• Title/Summary/Keyword: defect engineering

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Capping Intercrystalline Defects of Polycrystalline UiO-66 Membranes by Polydimethylsiloxane Coating (폴리다이메틸실록산 코팅을 통한 다결정성 UiO-66 분리막의 비선택적 결정립계 결함 캡핑)

  • Ik Ji Kim;Hyuk Taek Kwon
    • Clean Technology
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    • v.29 no.1
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    • pp.71-75
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    • 2023
  • In general, the presence of non-selective intercrystalline (grain boundary) defects in polycrystalline metal-organic framework (MOF) or zeolite membranes, which are known to be ca. 1 nm in size, causes lower membrane performance (selectivity) than the intrinsically expected. In this study we show that applying a thin polymeric coating of polydimethylsiloxane (PDMS) on a polycrystalline MOF membrane is effective to cap the non-selective intercrystalline defects and therefore improve membrane performance. To demonstrate the concept, first, polycrystalline UiO-66, one of Zr-based MOFs, membranes were prepared by an in-situ solvothermal growth. By controlling membrane growth condition with respect to growth temperature, we were able to obtain polycrystalline UiO-66 membranes at 150 ℃ with intercrystalline defects of which the quantity is not significant, so it can be plugged by the suggested PDMS deposition. Second, their performances were compared before and after the PDMS deposition. As expected, the PDMS deposition ended up with a noticeable increase in CO2/N2 ideal selectivity from 6 to 14, indicating successful intercrystalline defect plugging. However, the enhancement in CO2/N2 selectivity was accompanied by a significant reduction in CO2 permeance from 5700 to 33 GPU because the PDMS deposition not only plugs defects but also forms a continuous coating on membrane surface, adding an additional transport resistance.

Detection Fastener Defect using Semi Supervised Learning and Transfer Learning (준지도 학습과 전이 학습을 이용한 선로 체결 장치 결함 검출)

  • Sangmin Lee;Seokmin Han
    • Journal of Internet Computing and Services
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    • v.24 no.6
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    • pp.91-98
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    • 2023
  • Recently, according to development of artificial intelligence, a wide range of industry being automatic and optimized. Also we can find out some research of using supervised learning for deteceting defect of railway in domestic rail industry. However, there are structures other than rails on the track, and the fastener is a device that binds the rail to other structures, and periodic inspections are required to prevent safety accidents. In this paper, we present a method of reducing cost for labeling using semi-supervised and transfer model trained on rail fastener data. We use Resnet50 as the backbone network pretrained on ImageNet. At first we randomly take training data from unlabeled data and then labeled that data to train model. After predict unlabeled data by trained model, we adopted a method of adding the data with the highest probability for each class to the training data by a predetermined size. Futhermore, we also conducted some experiments to investigate the influence of the number of initially labeled data. As a result of the experiment, model reaches 92% accuracy which has a performance difference of around 5% compared to supervised learning. This is expected to improve the performance of the classifier by using relatively few labels without additional labeling processes through the proposed method.

Investigating InSnZnO as an Active Layer for Non-volatile Memory Devices and Increasing Memory Window by Utilizing Silicon-rich SiOx for Charge Storage Layer

  • Park, Heejun;Nguyen, Cam Phu Thi;Raja, Jayapal;Jang, Kyungsoo;Jung, Junhee;Yi, Junsin
    • Proceedings of the Korean Vacuum Society Conference
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    • 2016.02a
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    • pp.324-326
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    • 2016
  • In this study, we have investigated indium tin zinc oxide (ITZO) as an active channel for non-volatile memory (NVM) devices. The electrical and memory characteristics of NVM devices using multi-stack gate insulator SiO2/SiOx/SiOxNy (OOxOy) with Si-rich SiOx for charge storage layer were also reported. The transmittance of ITZO films reached over 85%. Besides, ITZO-based NVM devices showed good electrical properties such as high field effect mobility of 25.8 cm2/V.s, low threshold voltage of 0.75 V, low subthreshold slope of 0.23 V/dec and high on-off current ratio of $1.25{\times}107$. The transmission Fourier Transform Infrared spectroscopy of SiOx charge storage layer with the richest silicon content showed an assignment at peaks around 2000-2300 cm-1. It indicates that many silicon phases and defect sources exist in the matrix of the SiOx films. In addition, the characteristics of NVM device showed a retention exceeding 97% of threshold voltage shift after 104 s and greater than 94% after 10 years with low operating voltage of +11 V at only 1 ms programming duration time. Therefore, the NVM fabricated by high transparent ITZO active layer and OOxOy memory stack has been applied for the flexible memory system.

