• Title/Summary/Keyword: complex particle

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Development and Application of High-resolution 3-D Volume PIV System by Cross-Correlation (해상도 3차원 상호상관 Volume PIV 시스템 개발 및 적용)

  • Kim Mi-Young;Choi Jang-Woon;Lee Hyun;Lee Young-Ho
    • Proceedings of the KSME Conference
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    • 2002.08a
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    • pp.507-510
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    • 2002
  • An algorithm of 3-D particle image velocimetry(3D-PIV) was developed for the measurement of 3-D velocity Held of complex flows. The measurement system consists of two or three CCD camera and one RGB image grabber. Flows size is $1500{\times}100{\times}180(mm)$, particle is Nylon12(1mm) and illuminator is Hollogen type lamp(100w). The stereo photogrammetry is adopted for the three dimensional geometrical mesurement of tracer particle. For the stereo-pair matching, the camera parameters should be decide in advance by a camera calibration. Camera parameter calculation equation is collinearity equation. In order to calculate the particle 3-D position based on the stereo photograrnrnetry, the eleven parameters of each camera should be obtained by the calibration of the camera. Epipolar line is used for stereo pair matching. The 3-D position of particle is calculated from the three camera parameters, centers of projection of the three cameras, and photographic coordinates of a particle, which is based on the collinear condition. To find velocity vector used 3-D position data of the first frame and the second frame. To extract error vector applied continuity equation. This study developed of various 3D-PIV animation technique.

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Particle Size, Morphology and Color Characteristics of C.I. Pigment Red 57:1 : 1. Effect of Synthesis Conditions

  • Seo, Hee Sung;Lee, Hyun Kyung;Yoo, Eui Sang
    • Textile Coloration and Finishing
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    • v.27 no.4
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    • pp.229-244
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    • 2015
  • The effects of synthesis conditions on characteristics of the calcium-azo complex pigment, C.I. Pigment Red 57:1, were studied. It was mainly considered that the industrially required synthesis conditions for lowering electrical conductivity of the pigment solution keeping pigment quality such as particle size and color characteristics. Three parameters were chosen as control factors during the synthesis. The first was the amount of hydrochloric acid added to transform sodium nitrite into nitrous acid. The second was the amount of calcium chloride added to insolubilize the synthesized azo dye. The final factor was pH control during the coupling reaction. The electrical conductivity and pigment aggregate particle size were dependent on the amount of hydrochloric acid and calcium chloride. Higher HCl concentration gave brighter yellowish-red color because of smaller particle aggregate size and narrower size distribution. Amount of charged ions in the synthesis process might affect the "lake" formation resulting different particle aggregate size and color shade.

Velocity measurements in complex flows of non-Newtonian fluids

  • Muller, Susan J.
    • Korea-Australia Rheology Journal
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    • v.14 no.3
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    • pp.93-105
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    • 2002
  • Experimental methods for making quantitative measurements of velocity fields in non-Newtonian fluids are reviewed. Techniques based on light scattering spectroscopy - laser Doppler velocimetry and homodyne light scattering spectroscopy, techniques based on imaging the displacement of markers - including particle image velocimetry and molecular tagging velocimetry, and techniques based on nuclear magnetic resonance imaging are discussed. The special advantages and disadvantages of each method are summarized, and their applications to non-Newtonian flows are briefly reviewed. Example data from each technique are also included.

Determination of the Size Distribution of Magnetite Nanoparticles from Magnetic Measurements

  • Yoon, Sung-Hyun
    • Journal of Magnetics
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    • v.16 no.4
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    • pp.368-373
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    • 2011
  • Particle size distributions in 10 nm magnetite ferrofluids are analyzed based on both dc and ac magnetic measurements. Modified log-normal distributions are used for fitting the experimental results, which allows for a proper account of the narrow distributions. The calculated average particle sizes are in good agreement with the TEM results. However the ac method gives a much narrower distribution width than that of the dc magnetization curve fit. The proposed measurements combined with the analysis methods are useful for the characterization of ferrofluids being considered for biomedical applications.

Studies on mixing of pharmaceutical powders

  • Choi, Woo-Sik
    • Archives of Pharmacal Research
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    • v.5 no.2
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    • pp.53-60
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    • 1982
  • The mixing of salicylic acid and wheat starch powders was studied using a V-type mixer. After the optimum operating conditions of the mixer were examined, the mixing characteristics relating to dilution ratio, particle size of active ingradient and addition ratio of lubricants were investigated. The coefficient of variation was expressed by a power law relating to the dilution ratio and the particle size of active ingredient. Furthermore, the comparison of results with the theoretically estimated value of mixing index suggested that the mixing of cohesive pharmacceutical powders is a complex stochastic process and cannot be explained fully by a simple theory based on a complete random mixing.

