• Title/Summary/Keyword: crude drug preparation drink

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Identification of Ginseng Saponin and Quantitative Determination of $Ginsenoside-Rb_1$ from Crude Drug Preparation Drink (생약복방제 드링크중 인삼 saponin의 확인 및 $Ginsenoside-Rb_1$의 분리 정량)

  • 최강주;고성룡
    • Journal of Ginseng Research
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    • v.14 no.2
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    • pp.112-116
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    • 1990
  • As a part of studies on the quality control of crude drug preparation drinks, ginseng saponins were identified by HPLC. Ginsenoside-Rb1 was determined quantitatively by HPLC. Ginsenoside MeOH/H2O(65:35:10, v/v) on Si-gel plate. Ginsenoside-Rb1 content determined by HPLC on Lichrosorbtract drinks was 57.5-70.4% compared to the content in the red ginseng extract.

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Identification of Cinnamon Components and Quantitative Determination of Cinnamlc Acid from Crude Drug Drink Preparations (생약복방 드링크제 중 계피성분의 확인 및 계피산의 분리정량)

  • 고성룡;김나미
    • Journal of Ginseng Research
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    • v.15 no.1
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    • pp.1-5
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    • 1991
  • For the quality control of crude drug drink preparations, methods for identification of cinnamon components and quantitative determination of cinnamic acid were established. Cinnamon components were identified by TLC with benzene/ethyl acetate (1:1, v/v) on silica gel plate by spraying p-anisaldehyde-sulfuric acid. Cinnamic acid contents were determined at UV 280 nm by HPLC on $\mu$-Bondapak Cls column with acetonitrile/water/acetic acid (40:60:2, v/v). Recoveries of cinnamic acid in three crude drug drink preparations were between 84.1-90.2% compared to the content of the cinnamon extract.

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Identification of Ginger Components and Quantitative Determination of 6-Gingerol from Crude Drugs-Drink Preparations (생약복방 드링크제 중 건강성분의 확인 및 6-Gingerol의 분리 정량)

  • 고성룡;최강주
    • Journal of Ginseng Research
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    • v.14 no.3
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    • pp.442-446
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    • 1990
  • As a part of studies on the quality control of crude drug-drink preparations, ginger components were identified by TLC and 6-gingerol was determined quantitatively by HPLC. Ginger components were identified by TLC with benzene/acetone (4:1, v/v, on silica gel plate by spraying a vanillinsulfuric acid reagent. 5-Gingerol contents were determined at 280 nm by HPLC on Lichro CART RP-18 column with acetonitrile/wate(38:62, v/v). Its transfer rate in the 3 types of crude drug extract drinks was 65.4-85.1% compared to the content in the ginger extract.

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