• 대한화학회지
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• 제20권5호
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• pp.417-423
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• 1976

PE, PP 및 PVC를 corona 放電으로 處理한 後 알루미늄과 接着을 시키면 接着强度가 크게 向上된다. 그러나 corona 放電으로 처리한 PE와 PP를 $80^{\circ}C$로 調節한 乾燥器에 넣고, PVC는 $50^{\circ}C$로 調節한 乾燥器에 넣어 15分間 放置하면 corona 放電處理만 했을 때 보다 接着力이 ${\frac{1}{2}}$밖에 되지 않는다. 따라서 高分子物質을 corona 放電處理 했을 때 接着强度의 增加는 高分子物質의 酸化에 依한 것이라고만은 볼 수 없다. 接着强度의 심한 振幅은 Weibull 分布函數를 이용하여 檢討하였다. 이 硏究에서는 corona 放電으로 처리한 高分子物質을 알루미늄과 接着시켰을 때 그 强度의 增加는 高分子物質의 表面에 執着된 electret의 影響이 크다는 것을 나타내었다.

• 비파괴검사학회지
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• 제14권2호
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• pp.112-121
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• 1994

초음파 C-scan 기법에 의해 스폿(spot)용접의 품질 평가를 위한 비파괴진단 평가에 관한 기초적인 실험적 검토를 하였다. 먼저, 스폿용접부 초음파탐상에 앞서 뉴우톤링의 모델링 실험을 통해 미소 간극을 갖는 접합계면에서의 초음파 반사 거동의 해석 결과를 근거로 스폿용접부의 너겟 형상과 크기, void 결함등의 정량적 평가와 corona bond의 정확한 식별에 최적한 초음파시험방법 및 조건의 설정을 시도하였다. 초음파시험 후 용접시험편을 절단하고, 그 절단면을 초음파현미경(SAM)과 광학현미경의 단면 관찰을 통해 스폿용접 품질 평가를 위한 초음파 비파괴평가법의 유용 가능성 유무, 적용 한계 등을 검토하였다. 그 결과 본 실험에 사용한 집속 초음파탐촉자(25MHz)에 의한 너겟 내부에 존재하는 void 크기의 검출한계는 $10{\mu}m$였으며 너겟 크기는 초음파시험의 경우가 최대 1mm정도 크게 측정되어 corona bond의 정확한 식별과 너겟 직경의 정량적 평가에 접근하기 위해서는 초음파 C-scan 데이터의 각종 화상 처리 기술의 적용에 의한 corona bond부의 명확한 식별 방법에 대한 연구 검토가 요망됨을 알 수 있었다.

• 대한화학회지
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• 제55권5호
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• pp.741-745
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• 2011

Well-resolved vibronic emission spectra were recorded in the visible region from the corona discharge of precursor alkylbenzenes in a technique of corona excited supersonic expansion using a pinhole-type glass nozzle. From the observed spectra, we found the evidence of the presence of benzyl-type radicals generated by dissociation of C-C or C-H bonds of alkyl group. After identification of benzyl-type radicals formed in the corona discharge, we suggest that energy densities in alkyl chain play a crucial role in determining the bond dissociation during corona excitation.

• Journal of Welding and Joining
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• 제12권3호
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• pp.109-117
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• 1994

Spot welding has wide used with a high work efficiency in the automotive and aerospace industries. Up to the present, the technique mainly used to test spot welds on production lines has been entirely depended upon destructive chisel or peel testing. Therefore, it's being very important assignment to secure the NDE technique which can be evaluate spot weld quality with more efficiency and high reliability. This paper discusses the feasibility of UNDE techniques to evaluate spot weld quality. For the sake of the approach to the quantitative measurement of nugget diameter and the discrimination of a the corona bond from nugget, ultrasonic c-scan image and distribution of reflective echo amplitude was measured by immersion method with the mechanical and the electronic scanning of point-focussed ultrasonic beam(25 MHz). As the results of this study, corona bond which is the most dangerous types of interface defects can be successfully detected, as well as expulsion and voids. Ultrasonic testing results were confirmed and compared by optical microscope and SAM(Scanning Acoustic Microscope) observation of the spot-weld cross section. The results show that the nugget diameter can be successfully measured with the accuracy of 0.8 mm.

• 한국공작기계학회:학술대회논문집
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• 한국공작기계학회 2003년도 추계학술대회
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• pp.301-306
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• 2003

Spot welding is frequently used for industrial purpose, such as automobile and aerospace industries and household appliances due to its high performance. In these day, robotization and systemization of welding process made it possible to produce more precise or smaller electric parts. And when it comes to welding of steel sheet, the size of nugget must be getting smaller. Therefore, welding conditions are limited to avoid defects, such as deformation, damage, weakening of joining area. In this research, the measurement of the nugget size by the nondestructive inspection has been conducted. As a result, the right estimation of the nugget size and void defects, the detection of corona bond near joining area, the selection of the optimum ultrasonic mode, and set up for ultrasonic inspection are studied. From the trustworthy solutions of nugget size estimated by results of measurement, the optimum inspection conditions depending upon the width of welding parts are determined as well.