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Rotor Fault Detection of Induction Motors Using Stator Current Signals and Wavelet Analysis

  • Hyeon Bae;Kim, Youn-Tae;Lee, Sang-Hyuk;Kim, Sungshin;Wang, Bo-Hyeun
    • Proceedings of the Korean Institute of Intelligent Systems Conference
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    • 2003.09a
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    • pp.539-542
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    • 2003
  • A motor is the workhorse of our industry. The issues of preventive and condition-based maintenance, online monitoring, system fault detection, diagnosis, and prognosis are of increasing importance. Different internal motor faults (e.g., inter-turn short circuits, broken bearings, broken rotor bars) along with external motor faults (e.g., phase failure, mechanical overload, blocked rotor) are expected to happen sooner or later. This paper introduces the fault detection technique of induction motors based upon the stator current. The fault motors have rotor bar broken or rotor unbalance defect, respectively. The stator currents are measured by the current meters and stored by the time domain. The time domain is not suitable to represent the current signals, so the frequency domain is applied to display the signals. The Fourier Transformer is used for the conversion of the signal. After the conversion of the signals, the features of the signals have to be extracted by the signal processing methods like a wavelet analysis, a spectrum analysis, etc. The discovered features are entered to the pattern classification model such as a neural network model, a polynomial neural network, a fuzzy inference model, etc. This paper describes the fault detection results that use wavelet decomposition. The wavelet analysis is very useful method for the time and frequency domain each. Also it is powerful method to detect the features in the signals.

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A Study on the Fracture Behavior of a Two Dimensional Crack in Gas Pipelines Considering Constraint Effects (구속효과를 구려한 가스배관 결함의 2차원적 파괴거동 해석에 관한 연구)

  • Sim, Do-Jun;Jang, Yeong-Gyun;Choe, Jae-Bung;Kim, Yeong-Jin;Kim, Cheol-Man
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.25 no.1
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    • pp.61-69
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    • 2001
  • EFP(Fitness For Purpose) type defect assessment methodologies based on ECA(Engineering Critical Analysis) have been established and are in use for the structural integrity evaluation of gas pipelines. ECA usually includes the fracture mechanics analysis, and it is assumed that the J-integral uniquely characterizes the crack-tip stress-strain field. However, it has been proven that the J-integral alone can not be sufficient to characterize the crack-tip field under low levels of constraint with a single parameter. Since pipeline structures are made of ductile material, locally loaded in tension, cracks may experience low level of constraint, and therefore, J-dominance will be lost. For this reason, the level of constraint must be quantified to establish a precise assessment procedure for pipeline defects. The objective of this paper is to investigate the fracture behavior of a crack in gas pipeline(KS D 3507) by quantifying the level of constraint. For this purpose, tensile tests and CTOD tests were performed at room temperature(24$\^{C}$) and low temperature(-40$\^{C}$) to obtain the material properties. J-Q analyses were performed for SENB and SENT specimens based on 2-D finite element analyses, in order to investigate the in-plane constraint effects on pipeline defects. For precise assessment of cracks, especially shallow cracks, in KS D 3507 pipeline, constraint effect must be considered.

Effect of defects on lifetime of silicon electrodes and rings in plasma etcher (플라즈마 에쳐용 실리콘 전극과 링의 수명에 미치는 결함의 영향)

  • Eum, Jung-Hyun;Chae, Jung-Min;Pee, Jae-Hwan;Lee, Sung-Min;Choi, Kyoon;Kim, Sang-Jin;Hong, Tae-Sik;Hwang, Choong-Ho;Ahn, Hak-Joon
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.20 no.2
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    • pp.101-105
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    • 2010
  • Silicon electrode and ring in a plasma etcher those are in contact with harsh plasma suffer from periodic heating and cooling during their lifetime. This causes the silicon components failure due to thermal stress remaining the persistent slip bands (PSBs) on their surfaces. The factors that determine the lifetime of silicon electrode and ring were discussed with respect to silicon ingot. The impurity level and the average defect concentration measured with glow discharge mass spectrometer (GDMS) and microwave photo-conductance decay (${\mu}$-PCD) were compared with the grade of silicon ingots those are divided to slip-free and slip-allowed ingot. Some silp-allowed samples showed planar defects along <110> direction on {001} surface. The role of these defects was suggested from the viewpoint of the lifetime of silicon components.

Round Robin Analysis for Probabilistic Structural Integrity of Reactor Pressure Vessel under Pressurized Thermal Shock

  • Jhung Myung Jo;Jang Changheui;Kim Seok Hun;Choi Young Hwan;Kim Hho Jung;Jung Sunggyu;Kim Jong Min;Sohn Gap Heon;Jin Tae Eun;Choi Taek Sang;Kim Ji Ho;Kim Jong Wook;Park Keun Bae
    • Journal of Mechanical Science and Technology
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    • v.19 no.2
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    • pp.634-648
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    • 2005
  • Performed here is a comparative assessment study for the probabilistic fracture mechanics approach of the pressurized thermal shock of the reactor pressure vessel. A round robin consisting of one prerequisite deterministic study and five cases for probabilistic approaches is proposed, and all organizations interested are invited. The problems are solved by the participants and their results are compared to issue some recommendation of best practices and to assure an understanding of the key parameters in this type of approach, like transient description and frequency, material properties, defect type and distribution, fracture mechanics methodology etc., which will be useful in the justification through a probabilistic approach for the case of a plant over-passing the screening criteria. Six participants from 3 organizations responded to the problem and their results are compiled and analyzed in this study.

