• Title/Summary/Keyword: controlled porosity

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On the Fabrication of Porous 316L Stainless Steel by Spark Plasma Sintering (방전플라즈마 소결에 의한 316L 스텐레스강 다공체 재료 제조에 관한 연구)

  • 권영순;김성기;김현식;김환태;최성일;석명진
    • Journal of Powder Materials
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    • v.9 no.1
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    • pp.50-60
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    • 2002
  • SPS(Spark Plasma Sintering ) is known to be an excellent sintering method for porous materials. In the present work an attempt has been made of fabricating porous 316L Stainless steel with good mechanical properties by using controlled SPS process Porosity was 21%~53% at sintering temperature of $600^{\circ}C$~100$0^{\circ}C$ The limit of porosity with available mechanical strength was 30% at given experimental conditions. Porosity can be controlled by manipulating the intial height of the compact by means of the supporter and punch length. The applied pressure can be exerted entirely upon the supporter, giving no influence on the specimen. The specimen is then able to be sintered pressurelessly. In this case porosity could be controlled from 38 to 45% with good mechanical strength at sintering temperature of 90$0^{\circ}C$. As the holding time increased, neck between the particles grew progressively, but shrinkage of the specimen did not occur, implying that the porosity remained constant during the whole sintering process.

Preparation of porous hydroxyapatite ceramics (Hydroxyapatite 다공체의 제조)

  • Song, J.T.;Ryou, D.W.;Choi, S.H.
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.4 no.3
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    • pp.284-293
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    • 1994
  • The various methods of preparation for the porous hydroxyapatite ceramics using naphthalene, $H_20_2$ and chlorinated paraffine with $H_20_2$ were investigated. And then the prepared orous hydroxyapatite ceramics were characterized by XRD, SEM, FT-IR and the apparent porosity. The pore size of porous hydroxyapatite ceramics was controlled by the content and size of naphthalene granular. It was found that the porosity of it was increased with the amount of naphthalene, but the bending strength was decreased. The application of hydrogen peroxide produced porous materials like a sponge tissue, but the porosity and the shape of sintered body were hardly controlled. In the case of using chlorinated paraffine with the simultaneous addition of hydrogen peroxide, the sponge tissue was obtained and also could be controlled from 50 up to about 65% porosity of it.

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Fermentation Characteristics of Kochujang in Onggis with Different Porosities (통기성이 다른 옹기에서의 고추장 발효 특성)

  • Chung, Sun-Kyung;Lee, Kwang-Soo;An, Duck-Soon
    • KOREAN JOURNAL OF PACKAGING SCIENCE & TECHNOLOGY
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    • v.14 no.1
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    • pp.9-14
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    • 2008
  • The effect of different porosity of onggis, Korean earthenware, on the fermentation of kochujang was investigated. The porosity was controlled with glazing treatment. Three kinds of onggis were made: one with no glazing treatment, one with outside glazing treatment, and one with both inside and outside glazing treatment. During 4 month fermentation of kochujang in porosity-controlled earthenwares, physical, chemical, microbiological, and sensory quality attributes were monitored. Higher protease activity and higher contents of amino nitrogen, free amino acids, and total neucleotide were observed in kochujang fermented in the onggi with outside glazing treatment, which might have resulted in better sensory quality. Onggi with medium porosity could be effective for fermentation of kochujang.

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Fermentation of Kanjang, Korean Soy Sauce, in Porosity-Controlled Earthenwares with Changing the Mixing Ratio of Raw Soils (흙배합비를 달리하여 기공율이 조절된 담금용기 항아리에서의 간장 발효)

  • Chung, Sun-Kyung;Lee, Kwang-Soo;Lee, Dong-Sun
    • Korean Journal of Food Science and Technology
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    • v.38 no.2
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    • pp.215-221
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    • 2006
  • This study focuses on investigating the effect of porosity-controlled earthenware on fermentation of kanjang, Korean soy sauce. Porosity of fermentation vessel was controlled by changing the mixing ratio of raw soils at manufacturing earthenware. Earthenwares contented 0%, 40% and 60% of the mixture of red brown soil and powdered soil (1 : 1), respectively. The more contents of the mixed soil, the more porosity in earthenware. During fermentation of kanjang in porosity-controlled earthenwares at $30^{\circ}C$ for 4 months, physical, chemical, microbiological and sensory quality attributes were monitored. Compared to other containers, kanjang in the earthenware that had 0% mixed soil showed less water loss, salt content and pH. It also produced higher total acidity, protease activity, total nucleotide, and microbiological changes which included total aerobic bacteria, lactic acid bacteria and yeast. Total nitrogen and free amino acids in kanjang did not show the consistency with the mixed soil contents of fermentation containers, which may take more effect of other factors as water loss than the porosity of vessels. However, the percentage of glutamic acid in total free amino acids was a little higher in the earthenware that had 0% of mixed soil than other containers. These positive physicochemical, microbiological changes also resulted in higher sensory quality.

