• Proceedings of the Materials Research Society of Korea Conference
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• 2009.11a
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• pp.33.1-33.1
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• 2009

To date, nanostructured tungsten oxides with a variety of stoichiometries, such as WO3, WO2.9, W18O49, and WO2, have been prepared, because they are promising candidates for applications such as gas sensors, photocatalysts, electrochromic devices, and field emission devices. Among them, W18O49 and WO2 have been widely studied due to their outstanding chemical sensing, catalytic, and electron emissive properties. Here we report, for the first time, a one-pot solution-phase route to synthesizing a novel composite hierarchical hollow structure without adding catalysts, surfactants, or templates. The products, consisting of a WO2 hollow core sphere surrounded by a W18O49 nanorod shell (yielding a sea urchin-like structure), were generated as discrete structures via Ostwald ripening. To our knowledge, this type of composite hierarchical core/shell structure has not been reported previously. The morphological evolution and the detailed growth mechanism were carefully studied. We also demonstrate that the size of the hollow urchins is readily tunable by controlling the reactant concentrations.Interestingly, although bulk tungsten oxides are weakly paramagnetic or diamagnetic, the as-prepared products show unusual ferromagnetic behavior atroom temperature. The urchin structures also show a very high Brunauer-Emmet-Teller (BET) surface area, suggesting that they may potentially be applied to chemical sensor or effective catalyst technologies.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2005.04a
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• pp.17-20
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• 2005

In-situ structural health monitoring of filament wound pressure tanks were conducted during water-pressurizing test using embedded fiber Bragg grating (FBG) sensors. We need to monitor inner strains during working in order to verify the health condition of pressure tanks more accurately because finite element analyses on filament wound pressure tanks usually show large differences between inner and outer strains. Fiber optic sensors, especially FBG sensors can be easily embedded into the composite structures contrary to conventional electric strain gages (ESGs). In addition, many FBG sensors can be multiplexed in single optical fiber using wavelength division multiplexing (WDM) techniques. We fabricated a standard testing and evaluation bottle (STEB) with embedded FBG sensors and performed a water-pressurizing test. In order to increase the survivability of embedded FBG sensors, we suggested a revised fabrication process for embedding FBG sensors into a filament wound pressure tank, which includes a new protecting technique of sensor heads, the grating parts. From the experimental results, it was demonstrated that FBG sensors can be successfully adapted to filament wound pressure tanks for their structural health monitoring by embedding.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2005.11a
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• pp.153-156
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• 2005

Nondestructive sensing of electrospun PYDF web and multi-wall carbon nanotube (MWCNT)/epoxy composites were investigated using electro-micromechanical technique. Electrospinning is a technique used to produce micron to submicron diameter polymeric fibers. Electrospun PVDF web was also evaluated for the sensing properties by micromechanical test and by measurement electrical resistance. CNT composite was especially prepared for high volume contents, 50 vol% of reinforcement. Electrical contact resistivity on humidity sensing was a good indicator for monitoring as for multifunctional applications. Work of adhesion using contact angle measurement was studied to correlate acid-base surface energy between carbon fiber and CNF composites, and will study furher for interfacial adhesion force by micromechanical test.

• Transactions of the Korean Society of Mechanical Engineers
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• v.18 no.2
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• pp.359-371
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• 1994

A drop weight type impact test system is designed and set up to experimentally investigate impact responses of composite laminates subjected to the low-velocity impact. Using the test system, the impact velocity and the rebound velocity of the impactor as well as the impact force history are measured. An error of the measured data due to a difference in measuring position of the sensor is corrected and, for the estimation of real contact force history, a method of correcting an error due to friction forces is developed. Experimental methods to fix the boundary edgy of laminate specimens in impact testing are investigated and the impact tests on the specimens fixed by those methods are performed. Impact force histories and dynamic strains measured from the tests are compared with numerical results from the finite element analysis using the contact law. Consequently, the nonlinear numerical results considering the large deflection effects are agreed with the experimental results better than the linear ones.

• Journal of Power System Engineering
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• v.18 no.6
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• pp.166-173
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• 2014

In this study, a laminated composite material with dispersing aluminum oxide powder between the CFRP laminate plies, and also CFRP composites without aluminium oxide powder were fabricated for Mode I experiments using the DCB specimen and a tensile test. The behavior of the crack and the change of the interfacial fracture toughness were evaluated. Also in order to evaluate the damage mechanism for the crack extension, the AE sensor on the surface of the DCB test specimen was attached. AE amplitude was estimated for CFRP-alumina and CFRP composite. And the fracture toughness was evaluated by the stress intensity factor and energy release rate. The results showed that an unstable crack was propagated rapidly in CFRP composite specimen along with the interface, but crack propagation in CFRP-alumina specimen was relatively stable. From results, we show that aluminium oxide powder spreaded uniformly in the interface of the CFRP laminate carried out the role for preventing the sudden crack growth.

