• Title/Summary/Keyword: curing rate test

검색결과 122건 처리시간 0.021초

경화단계에서의 1성분형 실리콘 실란트의 거동대응성능에 관한 실험적 연구 (Experimental Study of the Joint Movement Responsiveness Performance to the One-Component Silicon Sealants at Curing Phase)

  • 손종원;오노 타다시
    • 한국건축시공학회:학술대회논문집
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    • 한국건축시공학회 2014년도 추계 학술논문 발표대회
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    • pp.63-64
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    • 2014
  • In this study, we has a purpose to estimate the joint movement responsiveness performance for the domestic products of one-component structural silicon sealants. For this purpose, we make a comparative study for the four domestic products focused on tensile properties after allowed the cyclic-movements for three days at initial step of curing phase. A joint movement range ±10% and the rate of compression and extension 3.2mm/h were assumed in those tests. As a result, the large space were induced inside the sealant by rupture, and then adhesion and cohesion failures were caused by stress concentration. The tensile properties were reduced by 15~60% in comparison with physical properties. In this case, the generating defect was caused and the service-life was decreased. Thus, further researches as relationship of test condition and products properties on this behavior would be studied.

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콘크리트 타설 초기온도가 압축강도에 미치는 영향 (An Effect on Early Temperature of Placing Concrete Affecting Compressive Strength of Concrete)

  • 박대오;박영신;박재명;강연우;전병채
    • 한국콘크리트학회:학술대회논문집
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    • 한국콘크리트학회 2008년도 춘계 학술발표회 제20권1호
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    • pp.641-644
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    • 2008
  • 콘크리트의 압축강도는 시멘트 수화반응에 의하여 발현되는 것으로, 이러한 수화반응은 온도에 민감한 영향을 받게 된다. 이에 본 연구에서는 온도에 의한 콘크리트의 영향을 확인하고자 콘크리트의 타설 초기온도 변화 및 양생 조건의 변화에 따른 특성을 실험적으로 평가하였다. 콘크리트의 타설 초기온도를 5$^{\circ}C$, 20$^{\circ}C$로 변화시켜 실험한 결과, 표준양생을 실시한 경우 타설 온도가 낮은 배합에서 재령 3일 이전까지 강도가 낮았으나, 재령 7일 이후에서는 강도가 높아지는 현상이 확인 되었다. 그러나 재령 28일에서는 두 배합의 압축강도 차가 미미하여 온도에 따른 영향이 크지 않은 것으로 확인 되었다. 기건양생을 실시한 경우는 모든 시험체에서 타설 초기온도가 높은 배합이 높은 강도를 나타내었다. 이러한 콘크리트의 타설 초기온도에 따른 압축강도 특성은 SEM관찰 결과 미세구조의 수화양상을 통하여 그 특성을 확인할 수 있었다.

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양생온도변화에 따른 콘크리트의 재료역학적 특성 (Mechanical Properties of Concrete with Different Curing Temperature)

  • 김진근;한상훈;양은익;조명석;우상균
    • 한국콘크리트학회:학술대회논문집
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    • 한국콘크리트학회 1997년도 가을 학술발표회 논문집
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    • pp.117-124
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    • 1997
  • In this study, mechanical properties of type V cement concrete with different curing temperature were investigated. The tests for mechancial properties, i.e., compressive strength and modulus of elasticity, were carried out on two kinds of type V cement concrete mixes. concrete cylinders cured at 10, 23, 35 and 50℃ were tested at 1, 3, 7 and 8 days. The 'rate constant model' was used to described the combined effects of time and temperature on compressive strength development. Test results show that concrete subjected to high temperature at early age attains greater strength than concrete to low temperature but eventually attains lower later-age strength than that. With type V cement concrete, the linear and Arrhenius rate constant models both accurately describe the development of relative strength as afunction of the equivalent age.

