• Title/Summary/Keyword: continuous deposition

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Measurement of Wax Appearance Temperature Using Image Processing (영상 처리기법을 이용한 오일의 왁스생성온도 측정)

  • Hwang, Soon-Hye;Kang, Pan-Sang;Lim, Jong-Se
    • Journal of Energy Engineering
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    • v.25 no.1
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    • pp.1-8
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    • 2016
  • When the oil is produced in the low temperature environment, wax can be accumulated in petroleum production system(pipeline, riser) and causes problems such as pipeline stucking, disturbance of the oil production. These problems can be lead to time-consuming and economic losses for flow assurance. For prediction and mitigation of wax deposition, it is necessary to measure the Wax Appearance Temperature(WAT) which is a temperature when the wax crystals start to be formed. WAT standard measurement method of transparent oil has to determine the cloud point of sample to the naked eye and cannot be applied to continuous change of the temperature. In this study, wax behavior of transparent oil samples are recorded depending on temperature using Visualized WAT Measurement System. Also, WATs of transparent oil samples are measured by image processing and compared with the result of the standard method.

Deposition of Nanocrystals using Phase Separation on Flexible Substrates (유연기판위에 상분리를 이용한 반도체 나노입자 증착)

  • Oh, Seung-Kyun;Chung, Kook-Chae;Kim, Young-Kuk;Choi, Chul-Jin
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2009.06a
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    • pp.284-284
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    • 2009
  • We have fabricated semiconductor nanocrystals using phase separation on flexible substrates for future application in QD-LEDs. The phase separation between the CdSe semiconductor nanocrystals and TPD organic underlayer can occur during the solvent drying, and the CdSe may rise towards the surface of the coated films, which is arranged into close packed array called self-assembly process. In this work, the polyethylene naphthalate (PEN) films of $200{\mu}m$ thickness was used as a flexible substrate, which was coated with indium tin oxide(ITO) as a transparent electrode of <$15{\Omega}/cm^2$. A number of solvents such as chloroform, toluene, and hexane was used and their coating properties were investigated using the spin coating process. The dispersion of both QD and TPD was rather poor in toluene and hexane and resulted in rougher surface and some aggregates. Meanwhile, the surface roughness of templates can be a very critical issue in the fabrication of QD-LED devices. Some experiments was performed to reduce the ~4nm surface roughness of the PEN films and It can be decreased to the minimum of ~0.7nm. Also discussed are the optical properties of semiconductor nanocrystals used in this phase separation and possible large area and continuous coating process for future application.

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Electro-deposition and Crystallization Behaviors of Cr-C and Cr-C-P Alloy Deposits Prepared by Trivalent Chromium Sulfate Bath (황화물계 3가 크롬도금욕에서 크롬-탄소 및 크롬-탄소-인 합금도금의 전착과 결정화거동)

  • Kim, Man;Kim, Dae-Young;Park, Sang-Eon;Kwon, Sik-Chul;Choi, Yong
    • Journal of the Korean institute of surface engineering
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    • v.37 no.2
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    • pp.80-85
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    • 2004
  • Chromium-carbon (Cr-C) and chromium-carbon-phosphorus (Cr-C-P) alloy deposits using trivalent chromium sulfate baths containing potassium formate were prepared to study their current efficiency, hardness change and phase transformations behavior with heat treatment, respectively. The current efficiencies of Cr-C and Cr-C-P alloy deposits increase with increasing current density in the range of 15-35 A/dm$^2$. Carbon content of Cr-C and phosphorous of Cr-C-P layers decreases with increasing current density, whereas, the carbon content of Cr-C-P layer is almost constant with the current density. Cr-C deposit shows crystallization at $400^{\circ}C$ and has (Cr+Cr$_{ 23}$$C_{6}$) phases at $800^{\circ}C$. Cr-C-P deposit shows crystallization at $600^{\circ}C$ and has (Cr+Cr$_{23}$ $C_{6}$$+Cr_3$P) phases at $800^{\circ}C$. The hardness of Cr-C and Cr-C-P deposits after heating treatment for one hour increase up to Hv 1640 and Hv 1540 and decrease about Hv 820 and Hv 1270 with increasing annealing temperature in the range of $400~^{\circ}C$, respectively. The hardness change with annealing is due to the order of occurring of chromium crystallization, precipitation hardening effect, softening and grain growth with temperature. Less decrease of hardness of Cr-C-P deposit after annealing above $700^{\circ}C$ is related to continuous precipitation of $Cr_{23}$ $C_{6}$ and $Cr_3$P phases which retard grain growth at the temperature.