• Journal of the Korean Society for Precision Engineering
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• v.11 no.1
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• pp.54-62
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• 1994

This paper presents active control methodologies to suppress structural deflections of a composite beam using a distributed piezoelectric-film actuator and sensor. Three types of different controllers are employed to achieve vibration suppression. The controllers are established depending upon the information on the velocity components of the structrue and on the deflection magnitudes as well. They are constant-amplitude controller(CAC), constant-gain mcontroller(CGC), and constant-amplitude-gain controller(CAGC). For the minimization of the residual vibration (chattering in a settled phase), which is the practical shortcoming of the conventional CAC dur to time delay phenomenon of the hardware system, a new control algoritym CAGCis designed by selecting switching constants in an optimal manner with respect to the initial tip deflection and the applied voltage. The experimental investigations of the transient and forced vibration control for the first vibrational mode are undertaken in order to compare the suppression efficiency of each control algorithm. Moreover, simultaneous controllability of various vibrational modes through the proposed scheme is also experimentally verified by pressenting both the transfer function and the phase.

• Composites Research
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• v.30 no.2
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• pp.138-144
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• 2017

Damage sensing of polymer composite films consisting of poly(dicyclopentadiene) p-DCPD and carbon nanotube (CNT) was studied experimentally. Only up to 1st ring-opening polymerization occurred with the addition of CNT, which made the modified film electrically conductive, while interfering with polymerization. The interfacial adhesion of composite films with varying CNT concentration was evaluated by measuring the wettability using the static contact angle method. 0.5 wt% CNT/p-DCPD was determined to be the optimal condition via electrical dispersion method and tensile test. Dynamic fatigue test was conducted to evaluate the durability of the films by measuring the change in electrical resistance. For the initial three cycles, the change in electrical resistance pattern was similar to the tensile stress-strain curve. The CNT/p-DCPD film was attached to an epoxy matrix to demonstrate its utilization as a sensor for fracture behavior. At the onset of epoxy fracture, electrical resistance showed a drastic increase, which indicated adhesive fracture between sensor and matrix. It leads to prediction of crack and fracture of matrix.

• Composites Research
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• v.33 no.4
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• pp.228-233
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• 2020

In this paper, a single lap shear test was performed using a glass fiber reinforced composite material (GFRC). Pencil lead drawn paper sensor (PLDPS) was applied for single lap shear test being performed. Bisphenol-A epoxy and amine hardener were used as adhesives combining with composite materials. To make a difference in adhesive properties, the adhesive was cured under different conditions. PLDPS was made of a 4B pencil on A4 paper. Because graphite in a pencil was an electrically conductive substance, electric resistance (ER) could be measured. A change in ER was observed by a position where a PLDPS was attached to single lap shear specimens. It was confirmed that the change in ER was different depending on two attached positions and was observed by lap shear strain as well. In case the lap shear strain was large, the change in ER of PLDPS was high. This was because the larger the extension of the adhesive part, the larger the degree of bending of the specimen and thus the larger the distance change between two electrodes.

• Journal of Sensor Science and Technology
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• v.10 no.6
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• pp.286-294
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• 2001

In this study, 3-D underwater object recognition using the self-made 3-3 type composite ultrasonic transducer and modified SOFM(Self Organizing Feature Map) neural network are investigated. Properties of the self-made 3-3 type composite specimens are satisfied considerably with requirements as an underwater ultrasonic transducer's materials. 3-D underwater all object's recognition rates obtained from both the training data and testing data in different objects, such as a rectangular block, regular triangular block, square block and cylinderical block, were 100% and 94.0%, respectively. All object's recognition rates are obtained by utilizing the self-made 3-3 type composite transducer and SOFM neural network. From the object recognition rates, it could be seen that an ultrasonic transducer fabricated with the self-made 3-3 type composite resonator will be able to have application for the underwater object recognition.

• Polymer(Korea)
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• v.26 no.1
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• pp.105-112
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• 2002

The low actuation voltage and quick bending response of IPMC(ion-exchange polymer metal composite) are considered attractive for the construction of various types of actuators. In this study, in order to develop a new type actuators by using the IPMC platinum electrode of IPMC are fabricated by using electroless impregnation-reduction method plating. As the platinum-plating times are increased, IPMC performance was improved in terms of bending displacement and force due to the enhanced surface conductivity. In addition, we investigated the basic actuation characteristics of resonance frequency and actuator length as well as the effect of water uptake and ion mobility. Using the classical laminate theory(CLT), a modeling methodology was developed to predict the deformation, bending moment, and residual stress distribution of anisotropic IPMC thin plates. In this modeling methodology, the internal stress evolved by the unsymmetric distribution of water inside IPMC was quantitatively calculated and subsequently the bending moment and the curvature were estimated for various geometry of IPMC actuator.