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액상봉지재용 Diglycidyl Ether of Bisphenol F/Nadic Methyl Anhydride 수치 시스템의 경화 및 유변학적 거동 (The Cure and Rheological Behavior of Diglycidyl Ether of Bisphenol F /Nadic Methyl Anhydride Resin System for Liquid Encapsulant)

  • 김윤진;김창제;윤호규
    • 한국마이크로전자및패키징학회:학술대회논문집
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    • 한국마이크로전자및패키징학회 2002년도 춘계 기술심포지움 논문집
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    • pp.152-157
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    • 2002
  • The cure and rheological behavior of Diglycidyl ether of bisphenol F, catalyzed by four kinds of imidazoles and a Nadic methyl anhydride curing agent were studied using a differential scanning calorimeter (DSC) and rheometer. The isothermal traces were employed to analyze cure reaction. The DGEBF/anhydride conversion profiles showed autocatalyzed reaction characterized by maximum conversion rate at 20~40 % of the reaction. The rate constants obtained from isothermal test showed temperature dependance, but reaction order did not. The order of reaction (m+n) was calculated to be close to 3. The measurements of viscosity and relation time in the presence of inorganic fillers were carried out at different isothermal curing temperatures. The viscosity and gelation time increased with filler content at the same isothermal temperature.

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플랜트 생산 재활용 상온 혼합물의 도로 표층 적용성에 관한 기초연구 (Fundamental Study on the Application of a Surface Layer using Cold Central-Plant Recycling)

  • 최준성
    • 한국도로학회논문집
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    • 제20권1호
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    • pp.69-76
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    • 2018
  • PURPOSES : This study determined the optimal usage rate of RAP (reclaimed asphalt pavement) using cold central-plant recycling (CCPR) on a road-surface layer. In addition, a mixture-aggregate gradation design and a curing method based on the proposed rate for the surface-layer mix design were proposed. METHODS : First, current research trends were investigated by analyzing the optimum moisture content, mix design, and quality standards for surface layers in Korea and abroad. To analyze the aggregate characteristics of the RAP, its aggregate-size characteristics were analyzed through the combustion asphalt content test and the aggregate sieve analysis test. Moreover, aggregate-segregation experiments were performed to examine the possibility of RAP aggregate segregation from field compaction and vehicle traffic. After confirming the RAP quality standards, coarse aggregate and fine aggregate, aggregate-gradation design and quality tests were conducted for mixtures with 40% and 50% RAP usage. The optimum moisture content of the surface-layer mixture containing RAP was tested, as was the evapotranspiration effect on the surface-layer mixture of the optimum moisture content. RESULTS : After analyzing the RAP recycled aggregate size and extraction aggregate size, 13-8mm aggregate was found to be mostly 8mm aggregate after combustion. After using surface-chipping and mixing methods to examine the possibility of RAP aggregate segregation, it was found that the mixing method contributed very little for 3.32%, and because the surface-chipping method applied compaction energy directly as the maximum assumption the separation ratio was 15.46%. However, the composite aggregate gradation did not change. Using a 40% RAP aggregate rate on the surface-layer mixture for cold central-plant recycling satisfied the Abroad quality standard. The optimum moisture content of the surface-layer mixture was found to be 7.9% using the modified Marshall compaction test. It was found that the mixture was over 90% cured after curing at $60^{\circ}C$ for two days. CONCLUSIONS : To use the cold central-plant recycling mixture on a road-surface layer, a mixture-aggregate gradation design was proposed as the RAP recycled aggregate size without considering aggregate segregation, and the RAP optimal usage rate was 40%. In addition, the modified Marshall compaction test was used to determine the optimum moisture content as a mix-design parameter, and the curing method was adapted using the method recommended by Asphalt Recycling & Reclaiming Association (ARRA).

함수비, 양생온도 및 흙의 입도가 Soil-Cement의 압축강도에 미치는 영향에 관한 연구(I) (Studies on the Effect of Water Content, Curing Temperature and Grain Size Distribution of Soils on Unconfined Compressive Strength of Soil-Cement Mixtures.)

