• Title/Summary/Keyword: composite powder

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Photocatalysis Characteristics of Nano Cu/TiO2 Composite Powders Fabricated from Salt Solution (염용액으로부터 제조된 Cu/TiO2복합분말의 광촉매 특성)

  • 고봉석;안인섭;배승열;이상진
    • Journal of Powder Materials
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    • v.10 no.2
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    • pp.136-141
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    • 2003
  • In the present study, $TiO_2$ imbedded copper matrix powders have been successfully prepared from the ($CuSO_4+TiO_2+Zn$) composite salt solution. The composite $Cu/TiO_2$ powders were formed by drying the solution at $200{\sim}~400^{\circ}C$ in the hydrogen atmosphere. Photocatalytic characteristics was evaluated by detecting TOC (total organic carbon) amount with TOC analyzer (model 5000A Shimadzu Co). Phase analysis of $Cu/TiO_2$ composite powders was carried out by XRD, DSC and powder size was measured with TEM. The mean particle size of composite powders was about 100 nm and a few zinc and copper oxide phases was included. The reduction ratio of TOC amount was 60% by the composite $Cu/TiO_2$ powders under the UV irradiation for 8 hours.

Fabrication of WC-17%Co Composite Powder for Thermal Spray by Spray-Drying Method and HVOF Thermal Spray Characteristics (분무건조법에 의한 용사용 WC-17%Co 복합분말제조 및 HVOF(High Velocity Oxy-Fuel) 용사특성)

  • 설동욱;김병희;임영우;정민석;서동수
    • Journal of Welding and Joining
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    • v.14 no.6
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    • pp.101-108
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    • 1996
  • In this study, WC-l7wt% Co composite powder for thermal spray was fabricated by spray drying method. The agglomerated composite powder had spheroidal morphology and the particle size distribution was 20~60${\mu}{\textrm}{m}$. WC and Co were distributed homogeneously. However, the strength of the spray-dried agglomerate was low due to the pores within the agglomerate. Therefore, the spray-dried agglomerate was broken down during HVOF thermal spray and the microstructure was inhomogeneous with many pores within the coating layer. And the decomposition of WC to W and $W_{6}$ $C_{2.54}$ was accelerated. The strength and flowability of the agglomerate were greatly improved by sintering heat treatment(110$0^{\circ}C$, 1 hour, hi atmosphere), and then the coating layer showed dense and homogeneous microstructure with well-developed splats. The hardness of the coating layer was H $v_{300}$ = 1072.2.2.

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Densification Behavior of Aluminum Alloy Powder Mixed with Zirconia Powder Inclusion Under Cold Compaction (냉간압축 하에서 지르코니아 분말이 혼합된 알루미늄합금 분말의 치밀화 거동)

  • Ryu, Hyun-Seok;Lee, Sung-Chul;Kim, Ki-Tae
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.26 no.7
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    • pp.1324-1331
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    • 2002
  • Densification behavior of composite powders was investigated during cold compaction. Experimental data were obtained for aluminum alloy powder mixed with zirconia powder inclusion under triaxial compression. The Cap model with constraint factors was implemented into a finite element program (ABAQUS) to simulate compaction responses of composite powders during cold compaction. Finite element results were compared with experimental data for densification behavior of composite powders under cold isostatic pressing and die compaction. The agreements between experimental data and finite element calculations from the Cap model with constraint factors were good.

Synthesis ofSialon-SiC Composite Powder from Alkoxides and the Powder Properties(I) (알콕사이드로부터 Sialon-SiC계 복합분말의 합성과 분말특성(I))

  • 전명철;이홍림
    • Journal of the Korean Ceramic Society
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    • v.27 no.2
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    • pp.265-273
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    • 1990
  • Fine Si-Al-OH-C coprecipitate powders were prepared from Si(OC2H5)4, Al(i-OC3H7)3, and carbon black by a hydrolysis method before fabrication of Sialon-SiC composite powder by carbothermal reduction at 1350$^{\circ}C$ for 10h under N2/H2 mixed atmosphere. The characterization of the synthesized Sialon-SiC composite powders was performed using XRD, BET, SEM, TEM and particle size analysis methods. The average particle size and specific surface area of the synthesized Sialon-SiC composite powder were 0.13$\mu\textrm{m}$ and 20.1㎡/g, respectively when Z=1 and N2 : H2=50 : 50.

