• Journal of Korea Foundry Society
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• v.1 no.3
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• pp.14-18
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• 1981

The Mg-loss of AlSi 7% melts containing from 0 to 0.8% Mg during the Hexachloroethane tablet degassing was investigated. The results of the experiment was discussed in view of the free energy change and kinetics of $MgCl_2$ formation. The melts with Mg content less than 0.5% showed a Mg-loss proportional to Mg-content, while it was constant at about 24% of the weight of tablets, when Mg content of the melt became more than 0.5 %. The rate of Mg-loss was drastically reduced, when the amount of tablets used at a time increased ver a certain limit for a given melt quantity.

• Proceedings of the Korean Powder Metallurgy Institute Conference
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• 2006.09b
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• pp.716-717
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• 2006

Gas release behavior from aluminum and Al 7075 alloy powders during heating in argon was investigated by in-situ gas chromatography. Water vapor, hydrogen, carbon mono-oxide were detected as individual evolution spectra against heating temperature and time. The mechanisms of water and hydrogen evolutions were studied in detail for the determination of effective degassing condition. Magnesium in the alloy powder was found to lower the hydrogen evolution temperature to enhance overall hydrogen release.

• 대한치과보철학회:학술대회논문집
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• 1999.11a
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• pp.61-61
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• 1999

• The Journal of Korean Academy of Prosthodontics
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• v.27 no.2
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• pp.53-78
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• 1989

This study was taken to observe the changes of the residual stress in the alloy and to measure 3 dimensional distortions of the long span ceramo-metal bridge. The materials used in this study were Pors-on 4 (Pd-Ag alloy), and Ceramco and Vita VMK 68 powders. The residual stress of the alloy was measured on the six specimens (dia. 8m/m) by the X-ray diffraction stress analyzer according to the kind of ceramic powder and different measuring stages. And, for the measurement of the distortions, fifteen specimens of the anterior 8-unit ceramo-metal brige were fabricated and subjected to the 3-D coordinate measuring machine. Variables included the 2 kinds of a ceramic powder and the presence or absence of a splint bar at the cast metal framework. The measuring stages in both were after casting, after degassing and after glazing. The following conclusions were obtained : 1. The residual stress of the alloy showed increasing tendency for the tension by the ceramic fusing, but there was not significance. 2. The tendency of the distortions in the cast metal frameworks were decrease of the width, the anterior displacement and sagging. 3. The amount of the distortions at the degassing stage were greater than that at the ceramic fusing stage. 4. The splint bar was effective to control the distortion only at ceramic fusing stage. 5. The sagging distortion in the Ceramco firing were even through all measuring stages, but in the Vita firing, pronounced at degassing stage.

• Proceedings of the Korean Vacuum Society Conference
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• 2010.02a
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• pp.416-416
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• 2010