  • 김재영;강신업
    • 한국농공학회지
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    • 제19권1호
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    • pp.4312-4322
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    • 1977
  • In order to investigate the effect of the water content and the accelerated curing on the strength of the soil-cement mixtures, laboratory test of soil cement mixtures was performed at five levels of water content, four levels of accelerated curing temperatures, three levels of normal curing periods, and six levels of accelerated curing time. Also this study was carried out to investigate the effect of grain size distribution of 21 types of soils on the strength of soil-cement mixtures at four levels of cement content and three levels of curing time. The results are summarized as follows: 1. Optimum moisture content increased with increase of the cement content, but maximum dry density was changed ununiformly with cement content. Water content corresponding to the maximum strength was a little higher than the optimum moisture content along the increase of cement content. 2. In molding the specimens with the optimum moisture content, the maximum strength appeared at the wet side of the optimum moisture content. 3. According to increase of curing temperature as 30, 40, 50, and 60$^{\circ}C$, unconiiend compressive strength of soil-cement mixtures increased, the rate of increase at the early curing period was large, and approximately 120 hours was suifficient to harden soil-cement mixtures completely. 4. The strength of soil-cement mixtures at the curing temperature of 10$^{\circ}C$ decreased at the rate of 30 to 50 percent than at the curing temperature of 20$^{\circ}C$, and the strength of soil-cement mixtures at the curing temperature of 0$^{\circ}C$ increased a little with increase of curing time. 5. Although the strength of soil-cement mixtures seemed to be a little affected by the temperature difference between day time and night, it was recommended that reasonable working period was the duration from July to August of which average maximum temperature of Korea was approximately 30$^{\circ}C$. 6. Accelerated curing time corresponding to the normal curing time of 28-day was shorten with increase of curing temperature, also it was a little affected by the cement. Accelerated curing time that the strength of soil-cement mixtures for the cement of 9 percent and the curing temperature of 60was shorten with increase of curing temperature, also it was a little affected by the cement. Accelerated curing time that the strength of soil-cement mix- tures for the cement of 9 percent and the curing temperature of 60$^{\circ}C$ was 45 hours at the KY sample, 50 hours at the MH, 40 hours at the SS, and 34 hours at the JJ respectively. 7. Accelerated curing time was depended upon the grain size distribution of soil, it decreased with increase the percent passing of No. 200 sieve. 8. Relationship between the normal curing times and the accelerated curing times showed that there was a linear relationship between them, its slope decreased with increase of curing temperature. 9. The most reasonable soil of the soil-cement mixtures was the sandy loam which was a well graded soil. Assuming the base of road requiring 7-day strength of 21 kg/$\textrm{cm}^2$ being used, the soil-cement mixtures could be obtained with adding 6 percent of cement in such a sails S-7, S-8, S-9, S-10, S-11, S-12, S-13. 10. The regression equation between the 28-day and the 7-day strength was obtained as follow; q28=1.12q7,+6.5(r=0.96).

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적산온도에 의한 FRC 기층의 강도발현 성능 분석 (Performance Analysis of Strength Development of FRC Base Depending on Maturity)

  • 최성용;박영환;정우태
    • 한국도로학회논문집
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    • 제18권1호
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    • pp.13-21
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    • 2016
  • PURPOSES : In this study, we analyzed the compressive strength characteristics of lean base concrete in relation to changes in the outdoor temperature after analyzing the cold and hot weather temperature standards and calculated the minimum and maximum temperatures when pouring concrete. We examined the rate of strength development of lean base concrete in relation to the temperature change and derived an appropriate analysis formula for FRC base structures by assigning the accumulated strength data and existing maturity formula. METHODS : We measured the strength changes at three curing temperatures (5, 20, and $35^{\circ}C$) by curing the concrete in a temperature range that covered the lowest temperature of the cold period, $5^{\circ}C$, to the highest temperature of the hot period, $35^{\circ}C$. We assigned the general lean concrete and FRC as test variables. A strength test was planned to measure the strength after 3, 5, 7, 14, and 28 days. RESULTS : According to the results of compressive strength tests of plain concrete and FRC in relation to curing temperature, the plain concrete had a compressive strength greater than 5 MPa at all curing temperatures on day 5 and satisfied the lean concrete standard. In the case of FRC, because the initial strength was substantially reduced as a result of a 30% substitution of fly ash, it did not satisfy the strength standard of 5 MPa when it was cured at $5^{\circ}C$ on day 7. In addition, because the fly ash in the FRC caused a Pozzolanic reaction with the progress into late age, the amount of strength development increased. In the case of a curing temperature of $20^{\circ}C$, the FRC strength was about 66% on day 3 compared with the plain concrete, but it is increased to about 77% on day 28. In the case of a curing temperature of $35^{\circ}C$, the FRC strength development rate was about 63% on day 3 compared with the plain concrete, but it increased to about 88% on day 28. CONCLUSIONS : We derived a strength analysis formula using the maturity temperatures with all the strength data and presented the point in time when it reached the base concrete standard, which was 5 MPa for each air temperature. We believe that our findings could be utilized as a reference in the construction of base concrete for a site during a cold or hot weather period.