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Fabrication of Reaction Sintered SiC Materials by Complex Slurry with Nano Size Particles (나노입자 혼합 복합슬러리를 이용한 반응소결 SiC 재료의 제조)

  • Lee Sang-Pill
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.29 no.3 s.234
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    • pp.425-431
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    • 2005
  • The efficiency of complex slurry preparation route for developing the high performance SiC matrix of $RS-SiC_{f}/SiC$ composites has been investigated. The green bodies for RS-SiC materials prior to the infiltration of molten silicon were prepared with various C/SiC complex slurries, which associated with both the sizes of starting SiC particles and the blending conditions of starting SiC and C particles. The characterization of Rs-SiC materials was examined by means of SEM, EDS and three point bending test. Based on the mechanical property-microstructure correlation, the process optimization is also discussed. The flexural strength of Rs-SiC materials greatly depended on the content of residual Si. The decrease of starting SiC particle size in the C/SiC complex slurry was effective for improving the flexural strength of RS-SiC materials.

Synthesis of ${\alpha}-Fe_2O_3$ Powders by the Polymerized Complex Method (Polymerized Complex법에 의한 ${\alpha}-Fe_2O_3$ 분말의 제조)

  • 강경원;정용선;오근호
    • Journal of the Korean Ceramic Society
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    • v.35 no.3
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    • pp.239-244
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    • 1998
  • Iron complexes were prepared using ferric nitrate and ethylene glycol as starting materials and the ul-trafine ${\alpha}-Fe_2O_3$ particles with the sizes smaller than 200nm were obtained by the pyrolysis of iron com-plexes at over $350^{\circ}C$ In addition the decomposition mechanism of the synthesized iron complexes was in-vestigated by differential scanning calorimeter X-ray diffractometer and IR spectrometer. Transmission electron microscopy and BET method were performed to analyze the effects of ferric nitrate contents and reaction temperatures on the size and shape of the particles.

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THE COMPLEX PERMEABILITY AND MATCHING FREQUENCY OF FERRITE MICROWAVE ABSORBER

  • Shin, Jae-Young;Oh, Jae-Hee
    • Journal of the Korean Magnetics Society
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    • v.5 no.5
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    • pp.800-804
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    • 1995
  • The complex permeability dispersions and the microwave absorbing phenomena are investigated in ferrite microwave absorber. The complex permeability of NiZn ferrite, NiZnCo ferrite, and Y-type hexagonal ferrite were measured in 200MHz-14GHz range. Two types of resonances, the domain wall and the spin rotational resonance, were observed. With a ferrite particle with a diameter of about $1\;\mu\textrm{m}$, only spin rotational resonance were observed. The theoretical matching frequency is determined by plotting the measured complex permeability locus on the impedance matching solution map. One or two impedance matching phenomena are observed in the ferrite absorbers according to their complex permeability loci on the impedance matching solution map. The first matching frequency, found in the ferrite-rubber composites, which was higher than that of spin rotational resonance, increased with spin rotational resonance frequency.

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Synthesis and Characteristics of SrAl2O4: Eu2+, Dy3+ Long Afterglow Phosphors by Polymerized Complex Method (착체중합법을 이용한 SrAl2O4: Eu2+, Dy3+ 축광성 형광체의 합성)

  • Kim, Tae-Ho;Hwang, Hae-Jin;Kim, Jin-Ho;Hwang, Kwang-Taek;Han, Kyu-Sung
    • Korean Journal of Materials Research
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    • v.26 no.10
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    • pp.561-569
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    • 2016
  • $SrAl_2O_4$: $Eu^{2+}$ and $Dy^{3+}$ phosphorescent phosphors were synthesized using the polymerized complex method. Generally, phosphorescent phosphors synthesized by conventional solid state reaction show a micro-sized particle diameter; thus, this process is restricted to applications such as phosphorescent ink and paint. However, it is possible to synthesize homogeneous multi-component powders with fine particle diameter by wet process such as the polymerized complex method. The characteristics of $SrAl_2O_4$: $Eu^{2+}$ and $Dy^{3+}$ powders prepared by polymerized complex method with one and two step calcination processes were comparatively analyzed. Temperatures of organic material removal and crystallization were observed through TG-DTA analysis. The crystalline phase and crystallite size of the $SrAl_2O_4$: $Eu^{2+}$ and $Dy^{3+}$ phosphorescent phosphors were analyzed by XRD. Microstructures and afterglow characteristics of the $SrAl_2O_4$: $Eu^{2+}$ and $Dy^{3+}$ phosphors were measured by SEM and spectrofluorometry, respectively.