores ranging from $80\;{\mu}m$ to $1000\;{\mu}m$, which were similar to natural cancellous bone. To enhance the mechanical properties of the porous scaffold, infiltration of polycaprolactone (PCL) was employed. The microstructure of the BCP scaffold was optimized using various volume percentages of polymethylmethacrylate (PMMA) for the infiltration process. PCL successfully infiltrated into the hollow space of the strut formed after the removal of the polymer sponge throughout the degassing and high pressure steps. The microstructure and material properties of the BCP scaffold (i.e., pore size, morphology of infiltrated and coated PCL, compressive strength, and porosity) were evaluated. When a 30 vol% of PMMA was used, the PCL-BCP scaffold showed the highest compressive strength. The compressive strength values of the BCP and PCL-BCP scaffolds were approximately 1.3 and 2MPa, respectively. After the PCL infiltration process, the porosity of the PCL-BCP scaffold decreased slightly to 86%, whereas that of the BCP scaffold was 86%. The number of pores in the $10\;{\mu}m$ to $20\;{\mu}m$ rage, which represent the pore channel inside of the strut, significantly decreased. The in-vitro study confirmed that the PCL-infiltrated BCP scaffold showed comparable cell viability without any cytotoxic behavior.

The Early Detection of the Protein Toxin using Sanification and Fluorescent Dye in the Field (현장에서 초음파 파쇄와 형광시약을 이용한 단백질 독소의 조기 탐지)

  • Ha, Yeon-Chul;Choi, Ki-Bong;Kim, Seong-Joo;Choi, Jung-Do
    • KSBB Journal
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    • v.22 no.1
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    • pp.48-52
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    • 2007
  • This study was carried out to establish the optimum disruption condition of a sonificator for the protein toxin for the purpose of developing automatic biological agent detector equipped a sonificator. One of the best-known collisional quenchers is molecular oxygen, which quenches almost all known fluorophores. The sonification does an excellent job of degassing, which decreased the quenching effect and increased the fluorescence quantity. The fluorescence measurement for the protein using 0.7 X fluorescent dye concentration and above must be done in 1 minute and the fluorescence measurement for the protein using 0.3 X fluorescent dye concentration and below has to be done between 2 and 3 minute. The fluorescence quantity of the sonificatied protein sample was much higher that of the non-sonificatied protein sample. Sonificating the sample turned out to be favorable for the fluorescence measurement when measuring at the low protein concentration.

HEAT-TREATMENT OF LARGE-SCALE GLASS BACKPLANES IN A MUFFLE FURNACE (머플 가열로에서의 대면적 유리기판의 가열공정에 대한 열적 연구)

  • Kim, D.H.;Son, G.;Hur, N.;Kim, B.K.;Kim, H.J.;Park, S.H.
    • Journal of computational fluids engineering
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    • v.17 no.4
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    • pp.16-23
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    • 2012
  • Current display manufacturing processes apply thermal treatment of glass backplanes widely for hydrogen degassing, crystallization of thin-films, tempering, forming, and precompaction. Estimation of the characteristics of transient heating stages and thermal non-uniformities on a single glass substrate or in a stack of glasses are extremely helpful to understand non-homogeneity of mechanical and electronic features of nano/micro structures of end products. Based on simple heat transfer models and using an electric muffle furnace, temperature variations in a glass stack were predicted and measured for glass backplanes of $1.5{\times}1.85m^2$ in size and 0.7 mm in thickness. Except for the period of putting glass backplanes into the furnace, thermal radiation was the major heating mechanism for the treatment and theoretical predictions agreed well to the experimental temperatures on the backplanes. Using the theoretical model, thermal fields for a glass stack of glass-size, $2.2{\times}2.5m^2$, and of the number of sheets, 1 to 12, were calculated for practical design and manufacturing of the muffle furnace for large-scale displays, e.g. up to $8^{th}$ generation.

The Effect of Surface Defects on the Optical Properties of ZnSe:Eu Quantum Dots (ZnSe:Eu 양자점의 표면결함이 광학특성에 미치는 영향)

  • Jeong, Da-Woon;Park, Ji Young;Seo, Han Wook;Lim, Kyoung-Mook;Seong, Tae-Yeon;Kim, Bum Sung
    • Journal of Powder Materials
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    • v.23 no.5
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    • pp.348-352
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    • 2016
  • Quantum dots (QDs) are capable of controlling the typical emission and absorption wavelengths because of the bandgap widening effect of nanometer-sized particles. These phosphor particles have been used in optical devices, photovoltaic devices, advanced display devices, and several biomedical complexes. In this study, we synthesize ZnSe QDs with controlled surface defects by a heating-up method. The optical properties of the synthesized particles are analyzed using UV-visible and photoluminescence (PL) measurements. Calculations indicate nearly monodisperse particles with a size of about 5.1 nm at $260^{\circ}C$ (full width at half maximum = 27.7 nm). Furthermore, the study results confirm that successful doping is achieved by adding $Eu^{3+}$ preparing the growth phase of the ZnSe:Eu QDs when heating-up method. Further, we investigate the correlation between the surface defects and the luminescent properties of the QDs.

