• Title/Summary/Keyword: crack density analysis

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The Properties of $\beta-SiC-TiB_2$ Electroconductive Ceramic Composites Densified by Liquid-Phase Sintering (액장 소결한 $\beta-SiC-TiB_2$계 전도성 복합체의 특성)

  • Yim, Seung-Hyuk;Shin, Yong-Deok;Song, Joon-Tae
    • The Transactions of the Korean Institute of Electrical Engineers C
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    • v.49 no.9
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    • pp.510-515
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    • 2000
  • The mechanical and electrical properties of the hot-pressed and annealed $\beta-SiC-TiB_2$ electroconductive ceramic composites were investigated as a function of the liquid forming additives of Al_2O_3+Y_2O_34. The result of phase analysis of composites by XRD revealed $\alpha-SIC(6H)\;TiB_2,\; and YAG(Al5Y3O12) crystal phase. The relative density and the mechanical properties of composites were increased with increasing $Al_2O_3+Y_2O_34 contents because YAG of reaction between $Al_2O_3\; and\; Y_2O_3$ was increased. The Flexural strength showed the highest value of 432.5MPa for composites added with 12wt% $Al_2O_3+Y_2O_34 additives at room temperature. Owing to crack deflection crack bridging phase transition and TAG of fracture toughness mechanism the fracture toughness showed 7.1MPa.m1/2 for composites added with 12wt% $Al_2O_3+Y_2O_34 additives at room temperature. The electrical resistivity and the resistance temperature coefficient showed the lowest of $6.0\times10-4\Omega.cm\; and\; 3.1\times10-3/^{\circ}C4 respectively for composite added with 12wt% \Omega additives at room temperature. The electrical resistivity of the composites was all positive temperature coefficient resistance (PTCR) in the temperature range of $25^{\circ}C\; to\; 700^{\circ}C$.

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Manufacturing and Evaluation of the Properties of Hybrid Bulk Material by Shock-compaction of Nanocrystalline Cu-Ni Mixed Powder (나노 구리-니켈 혼합분말의 충격압축법을 통한 복합벌크재의 제조 및 특성평가)

  • Kim, Wooyeol;Ahn, Dong-Hyun;Park, Lee Ju;Kim, Hyoung Seop
    • Journal of Powder Materials
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    • v.21 no.3
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    • pp.196-201
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    • 2014
  • In this study, nanocrystalline Cu-Ni bulk materials with various compositions were cold compacted by a shock compaction method using a single-stage gas gun system. Since the oxide layers on powder surface disturbs bonding between powder particles during the shock compaction process, each nanopowder was hydrogen-reduced to remove the oxide layers. X-ray peak analysis shows that hydrogen reduction successfully removed the oxide layers from the nano powders. For the shock compaction process, mixed powder samples with various compositions were prepared using a roller mixer. After the shock compaction process, the density of specimens increased up to 95% of the relative density. Longitudinal cross-sections of the shock compacted specimen demonstrates that a boundary between two powders are clearly distinguished and agglomerated powder particles remained in the compacted bulk. Internal crack tended to decrease with an increase in volumetric ratio of nano Cu powders in compacted bulk, showing that nano Cu powders has a higher coherency than nano Ni powders. On the other hand, hardness results are dominated by volume fraction of the nano Ni powder. The crystalline size of the shock compacted bulk materials was greatly reduced from the initial powder crystalline size since the shock wave severely deformed the powders.

Development of a novel fatigue damage model for Gaussian wide band stress responses using numerical approximation methods

  • Jun, Seock-Hee;Park, Jun-Bum
    • International Journal of Naval Architecture and Ocean Engineering
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    • v.12 no.1
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    • pp.755-767
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    • 2020
  • A significant development has been made on a new fatigue damage model applicable to Gaussian wide band stress response spectra using numerical approximation methods such as data processing, time simulation, and regression analysis. So far, most of the alternative approximate models provide slightly underestimated or overestimated damage results compared with the rain-flow counting distribution. A more reliable approximate model that can minimize the damage differences between exact and approximate solutions is required for the practical design of ships and offshore structures. The present paper provides a detailed description of the development process of a new fatigue damage model. Based on the principle of the Gaussian wide band model, this study aims to develop the best approximate fatigue damage model. To obtain highly accurate damage distributions, this study deals with some prominent research findings, i.e., the moment of rain-flow range distribution MRR(n), the special bandwidth parameter μk, the empirical closed form model consisting of four probability density functions, and the correction factor QC. Sequential prerequisite data processes, such as creation of various stress spectra, extraction of stress time history, and the rain-flow counting stress process, are conducted so that these research findings provide much better results. Through comparison studies, the proposed model shows more reliable and accurate damage distributions, very close to those of the rain-flow counting solution. Several significant achievements and findings obtained from this study are suggested. Further work is needed to apply the new developed model to crack growth prediction under a random stress process in view of the engineering critical assessment of offshore structures. The present developed formulation and procedure also need to be extended to non-Gaussian wide band processes.