THE HEALING EFFECTS OF LOW POWER DENSITY LASER TO THE EXPERIMENTAL PERIODONTITIS;HISTOPATHOLOGIC STUDY (저출력 레이저 조사가 성견의 실험적 치주질환 치유에 미치는 영향에 관한 조직병리학적 연구)

  • Kim, Dong-Woon;Lee, Jae-Hyun;Chung, Chin-Hyung
    • Journal of Periodontal and Implant Science
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    • v.23 no.1
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    • pp.16-26
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    • 1993
  • In order to investigate the healing effect on inflammation and bone regeneration of low power density laser radiation in dogs, experimental periodontitis was made in dog mandibular 3rd, 4th premolars. All teeth were classified with four groups of two experimental group and control groups. The second group were irradiated on periodontitis site and the first group were control. The fourth group were irradiated on periodontitis site flap operation and the third group were flap control. Experimental groups were irradiated with GaAs low power density laser of pulse wave and continuous wave of 904nm every day by five days respectively and then control group and experimental groups were evaluated by histo-pathological study. The results were as follows : 1. Experimental periodontits site of dog were irradiated with GaAs low power laser results in reducing of pseudoepitheliomatous proliferation and inflammation at light microscope. 2. After irradiation with low power density laser, experimental groups were revealed that PDL forming activity were increased and newly formed collagen deposition were observed. 3. Low power density lsaer irradiation on experimental periodontits site after flap operation showed that decreasing of inflammation, reducing of osteoclast activity. Capillary proliferation, reduction of pseudoepitheliomatous proliferation. 4. After irradiation with low power density laser on flap experimental site, experimental groups were revealed that newly formed collagen in periodontal ligament and alveolar bone were detected on MT staining.

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Delta Development in the Nakdong River Estuary: a Literature Survey (낙동강 하구역 삼각주 발달에 관한 문헌 고찰 연구)

  • Yoon, Han-Sam;Yoo, Chang-Ill;Kang, Yoon-Koo;Ryu, Cheong-Ro
    • Journal of Ocean Engineering and Technology
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    • v.21 no.2 s.75
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    • pp.22-34
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    • 2007
  • We present basic data for developing new research topics and closely examine the existing data on the development and organization of the Nakdong River Estuary Delta by analyzing various studies of the area, including ocean engineering, coastal engineering, ocean environmental engineering, geomorphological, and geological studies. We first defined the general concepts related to the estuary and delta and reviewed the historical development of the Nakdong River Estuary Delta over the past 100 years. We then examined the origin and core elements of the estuary deposits that constitute the delta. In addition, we scrutinized the main factors affecting the development of the delta and analyzed existing research on delta development mechanisms by core researchers. The construction of an estuary barrage is one of the main factors effecting estuarine circulation and has altered the physical oceanic environment, area of deposition, atmospheric environment, and vegetation community of the delta. These factors affect the estuary circulation in turn, altering the delta. Along the Nakdong River, an unsteady-state sandy barrier appears at approximately three times the distance of the wavelength of incident offshore waves, and this terrain forms approximately 10-15 years after reclamation in the interdistributary upper stream and transforms the shoreline. It is necessary to develop a technique to predict terrain change that reproduces the erosion and accumulation of estuarine deposits. To determine the parameters and variables necessary to reproduce this system, continuous on-site monitoring is necessary. The existing research did not fully examine the terrain changes in Nakdong River Estuary or the periodic developmental characteristics. To understand the future process of estuary delta development, it is necessary to establish an integrated management system.

Real-Time Scheduling System Re-Construction for Automated Manufacturing in a Korean 300mm Wafer Fab (반도체 자동화 생산을 위한 실시간 일정계획 시스템 재 구축에 관한 연구 : 300mm 반도체 제조라인 적용 사례)

  • Choi, Seong-Woo;Lee, Jung-Seung
    • Journal of Intelligence and Information Systems
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    • v.15 no.4
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    • pp.213-224
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    • 2009
  • This paper describes a real-time scheduling system re-construction project for automated manufacturing at a 300mm wafer fab of Korean semiconductor manufacturing company. During executing this project, for each main operation such as clean, diffusion, deposition, photolithography, and metallization, each adopted scheduling algorithm was developed, and then those were implemented in a real-time scheduling system. In this paper, we focus on the scheduling algorithms and real-time scheduling system for clean and diffusion operations, that is, a serial-process block with the constraint of limited queue time and batch processors. After this project was completed, the automated manufacturing utilizations of clean and diffusion operations became around 91% and 83% respectively, which were about 50% and 10% at the beginning of this project. The automated manufacturing system reduces direct operating costs, increased throughput on the equipments, and suggests continuous and uninterrupted processings.