에폭시 레진의 경화방법에 따른 이방성 전도필름의 접합신뢰성 및 열적기계적 특성 변화 (A Study on the Thermo-mechanical Characteristics and Adhesion Reliability of Anisotropic Conductive Films Depend on the Curing Methods of Epoxy Resins)

  • 길만석;서경원;김재한;이종원;장은희;정도연;김수자;김정수
    • 폴리머
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    • 제34권3호
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    • pp.191-197
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    • 2010
  • 이방성 전도필름(ACF)의 경화방법을 개선하기 위하여 이미다졸계 경화제 대신에 저온에서도 경화가 빠른 열잠재성 양이온 개시제형 경화제를 사용한 에폭시 수지의 경화를 연구하였다. 경화특성의 분석을 위해 유리전이온도, 저장모듈러스, 열팽창계수를 포함한 열적기계적 특성을 조사하였으며 열사이클, 고온고습 신뢰성을 관찰하였다. 열잠재성 양이온 개시제형 경화제를 사용한 ACF가 이미다졸계 경화제를 사용한 경우보다 경화속도는 빨랐으며, 열팽창계수는 낮았고, $T_g$가 높아서 고온안정성도 우수하였다. 또 낮은 온도와 빠른 경화에도 불구하고 안정적인 접속 저항을 유지하여 높은 신뢰성을 나타내었다. 본 연구를 통하여 에폭시 경화방법은 ACF의 열적기계적 특성과 신뢰성에 큰 영향을 미치는 중요한 인자임을 확인하였다.

Modeling of Compressive Strength Development of High-Early-Strength-Concrete at Different Curing Temperatures

  • Lee, Chadon;Lee, Songhee;Nguyen, Ngocchien
    • International Journal of Concrete Structures and Materials
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    • 제10권2호
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    • pp.205-219
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    • 2016
  • High-early-strength-concrete (HESC) made of Type III cement reaches approximately 50-70 % of its design compressive strength in a day in ambient conditions. Experimental investigations were made in this study to observe the effects of temperature, curing time and concrete strength on the accelerated development of compressive strength in HESC. A total of 210 HESC cylinders of $100{\times}200mm$ were tested for different compressive strengths (30, 40 and 50 MPa) and different curing regimes (with maximum temperatures of 20, 30, 40, 50 and $60^{\circ}C$) at different equivalent ages (9, 12, 18, 24, 36, 100 and 168 h) From a series of regression analyses, a generalized rate-constant model was presented for the prediction of the compressive strength of HESC at an early age for its future application in precast prestressed units with savings in steam supply. The average and standard deviation of the ratios of the predictions to the test results were 0.97 and 0.22, respectively.

풍쇄슬래그 잔골재를 사용한 콘크리트의 공학적 특성에 관한 실험적 연구 (An Experimental Study on the Engineering Properties of Concrete using Fine Aggregate of PS ball Slag)

  • 이상수;송하영;김을용
    • 한국건축시공학회지
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    • 제6권3호
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    • pp.107-114
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    • 2006
  • In this study, the experiment was carried out to investigate and analyze the engineering properties of concrete using fine aggregate of PS bal slagl. The main experimental variables were water/cement ratio 30, 40, 50(%), water content $170kg/m^3$, replacement ratio of slag fine aggregate 0, 25, 50, 75(%) in experiment I and water/cement ratio 30, 40, 50(%), water content 165, 170, 175($kg/m^3$), replacement ratio of fine aggregate of PS ball 0, 50 in experiment II. According to the test results, the principle conclusions are summarized as follows (1) The workability of slag fine aggregate-mixed concrete tends to improve, as the replacement rate increases. (2) The air content of slag fine aggregate-mixed concrete tends to decrease, as the replacement rate increases. (3) The unit volume weight of slag fine aggregate-mixed concrete tends to significantly increase, as the replacement rate increases. (4) The compressive strength of slag fine aggregate-mixed concrete tends to show more increasing propensity, in case the curing period is relatively long, as the replacement rate increases.