• 한국공작기계학회:학술대회논문집
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• 한국공작기계학회 2004년도 추계학술대회 논문집
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• pp.49-53
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• 2004

Thin spot welding is frequently used for industrial purpose, such as automobile and aerospace industries and household appliances due to its high performance. In these days, the systemization of welding process made it possible to produce more precise or smaller electric parts. And when it comes to welding of steel sheets, the size of nugget must be getting smaller. Therefore, welding conditions are limited to avoid defects, such as deformation, damage and weakening of joining area. In this research, thin spot welding establishes the welding conditions, and then the measurement of the nugget size by the nondestructive inspection has been conducted. As a result, the right estimation of the nugget size, the detection of corona bond near joining area, the selection of the optimum ultrasonic mode, and setup for ultrasonic inspection are studied. From the trustworthy solutions of the nugget size estimated by results of measurement, the optimum inspection conditions depending upon the width of welding parts are determined as well.

• Restorative Dentistry and Endodontics
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• 제47권3호
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• pp.28.1-28.12
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• 2022

Objectives: Metalloproteinase-inhibiting agents, such as chitosan, can prevent collagen degradation in demineralized dental substrates, thereby improving the adhesive interface. This study evaluated the bond strength (BS) and chemical and morphological characterization of the adhesive interface after applying chitosan solution to demineralized dentin. Materials and Methods: The 80 third molars were selected. Forty teeth underwent caries induction using the pH cycling method. The teeth were divided according to the treatment: distilled water (control) and 2.5% chitosan solution. The surfaces were restored using adhesive and composite resins. Half of the specimens in each group were aged, and the other half underwent immediate analyses. The teeth were sectioned and underwent the microtensile bond strength test (µTBS), and chemical and morphological analyses using energy-dispersive spectroscopy and scanning electron microscopy, respectively. Data analysis was performed using 3-way analysis of variance. Results: For µTBS, sound dentin was superior to demineralized dentin (p < 0.001), chitosan-treated specimens had higher bond strength than the untreated ones (p < 0.001), and those that underwent immediate analysis had higher values than the aged specimens (p = 0.019). No significant differences were observed in the chemical or morphological compositions. Conclusions: Chitosan treatment improved bond strength both immediately and after aging, even in demineralized dentin.

• Journal of Welding and Joining
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• 제35권1호
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• pp.34-42
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• 2017

This paper presents a comparative study of the AC and MFDC resistance spot welding process with consideration of sheet thickness. The previous studies have confirmed that there is difference in the optimum welding current and expulsion current with AC and MFDC. The aim of this study was revealing the effect of sheet thickness on weldable current range and expulsion behavior for AC and MFDC welding processes. The optimum welding current of AC was lower (1.6 kA) than MFDC welding process in 0.8 mm sheet thickness. Early nugget growth being caused by the peak current of AC developed weld interface deformation, which resulted in suppressing the growth of corona bond and occurrence of low current expulsion. The resistance spot welding for thicker sheet (1.4 mm) required lower current of 0.6 kA for the expulsion on the MFDC welding process. The growth of contact diameter (size of corona bond) and button diameter was linear up to the expulsion current with MFDC welding process. Therefore, more attention is required when the AC and MFDC resistance spot welding process is applied for different thickness of steel sheet combination for automotive application.

• 한국기계가공학회지
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• 제21권3호
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• pp.1-11
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• 2022

In this study, an electric resistance dual-spot welding process using a copper electrode inserted in a heating electrode is suggested for the spot welding of AZ31 magnesium sheets. This spot-welding process involves two heating methods for welding at the interfacial zone between the magnesium sheets, one of which is the heating method by thermal conduction from the heating electrode heated by the welding current induced to the steel electrode, and the other heating method uses the electric resistance between the contacted surfaces of the two sheets by the welding current induced to the copper electrode. This welding process includes the welding variables, such as the current induced in the heating electrode and the copper electrode, and the outer diameters of the heating electrode. This is because the heat conducted from the heating electrode can be maintained at a higher temperature in the welding zone, which has a slow cooling effect on the nugget of the melted metal after the welding step. The pressure exerted during the pressing of the magnesium sheets by the heating electrode can be increased around the nugget zone at the spot-welding zone. Thus, it not only reduces the warping effect of the elastoplastic deformation of sheets, but also the corona bond can make it less prone to cracking at the welded zone, thereby reducing the number of nuggets expelled out of the corona bond. In conclusion, it was known that an electric resistance dual spot welding process using the copper electrode inserted in the heating electrode can improve the welding properties in the electric resistance spot welding process of AZ31 magnesium sheets.

• 한국구조물진단유지관리공학회 논문집
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• 제18권3호
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• pp.153-159
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• 2014

본 연구에서는 고경질 도막재로 PET 필름을 접합하는 시공방법에 있어서 PET 필름의 표면처리 조건 및 겹침이음 길이에 따른 접합특성 및 내구특성을 검토하였는데, 그 결과 무처리 보다 코로나 방전 처리에 의해 접촉각, 접합 인장강도, 벗김저항성이 개선되었다. 특히 시험체 E (코로나 방전+프라이머+강접접착제+폴리에스터 부직포)에서 가장 높은 것으로 나타났으며, 특히 겹침 이음길이 15mm 이상일 때 16주간 장기간 열화처리에도 안정적인 접합성능을 확보하는 것으로 나타나 방수재료로서 수밀성을 확보할 것으로 판단된다.