본 연구에서는 저가격, 대면적화를 위한 롤투롤 스퍼터를 설계&개발하고, 성막직전 PET 기판의 열처리 유무를 통한 ITO 박막을 성막 시킨 저항막 방식의 터치 패널용 투명 전극에 대하여 전기적, 광학적, 구조적, 표면적 특성을 분석하였다. 롤투롤 스퍼터는 degassing챔버와 스퍼터 챔버가 한 시스템에 구성되었고, Degassing 챔버는 좌우측의 Rewinder/Unwinder 롤러에 의해 감고 풀어지는 PET기판의 수분 및 가스를 중앙부에 위치한 히터를 통해 제거하며, 수분 제거 후 스퍼터 챔버로 옮겨진 1250 mm폭의 PET기판을 Unwinder/Rewinder 롤러에 장착하며, Unwinder 롤러로부터 풀려진 PET 기판은 guide 롤러를 거쳐 cooling drum과의 물리적 접촉에 의해 PET 기판의 냉각이 일어나게 된다. ITO 캐소드 전에 장착된 할로겐 히터 상부로 기판이 지나가면서 열처리가 진행되고 열처리 후 두 개의 ITO 캐소드 상부를 지나면서 연속적으로 ITO 박막이 PET 기판에 성막 되게 된다. ITO 박막의 주요 성막 변수인 DC Power, Ar/$O_2$ 가스 유량비, 기판의 속도는 최적으로 고정하고, 성막 직전 기판의 열처리에 유무에 따른 ITO박막의 필름을 각각 고온 챔버에서 $140^{\circ}C{\times}90min$ 동안 열처리를 통한 내열성 테스트를 진행하여 ITO 필름의 특성 향상을 비교 분석하였다. 분석을 위해 전기적 특성은 four-point probe로 측정했고, 투과도는 Nippon Denshoku사(社)의 COH-300A를 이용해 가시광(550nm)에서 분석했고, FE-SEM으로 ITO박막 의 표면 상태를 분석하였다. 또한 Bending Tester(Z-100)를 이용하여 기계적 안정성을 분석하였다. 성막직전 PET 기판의 열처리를 하지 않은 ITO박막은 고온의 챔버 에서 $140^{\circ}C{\times}90min$ 동안 내열성 테스트 후 면저항이 511($\omega/\Box$)에서 630($\omega/\Box$)으로 높아졌으나, 성막직전 열처리를 통한 ITO 박막인 경우에는 465($\omega/\Box$)에서 448($\omega/\Box$)로 안정화 되었고, 투과율은 성막직전 열처리를 통해 1%향상되어 89%를 보였고, 유연성 또한 보다 우수한 특성을 보였다. 표면 조도는 평균 0.416 nm의 낮은 값을 보였다. 이는 PET 기판의 degassing 공정 중 충분히 제거되지 않은 가스나 불순물을 성막직전 열처리 공정으로 충분히 제거하여 깨끗한 PET 기판 상에 ITO 박막을 성막시키고, 열처리시 기판에 주어진 열에너지에 의해 보다 밀도가 높은 ITO 박막이 성장했기 때문으로 사료 된다.

• Proceedings of the Korean Vacuum Society Conference
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• 2013.02a
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• pp.306-306
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• 2013

본 연구에서는 저가격, 대면적화를 위한 롤투롤 스퍼터를 이용하여, Index matching (히가시 야마 $125{\mu}m$)의 PET 기판 위에 ITO 박막을 성막 시킨 정전용량 방식의 터치 패널용 투명 전극에 대하여 전기적, 광학적, 구조적, 표면적 특성을 분석하였다. ITO 타겟은 미쓰이사(일본의) 주석 함량 5 wt%을 사용하였으며, 롤투롤 스퍼터는 degassing챔버와 스퍼터 챔버가 한 시스템에 구성되었고, Degassing 챔버는 좌우측의 Rewinder/Unwinder 롤러에 의해 감고 풀어지는 PET 기판의 수분 및 가스를 중앙부에 위치한 히터를 통해 제거하며, 수분 제거 후 스퍼터 챔버로 옮겨진 1,250 mm폭의 PET기판을 Unwinder/Rewinder 롤러에 장착하며, Unwinder 롤러로부터 풀려진 PET 기판은 guide 롤러를 거쳐 cooling drum과의 물리적 접촉에 의해 PET 기판의 냉각이 일어나게 된다. ITO 캐소드 전에 장착된 할로겐 히터 상부로 기판이 지나가면서 열처리가 진행되고 열처리 후 두 개의 ITO 캐소드 상부를 지나면서 연속적으로 ITO 박막이 PET 기판에 성막 되게 된다. ITO 박막의 주요 성막 변수인 DC Power, Ar/$O_2$ 가스 유량비, 기판의 속도는 최적으로 고정하고, 성막된 ITO박막의 필름을 각각 고온 챔버에서 $150^{\circ}C$도에서 10 min에서 60 min 동안 각각 열처리를 통한 내열성 테스트를 진행하여 ITO 필름의 특성 향상을 비교 분석하였다. 분석을 위해 전기적 특성은 four-point probe로 측정했고, 투과도는 Nippon Denshoku사(社)의 COH-300A를 이용해 가시광(550 nm)에서 분석했고, FE-SEM으로 ITO박막의 표면 상태를 분석하였다. 또한 Rolling Tester (Z-300)를 이용하여 기계적 안정성을 분석하였다.