Evaluation of Analysis Code of Corrugated Steel Plate Lining in Cut-and-Cover Tunnel (개착식 터널에서 파형강판 라이닝의 해석 기법 평가)

  • Kim, Jung-Ho;Kim, Nak-Young;Lee, Yong-Jun;Lee, Seung-Ho;Hwang, Young-Chul;Cho, Chul-Shin;Chung, Hyung-Sik
    • Proceedings of the Korean Geotechical Society Conference
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    • 2005.03a
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    • pp.1316-1323
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    • 2005
  • Most tunnel lining material which has been used in the domestic is a concrete. But many problems as the construction period, the cost, and the crack occurrence for the design, construction, and management were happened in the concrete lining. For this reason, many research institutes like the Korea Highway Corporation recognize the necessity of an alternate material development and grow on the interest for that. So in this study, the behaviour characteristics for the application of the Corrugated Steel Plate Lining in cut-and-cover tunnel are evaluated as several conditions for the backfill height, the cutting slope, and the relative density of backfill soil are changed. In addition, through using that conditions, CHBDC(2000, Canadian Highway Bridge Design Code) is evaluated if it could be applied to the design by comparing with the numerical analysis results. As the behaviour characteristics of the Corrugated Steel Plate Lining by CHBDC and the static numerical analysis are analyzed, both the methods show the same linear increases of the compressive stress according to the increase of the backfill height. The CHBDC of the dead load condition has very similar tendency by comparing with the result of the static numerical analysis.

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Phase Transformation and Mechanical Properties on Sintering Temperature of $\alpha$-SiC Manufactured by Pressureless Sintering (상압소결법에 의해 제조한 $\alpha$-SiC의 소결온도에 따른 상전이와 기계적 특성)

  • 주진영;신용덕;박미림;이종덕
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2001.07a
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    • pp.431-434
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    • 2001
  • The mechanical and phase transformation of the cold isostatically pressed $\alpha$-SiC ceramic were investigated as a function of the sintering temperature. The result of phase analysis by XRD revealed 6H, 4H, 3C and phase transformation between 6H and 4H showed a sudden change over 200$0^{\circ}C$. However, the alongrightarrow$\beta$ reverse transformation did not occur to any sintering temperature. The relative density and the mechanical properties of $\alpha$-SiC ceramic was increased with increased sintering temperature. The flexural strength rapidly inclosed below 210$0^{\circ}C$ and showed the highest value of 410 MPa at 220$0^{\circ}C$. This reason is because crack was propagated through surface flaw. The fracture toughness showed the highest value of 3.3 MPa.m$_{1}$2/ at 220$0^{\circ}C$.

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Optimization of PMD(Pre-Metal Dielectric) Linear Nitride Process (PMD(Pre-Metal Dielectric) 선형 질화막 공정의 최적화)

  • Jeong, So-Young;Seo, Yong-Jin;Seo, Sang-Yong;Lee, Woo-Sun;Lee, Chul-In;Chang, Eui-Goo
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2001.05b
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    • pp.38-41
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    • 2001
  • In this work, we have been studied the characteristics of each nitride film for the optimization of PMD(pre-metal dielectric) liner nitride process, which can applicable in the recent semiconductor manufacturing process. The deposition conditions of nitride film were splited by PO (protect overcoat) nitride, baseline, low hydrogen, high stress and low hydrogen, respectively. And also we tried to catch hold of correlation between BPSG(boro-phospho silicate glass) deposition and densification. Especially, we used FTIR area method for the analysis of density change of Si-H bonding and Si-NH-Si bonding, which decides the characteristics of nitride film. To judge whether the deposited films were safe or not, we investigated the crack generation of wafer edge after BPSG densification, and the changes of nitride film stress as a function of RF power variation.