Investigation of Relationship between Etch Current and Morphology and Porosity of Porous Silicon

  • Jang, Seunghyun
    • Journal of Integrative Natural Science
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    • v.3 no.4
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    • pp.210-214
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    • 2010
  • Relationship between etch current and morphology and porosity of porous silicon (PS) has been investigated. The gravimetric method is applied to measured the porosity of PS. As the current density increase, the silicon dissolution rate increases, resulting in a higher porosity and etching rate. The result shows that linear dependence of PS porosity and etching rate as a function of current density. The morphology of porous silicon was investigated by using cold field emission scanning electron micrograph (FE-SEM). The size of pores formed during anodization is predominantly controlled by the current density, with an increase in the pore size corresponding to an increase in the current density.

Characterization of Pore Structures for Porous Sintered Reaction-Bonded Silicon Nitrides with Varied Pore-Former Content

  • Park, Young-Jo;Song, In-Hyuck;Kim, Hai-Doo
    • Journal of the Korean Ceramic Society
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    • v.45 no.11
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    • pp.675-680
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    • 2008
  • The effect of pore former content on both porosity and pore structure was investigated for porous sintered reaction-bonded silicon nitrides (SRBSNs). A spherical PMMA with $d_{50}=8{\mu}m$ was employed as a pore-former. Its amount ranged from 0 to 30 part. Porous SRBSNs were fabricated by post-sintering at various temperatures where the porosity was controlled at $12{\sim}52%$. The strong tendency of increasing porosity with PMMA content and decreasing porosity with sintering temperature was observed. Measured pore-channel diameter increased $(0.3{\rightarrow}1.1{\mu}m)$ with both PMMA content and sintering temperature.

Effect of Clay-Mineral Composition on Flexural Strength of Clay-based Membranes (점토 광물 조성이 점토기반 분리막의 곡강도에 미치는 영향)

  • Lee, Young-Il;Eom, Jung-Hye;Kim, Young-Wook;Song, In-Hyuck
    • Journal of the Korean Ceramic Society
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    • v.51 no.5
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    • pp.380-385
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    • 2014
  • Clay-based membranes with submicron pore size were successfully prepared by a simple pressing process using low-cost starting materials(e.g., kaolin (K), bentonite (B), talc (T), and sodium borate). The green bodies were sintered at $1000^{\circ}C$ for 2 h in air. The effect of clay-mineral composition on the flexural strength of clay-based membranes was investigated. The porosity of the clay-based membranes could be controlled within the range of 34 - 42% by adjusting the starting composition. The flexural strength of the low-cost membranes depended on both the porosity and the ${\alpha}$-quartz content. In turn, the porosity and ${\alpha}$-quartz content were affected by the (B+T) /(K+B+T) ratio. The plot of strength relative to this ratio, showed a maximum when the ratio was 0.4. The typical flexural strength of these clay-based membranes (with ratio 0.4) was 28 MPa at 34% porosity.

Porous Alumina/Mullite Layered Composites with Unidirectional Pore Channels and Improved Compressive Strength (일축배향 기공채널과 향상된 압축강도를 갖는 다공질 알루미나/뮬라이트 층상 복합체)

  • Kim, Kyu Heon;Kim, Tae Rim;Kim, Dong Hyun;Yoon, Seog Young;Park, Hong Chae
    • Journal of the Korean Ceramic Society
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    • v.51 no.1
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    • pp.19-24
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    • 2014
  • Three-layer porous alumina-mullite composites with a symmetric gradient porosity are prepared using a controlled freeze/gel-casting method. In this work, tertiary-butyl alcohol (TBA) and coal fly ash with an appropriate addition of $Al_2O_3$ were used as the freezing vehicle and the starting material, respectively. When sintered at $1300-1500^{\circ}C$, unidirectional macro-pore channels aligned regularly along the growth direction of solid TBA were developed. Simultaneously, the pore channels were surrounded by less porous structured walls. A high degree of solid loading resulted in low porosity and a small pore size, leading to higher compressive strength. The sintered porous layered composite exhibited improved compressive strength with a slight decrease in its porosity. After sintering at $1500^{\circ}C$, the layered composite consisting of outer layers with a 50 wt% solid loading showed the highest compressive strength ($90.8{\pm}3.7MPa$) with porosity of approximately 26.4%.