• Proceedings of the KSME Conference
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• 2001.11a
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• pp.87-92
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• 2001

In this paper, high strength pressure vessel steels having the same chemical compositions were manufactured by the two different steel-making processes, such as vacuum degassing(VD) and electro-slag remelting(ESR) methods. After the steel-making process, they were normalized at $955^{\circ}C$, quenched at $843^{\circ}C$, and finally tempered at $550^{\circ}C$ or $450^{\circ}C$, resulting in tempered martensitic microstructures with different yielding strengths depending on the tempering conditions. Low-cycle fatigue(LCF) tests, fatigue crack growth rate(FCGR) tests, and fracture toughness tests were performed to investigate the fatigue and fracture behaviors of the pressure vessel steels. In contrast to very similar monotonic, LCF, and FCGR behaviors between VD and ESR steels, a quite difference was noticed in the fracture toughness. Fracture toughness of ESR steel was higher than that of VD steel, being attributed to the removal of impurities in steel-making process.

• Transactions of the Korean Society of Mechanical Engineers B
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• v.27 no.5
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• pp.612-619
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• 2003

This work experimentally studies the fundamental mechanisms by which the ultrasonic vibration enhances convection and pool boiling heat transfer. A thin platinum wire is used as both a heat source and a temperature sensor. A high speed video imaging system is employed to observe the behavior of cavitation and thermal bubbles. It is found that when the liquid temperature is below its boiling point, cavitation takes place due to ultrasonic vibration while cavitation disappears when the liquid reaches the boiling point. Moreover, when the gas dissolved in liquid is removed by pre-degassing, the cavitation arises only locally. Depending on the liquid temperature, heat transfer rates in convection, subcooled boiling and saturated boiling regimes are examined. In convection heat transfer regime, fully agitated cavitation is the most efficient heat transfer enhancement mechanism. Subcooled boiling is most enhanced when tile local cavitation is induced after degassing. In saturated boiling regime, acoustic pressure is shown to be a dominant heat transfer enhancement mechanism.

• Journal of the Korean Society of Tobacco Science
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• v.20 no.2
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• pp.205-209
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• 1998

This study was conducted to evaluate the effect of triacetin(TA) treatment during manufacturing carbon dual filter for the adsorption of cigarette smoke components by activated carbons. The measurements were carried out by separation of activated carbon from carbon dual filter, and the specific surface area analyzed. The specific surface area of activated carbon from the domestic cigarette filter and from the foreign cigarette filter by degassing at 9$0^{\circ}C$ was 163$\pm$32$m^2$/g, and 16.6$\pm$1.9$m^2$/g, respectively. Those values were very lower than that of degassing at 35$0^{\circ}C$ (Domestic brand: 952$\pm$30$m^2$/g, and Foreign brand: 847$\pm$73$m^2$/g). By comparing the adsorption capacity of acetone and benzene with and without triacetin treated activated carbon, there was a 20% reduction of adsorption capacity by 5% triacetin treatment. Also, from the cilia toxicity test with carbon dual filter treated 0 % TA and 8 % TA, the cilia survival time was 706$\pm$74sec. and 603$\pm$64sec. for 0% TA and 8% TA, respectively. The delivery rate of vapour phase of cigarette smoke, which consists of main components of cilia toxicity, was higher at 8% TA filter than 0 % TA filter. Our results indicate that the treated TA covered the micro-pore of activated carbon, and then reduced specific surface area, finally, decreased the adsorption of vapour phase from cigarette smoke.

• Journal of Technologic Dentistry
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• v.38 no.2
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• pp.69-77
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• 2016

Purpose: This study was to evaluate the shear bond strength of ceramic fused to Ni-Cr alloy(Alophaloy) by heat treatment. Methods: The specimens were divided into 5 groups according to heat treatment conditions prior to porcelain application. Eighteen specimens from each group were subjected to the shear load a universal testing machine using a 0.1mm/min cross-head speed and two specimens from each group were observed with SEM and EDX line profile. Results: The observation of the oxide film on the metal surface by SEM photograph showed a coarsening with an increasing degassing hold time. The diffusion of metal oxide was observed farther from the opaque layer in the heat treated specimen than no heat treated specimen. The shear bond strength measured highest to A5(55.23MPa) in the 10min holding group and measured lowest from A1(24.38MPa) in the no heat treated group, and there was a significant difference(p<0.05). Conclusion: The shear bond strength of Ni-Cr alloy improved in the heat treatment compared to the no heat treatment specimen.