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Development of Novel Composite Powder Friction Modifier for Improving Wheel-rail Adhesion in High-speed Train (고속열차 점착계수 향상을 위한 신규 복합재료 분말 마찰조절재 개발 및 점착력 특성 평가)

  • Oh, Min Chul;Ahn, Byungmin
    • Journal of Powder Materials
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    • v.25 no.6
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    • pp.501-506
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    • 2018
  • With the recent remarkable improvements in the average speeds of contemporary trains, a necessity has arisen for the development of new friction modifiers to improve adhesion characteristics at the wheel-rail interface. The friction modifier must be designed to reduce slippage or sliding of the trains' wheels on the rails under conditions of rapid acceleration or braking without excessive rolling contact wear. In this study, a novel composite material consisting of metal, ceramic, and polymer is proposed as a friction modifier to improve adhesion between wheels and rails. A blend of Al-6Cu-0.5Mg metallic powder, $Al_2O_3$ ceramic powder, and Bakelite-based polymer in various weight-fractions is hot-pressed at $150^{\circ}C$ to form a bulk composite material. Variation in the adhesion coefficient is evaluated using a high-speed wheel-rail friction tester, with and without application of the composite friction modifier, under both dry and wet conditions. The effect of varying the weighting fractions of metal and ceramic friction powders is detailed in the paper.

Mechanical Properties of Polyethylene/Polypropylene/Waste Tire Rubber Powder Composites (폴리에틸렌/폴리프로필렌/폐타이어고무분말 복합체의 기계적 특성)

  • Choi, Jeong-Su;Park, Cha-Cheol
    • Elastomers and Composites
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    • v.46 no.4
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    • pp.318-323
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    • 2011
  • To recycle the waste tire rubber powder, rubber powder composite for waterproof sheet was prepared, and analyzed the effect of the kind of resin and the amount of crosslinking agent on the mechanical property of the composites. The elongation-at-break of the PE composite increased more than 3 times as EPDM was added into rubber composites. As the content of the crosslinking agent increased, the tensile strength of composite increased as well. When recycled polypropylene was used, the increase in composite's tensile strength was more than 3 times. Therefore to use the recycled PP in composite is more effective rather than PP in term mechanical properties.

Microstructure and Wear Properties of Oxide Dispersion Strengthened Steel Powder Added Steel-Based Composite Material for Automotive Part (산화물 분산 강화 강 분말이 첨가된 자동차 부품용 철계 복합 소재의 미세조직 및 마모 특성)

  • Kim, Young-Kyun;Park, Jong-Kwan;Lee, Kee-Ahn
    • Journal of Powder Materials
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    • v.25 no.1
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    • pp.36-42
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    • 2018
  • In order to expand the application of oxide dispersion-strengthened (ODS) steel, a composite material is manufactured by adding mechanically alloyed ODS steel powder to conventional steel and investigated in terms of microstructure and wear properties. For comparison, a commercial automobile part material is also tested. Initial microstructural observations confirm that the composite material with added ODS steel contains i) a pearlitic Fe matrix area and ii) an area with Cr-based carbides and ODS steel particles in the form of a $Fe-Fe_3C$ structure. In the commercial material, various hard Co-, Fe-Mo-, and Cr-based particles are present in a pearlitic Fe matrix. Wear testing using the VSR engine simulation wear test confirms that the seatface widths of the composite material with added ODS steel and the commercial material are increased by 24% and 47%, respectively, with wear depths of 0.05 mm and 0.1 mm, respectively. The ODS steel-added composite material shows better wear resistance. Post-wear-testing surface and cross-sectional observations show that particles in the commercial material easily fall off, while the ODS steel-added material has an even, smooth wear surface.

Fabrication and Evaluation of 5 vol%CNT/Al Composite Material by a Powder in Sheath Rolling Method (분말시스압연법에 의한 5 vol%CNT/Al 복합재료의 제조 및 평가)

  • Hong, Dongmin;Kim, Woo-Jin;Lee, Seong-Hee
    • Korean Journal of Materials Research
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    • v.23 no.11
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    • pp.607-612
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    • 2013
  • A powder in sheath rolling method was applied to the fabrication of a carbon nano tube (CNT) reinforced aluminum composite. A 6061 aluminum alloy tube with outer diameter of 31 mm and wall thickness of 2 mm was used as a sheath material. A mixture of pure aluminum powder and CNTs with a volume content of 5% was filled in the tube by tap filling and then processed to an 85% reduction using multi-pass rolling after heating for 0.5 h at $400^{\circ}C$. The specimen was then further processed at $400^{\circ}C$ by multi-pass hot rolling. The specimen was then annealed for 1 h at various temperatures that ranged from 100 to $500^{\circ}C$. The relative density of the 5vol%CNT/Al composite fabricated using powder in sheath rolling increased with increasing of the rolling reduction, becoming about 97% after hot rolling under 96 % total reduction. The relative density of the composite hardly changed regardless of the increasing of the annealing temperature. The average hardness also had only slight dependence on the annealing temperature. However, the tensile strength of the composite containing the 6061 aluminum sheath decreased and the fracture elongation increased with increasing of the annealing temperature. It is concluded that the powder in sheath rolling method is an effective process for fabrication of CNT reinforced Al matrix composites.