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Dielectric and Structural of BST Thin Films with Cr doped prepared by Sol-gel method for Tunable application (Tunable 소자 응용을 위한 Sol-gel 법으로 제작된 BST 박막의 Cr 첨가에 따른 구조적, 유전적 특성)

  • Kim, Seung-Bum;Kim, Kyoung-Tae;Kim, Chang-Il
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2004.07b
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    • pp.623-626
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    • 2004
  • [ $Ba_{0.6}Sr_{0.4}TiO_3$ ] (BST) dielectric thin films doped by Cr were prepared using an alkoxide-based sol-gel method on the Pt/Ti/SiO2/Si substrate. Atomic force microscopy and x-ray diffraction analysis showed that increasing the Cr doping ratio causes increased grain size while the surface remains smooth and crack-free. It was also found that compared with undoped films the increase of Cr content in BST improves the dielectric constant and the leakage-current characteristics. The figure of merit reached the maximum value of 72.3 at the 5 mol % of Cr doping. This composition showed the dielectric constant of 426, the loss factor of 0.0065, tenability of 47.7%, and leakage-current density (at the electric field of 100 kV/cm) of $5.31{\times}10^{-8}A/cm^2$. The results show that the Cr-doped BST thin films are prospective candidates for applications in tunable devices.

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Preparatio and properties of the paraelectric PLT thin film for the cpapcitor dielectrics of ULSI DRAM (ULSI DRAM의 캐패시터 절연막을 위한 Paraelectric PLT 박막의 제작과 특성)

  • 강성준;윤영섭
    • Journal of the Korean Institute of Telematics and Electronics A
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    • v.32A no.8
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    • pp.78-85
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    • 1995
  • We fabricated the Pb$_{1-0.28{\alpha}}La_{0.28}TiO_{3}$ (PLT(28)) thin film successfully by using the sol-gel method and characterized it to evaluate its potential for being utilized as the capacitor dielectrics of ULSI DRAMs. In our sol-gel process, the acetates were used as the starting materials. Through the TGA-DTA analysis, we established the excellent fabrication conditions of the sol-gel method for the PLT(28) thin film. We obtained the dense and crack-free PLT(28) thin film of 100% perovskite phase by drying at 350$^{\circ}C$ after each coating and final annealing at 650$^{\circ}C$. Its electrical properties were measured from the planar capacitors fabricated on the Pt/Ti/SiO$_{2}$/Si substrate. By the P-E hysteresis measurement, its paraelectric phase was identified and its dielectric constant and leakage current density were measured as 936 and 1.1${\mu}A/cm^{2}$, respectively. Those electrical values indicate that the PLT(28) thin film is the most successful candidate for the capacitor dielectrics of ULSI DRAMs at the present.

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Failure analysis of damaged tungsten monoblock components of upper divertor outer target in EAST fusion device

  • Kang Wang;Ya Xi;Xiang Zan;Dahuan Zhu;Laima Luo;Rui Ding;Yucheng Wu
    • Nuclear Engineering and Technology
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    • v.56 no.6
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    • pp.2307-2316
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    • 2024
  • A melting failure of W monoblock components of the upper divertor outer target in EAST occurred during the plasma campaigns in 2019. The failure characters and microstructure evolution of the failed W monoblock have been well investigated on one string (W436 string). Near the strike point region where heat flux density is highest, macroscopic cracks and severe surface damage such as dimensional change, melting and solidification are visible in several W monoblocks. At the same time, debonding, melting and migration of Cu/CuCrZr cooling tube components introduced fatal damage to the structure and function. The heat-induced microstructure evolution in the rest part has been examined via hardness tests and metallography. From the heat flux surface to the cooling tube, hardness increased gradually and the recrystallized grains could be found in the region with the highest temperature, while recrystallization grains also appear in some W monoblocks near the cooling tube area. The detailed microstructure has been investigated by metallography and EBSD. Such cases in EAST provide experiences on the extreme condition of accidental loss of coolant or higher discharge power in future devices.

A study on the analysis of the failure probability based on the concept of loss probability (결손확률모델에 의한 파손확률 해석에 관한 연구)

  • 신효철
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.15 no.6
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    • pp.2037-2047
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    • 1991
  • Strength is not simply a single given value but rather is a statistical one with certain distribution functions. This is because it is affected by many unknown factors such as size, shape, stress distribution, and combined stresses. In this study, a model of loss probability is proposed in view of the fact that one of the fundamental configuration of nature is hexagonal, for example, the shapes of lattice unit, grain, and so on. The model sues the concept of loss of certain element in place of Jayatilaka-Trustrum's length and angle of cracks. Using this model, the loss probability due to each loss of certain elements is obtained. Then, the maximum principal stress is calculated by the finite element method at the centroid of the elements under the tensile load for the 4,095 models of analysis. Finally, the failure probability of the brittle materials is obtained by multiplying the loss probability by the ratio of the maximum principal stress to theoretical tensile strength. Comparison of the result of the Jayatilaka-Trustrum's model and the proposed model shows that the failure probabilities by the two methods are in good agreement. Further, it is shown that the parametric relationship of semi-crack lengths for various degrees of birittleness can be determined. Therefore, the analysis of the failure probability suing the proposed model is shown to be promising as a new method for the study of the failure probability of birttle materials.