A Study on the Improvement of Plastic Boat Manufacturing Process Using TOC & Statistical Analysis (TOC와 통계적 분석에 의한 플라스틱보트 제조공정 개선에 관한 연구)

  • Yoon, Gun-Gu;Kim, Tae-Gu;Lee, Dong-Hyung
    • Journal of Korean Society of Industrial and Systems Engineering
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    • v.39 no.1
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    • pp.130-139
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    • 2016
  • The purpose of this paper is to analyze the problems and the sources of defective products and draw improvement plans in a small plastic boat manufacturing process using TOC (Theory Of Constraints) and statistical analysis. TOC is a methodology to present a scheme for optimization of production process by finding the CCR (Capacity Constraints Resource) in the organization or the all production process through the concentration improvement activity. In this paper, we found and reformed constraints and bottlenecks in plastic boat manufacturing process in the target company for less defect ratio and production cost by applying DBR (Drum, Buffer, Rope) scheduling. And we set the threshold values for the critical process variables using statistical analysis. The result can be summarized as follows. First, CCRs in inventory control, material mix, and oven setting were found and solutions were suggested by applying DBR method. Second, the logical thinking process was utilized to find core conflict factors and draw solutions. Third, to specify the solution plan, experiment data were statistically analyzed. Data were collected from the daily journal addressing the details of 96 products such as temperature, humidity, duration and temperature of heating process, rotation speed, duration time of cooling, and the temperature of removal process. Basic statistics and logistic regression analysis were conducted with the defection as the dependent variable. Finally, critical values for major processes were proposed based on the analysis. This paper has a practical importance in contribution to the quality level of the target company through theoretical approach, TOC, and statistical analysis. However, limited number of data might depreciate the significance of the analysis and therefore it will be interesting further research direction to specify the significant manufacturing conditions across different products and processes.

Optimum design and vibration control of a space structure with the hybrid semi-active control devices

  • Zhan, Meng;Wang, Sheliang;Yang, Tao;Liu, Yang;Yu, Binshan
    • Smart Structures and Systems
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    • v.19 no.4
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    • pp.341-350
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    • 2017
  • Based on the super elastic properties of the shape memory alloy (SMA) and the inverse piezoelectric effect of piezoelectric (PZT) ceramics, a kind of hybrid semi-active control device was designed and made, its mechanical properties test was done under different frequency and different voltage. The local search ability of genetic algorithm is poor, which would fall into the defect of prematurity easily. A kind of adaptive immune memory cloning algorithm(AIMCA) was proposed based on the simulation of clone selection and immune memory process. It can adjust the mutation probability and clone scale adaptively through the way of introducing memory cell and antibody incentive degrees. And performance indicator based on the modal controllable degree was taken as antigen-antibody affinity function, the optimization analysis of damper layout in a space truss structure was done. The structural seismic response was analyzed by applying the neural network prediction model and T-S fuzzy logic. Results show that SMA and PZT friction composite damper has a good energy dissipation capacity and stable performance, the bigger voltage, the better energy dissipation ability. Compared with genetic algorithm, the adaptive immune memory clone algorithm overcomes the problem of prematurity effectively. Besides, it has stronger global searching ability, better population diversity and faster convergence speed, makes the damper has a better arrangement position in structural dampers optimization leading to the better damping effect.

Static behavior of stud shear connectors with initial damage in steel-UHPC composite bridges

  • Qi, Jianan;Tang, Yiqun;Cheng, Zhao;Xu, Rui;Wang, Jingquan
    • Advances in concrete construction
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    • v.9 no.4
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    • pp.413-421
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    • 2020
  • For steel-concrete girders made composite using shear studs, initial damage on studs induced by weld defect, unexpected overloading, fatigue and others might degrade the service performance and even threaten the structural safety. This paper conducted a numerical study to investigate the static behavior of damaged stud shear connectors that were embedded in ultra high performance concrete (UHPC). Parameters included damage degree and damage location. The material nonlinear behavior was characterized by multi-linear stress-strain relationship and damage plasticity model. The results indicated that the shear strength was not sensitive to the damage degree when the damage occurred at 2/3d (d is the stud diameter) from the stud root. An increased stud area would be engaged in resisting shear force as the distance of damage location from stud root increased and the failure section becomes inclined, resulting in a less reduction in the shear strength and shear stiffness. The reduction factor was proposed to consider the degradation of the shear strength of the damaged stud. The reduction factor can be calculated using two approaches: a linear relationship and a square relationship with the damage degree corresponding to the shear strength dominated by the section area and the nominal diameter of the damaged stud. It was found that the proposed method is preferred to predict the shear strength of a stud with initial damage.