A Study of the Optimization Process Combination on the Ultrapure Water Treatment System (초순수 생산을 위한 최적공정 조합 평가)

  • Lee, Kyung Hyuk;Kim, Dong Gyu;Kwon, Boung Su;Jung, Kwan Sue
    • Journal of Korean Society of Environmental Engineers
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    • v.38 no.7
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    • pp.364-370
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    • 2016
  • In this paper, the technique that determines efficient process combinations for the ultrapure water production was studied. The ultrapure water is one of the industrial water used in industrial activity and required in the advanced technology integrated industry. It is produced by combined process including filtration, ion exchange processes, the reverse osmosis (RO) process, degassing (DG) process and UV-oxidation (UVox) process. An ultrapure water production process consists of 15-20 different water treatment unit process. In this study, a pilot plant was built and operated to research the design parameters for the individual process. Through the pilot plant operation, 19 effective combinations were optimized among various processes. And then, 11 of them satisfied the final quality of the ultrapure water. The stability and economic feasibility were evaluated about the final 11 process combinations.

PEI Hollow Fiber Membranes Modified with Fluorinated Silica Nanoparticles for the Recovery of Biogas from Anaerobic Effluents (불화 실리카로 개질된 폴리에테르이미드 중공사막을 이용한 혐기성 유출수로부터 바이오가스 회수)

  • Yun, Kang Hee;Wongchitphimon, Sunee;Bae, Tae-hyun
    • Membrane Journal
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    • v.30 no.5
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    • pp.326-332
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    • 2020
  • In this study, polymer-fluorinated silica composite hollow fiber membranes were fabricated and applied to a membrane contactor for the recovery of methane dissolved in the anaerobic effluent. To prepare the composite membranes, porous hollow fiber substrates were fabricated with Ultem®, a commercial polyetherimide (PEI). Subsequently, fluorinated silica particles were synthesized and coated on the surface via strong covalent bonding. Due to the high porosity, our membrane showed a CH4 flux of 8.25 × 10-5 ㎤ (STP)/㎠·s at the liquid velocity of 0.03 m/s which is much higher that that of commercial polypropylene membrane designed for degassing processes. This is attributed to our membrane's high porosity as well as a superior surface hydrophobicity (120~122°) resulted from the coating with fluorinated silica nanoparticles.

Study of Seal-off Triggered Vacuum Switch(TVS) for High Voltage and High Current (고전압 대전류용, Seal-off TVS(Triggered Vacuum Switch) 연구)

  • Park, S.S.;Han, Y.J.;Kim, S.H.;Kwon, Y.K.;Kim, S.H.;Park, Y.J.;Hong, M.S.;Nam, S.H.
    • Proceedings of the KIEE Conference
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    • 2002.07c
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    • pp.1823-1826
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    • 2002
  • The purpose of this experiment was to develope Triggered Vacuum Switch (TVS) for the high voltage and high current. The TVS has an array of rods of alternate polarity in which a fixed gap spacing is maintained between the rods. The cross section of each rod has trapezoidal shape. It consists of electrode, ceramic chamber, getter and trigger. Currently, triggered vacuum switch (TVS) with seal-off has been designed and fabricated at PAL. An experimentation and trigger devices for TVS were designed for testing characteristics of electricity. For making the prototype of TVS, it is developed of fabrication process and fined of electrode material. The fabrication of the TVS is a lot of process which have manufacturing of part, chemical clean, ceramic brazing and metal welding. The fabricated TVS is tested of leak for vacuum, hold-off voltage and conditioning of trigger system. The TVS has pinch-off after it is removed of gas in the TVS and activated of getter in degassing furnace. The prototype TVS tested about 20 kV, 75 kA, 83 ${\mu}s$ with 100 kJ capacitor bank and inductance 5 ${\mu}H$. This paper describes the results of tests and the characteristics of the switch.

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Performance of Air Fresher System for the Removal of Various Odorants Released from Foodstuffs

  • Kim, Ki-Hyun;Adelodun, Adedeji A.;Deep, Akash;Kwon, Eilhann E.;Jeon, Eui-Chan;Kim, Yong-Hyun;Jo, Sang-Hee;Lee, Min-Hee;Cho, Sung-Back;Hwang, Ok-Hwa
    • Asian Journal of Atmospheric Environment
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    • v.11 no.1
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    • pp.37-53
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    • 2017
  • The effectiveness of four air fresher (AF) systems was evaluated with respect to their removal efficiencies against offensive odorants. For this purpose, malodorous species were generated by exposing freshly cooked foods emitting odorants with levels moderately above their respective threshold values in a confined room. The deodorization efficiency of the four AF systems was then tested for a period of 30 min by estimating the extent of reduction in odorant levels after the operation of each AF. The removal efficiency of the four AF units against each odorant was evaluated as follows: (1) between AF products from different manufacturers, (2) between odorants and ultrafine particulate matter ($PM_{2.5}$), and (3) between operation and natural degassing. The average sorptive removal of odorants was generally <80% and considered less effective or non-effective relative to $PM_{2.5}$. Further examination of odor reduction, if evaluated in terms of odor indices like odor intensity (OI) and odor activity value (OAV), recorded a mean of 33% and 87%, respectively. The overall results of this study confirmed that all tested AF units were not effective to resolve odor problems created under our testing conditions.