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High Quality Free-Standing GaN Substrate by Using Self-Separation Method (Self-Separation 방법을 적용한 고품질 Free-Standing GaN)

  • Son, Ho Ki;Lee, Young Jin;Kim, Jin-Ho;Hwang, Jonghee;Jeon, Dae-Woo;Lee, Hae-Yong
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.29 no.11
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    • pp.702-706
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    • 2016
  • We demonstrated that self-separation FS-GaN (freestanding-GaN) was grown on MELO (maskless epitaxially lateral overgrowth) GaN template by horizontal HVPE (hydride vapor phase epitaxy). Before thick GaN grwoth, MELO GaN template was grown on patterned GaN template by MOCVD (metal organic chemical vapor deposition). The laterally overgrown GaN would consist of a continuous well coalesced layer. The mixed TDD (threading dislocation density) of seed and wing region were $8{\times}10^8cm^{-2}$ and $7{\times}10^7cm^{-2}$, respectively. After thick GaN grown by HVPE, the self-separation between thick GaN and sapphire substrate was generated at seed region. The regions of self-separation for FS-GaN and sapphire were observed by FE-SEM. Moreover, Raman results indicated that the compressive strain of seed and wing regions at FS-GaN substrate were slightly released compared to that of thick GaN grown on conventional GaN template. The optical properties of the FS-GaN substrate were examined by using PL (photoluminescence). The PL exhibited that donor bound exciton and donor acceptor pair were observed at low temperature. The effects on optical and structural properties of FS-GaN substrate have been discussed in detail.

A Study on Control System of Multi Layer Sputtering Equipment (다층 박막 스퍼터링 장비의 제어시스템에 관한 연구)

  • Lee, Sun-Jong;Yoo, Heung-Ryol;Son, Yung-Deug
    • Journal of IKEEE
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    • v.22 no.2
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    • pp.302-308
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    • 2018
  • Multi-Layer Sputtering is aim to develop desired thickness thin film multi-layer with different materials. The multi-layer thin film deposition process occupies a relatively large portion in the process time, because the main reason is that it takes much time to move the substrate to be deposited and to make the chamber into a high vacuum state compared to the process time. Most of semiconductor and display industries sputter a single substance in one chamber and move boards through multi-continuous robots to another chamber to sputter other materials. This will inevitably require multiple chambers, vacuum pumps, and multi-contamination robots within the process facility. To solve these problems, this paper proposes a control system for multi-layer thin film sputtering devices that deposit different materials within a single vacuum chamber and is applied in TFT process. The manufacture and experiment of the control system proved its validity.

Effects of Bath Compositions and Plating Conditions on Electroless Copper Plating Rate with Sodium Hypophosphite as Reducing Agent (환원제로 차아인산나트륨을 사용한 무전해 동도금속도에 미치는 도금액 조성과 도금조건의 영향)

  • Oh, I.S;Park, J.D.;Bai, Y.H.
    • Journal of Power System Engineering
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    • v.5 no.2
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    • pp.71-78
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    • 2001
  • Using sodium hypophosphite as reducing agent, bath composition and plating condition of electroless copper plating on plating rate have been studied. The followings were determined as optimum, bath composition; $CuSO_4\;0.025M,\;NiSO_4\;0.002M,\;NaH_2PO_2\;0.4M$, sodium citrate 0.06M, $H_3BO_3$ 0.6M, thiourea or 2-MBT $0.2mg/{\ell}$, and operation conditions; pH $9{\sim}10$ at bath temperature rage of $60{\sim}70^{\circ}C$. A small amount of nickel ion($Ni^{2+}/Cu^{2+}$=0.002/0.025) to the hypophosphite reduced solution promotes autocatalysis and continuous plating. An additive such as thiourea or 2-MBT of a small amount($0.2mg/{\ell}$) can be used to stabilize the solution without changing plating rate much. The attivation energy between $20^{\circ}C\;and\;70^{\circ}C$ were calculated to be 11.3kcal/mol for deposition weight. Plating reaction had been ceased by the adjustment of pH above 13, temperature higher than $90^{\circ}C\;and\;under\;20^{\circ}C$. Deposited surface became worse in the case of increment of bath temperature above $80^{\circ}C$.

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Applicability Evaluation to Grid-based Rainfall-Runoff-Sediment Model for Sediment Discharge Estimation (격자기반 강우-유출-유사 모형의 유사량 산정에 관한 적용성 평가)

  • Choi, Hyun Gu;Park, Jun Hyung;Han, Kun Yeun
    • Journal of Wetlands Research
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    • v.19 no.1
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    • pp.132-143
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    • 2017
  • It is essential to obtain periodic sediment discharge data in a river in order to minimize problems that may arise from the erosion, transport, and deposition of sediment. However, it is difficult to estimate sediment discharge by the sediment discharge measurement plan in Korea at present, and empirical fomulas or numerical models are used to replace them. This paper has applied the K-DRUM model, a grid-based rainfall-runoff-sediment model, to estimate sediment discharge and ensure the continuity of the data in the watershed. Discharge and sediment load in 17 watersheds were estimated and the applicability of the model was analyzed through comparisons with measured data. For quantitative evaluation, NSE, PBIAS and RSR items were used, and discharge results reflected the tendency of rainfall and showed high statistical value. In case of sediment discharge, the soil erosion process of the watershed is physically well reflected. When the calibration was performed using the measure data, the applicability seems to be excellent in estimating the continuous sediment discharge data in the real watershed.