• Title/Summary/Keyword: cold-pressed

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Variation of Lattice Constant in Ni-W and Ni-W-Cu Alloys for YBCO Coated Conductor (YBCO 초전도 박막 선재용 Ni-W 및 Ni-W-Cu 합금의 격자상수 변화)

  • Kim Min-Woo;Jung Kyu-Dong;Jun Byung-Hyuk;Kim Hyoung-Seop;Kim Chan-Joong
    • Progress in Superconductivity
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    • v.7 no.1
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    • pp.64-68
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    • 2005
  • We fabricated Ni-based alloy substrates for YBCO coated conductor using powder metallurgy. Tungsten and copper were selected as alloy elements due to their mutual solubility to the base element of nickel. The alloying elements were mixed with nickel using ball milling and dried in air. The powder mixtures were packed in a rubber mold, cold isostatic pressed 200 MPa and made into rods. The compacted rods were sintered at $1150^{\circ}C$ for 6 hours for densification. It was confirmed by neutron diffraction experiment that W and Cu atoms made complete solid solution with Ni. Lattice constant of nickel alloy increased by $0.004{\AA}$ for 1at. $\%$ W in Ni-W alloy, $0.0006{\AA}$ for 1 at. $\%$ Cu in Ni-W-Cu alloy.

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Fabrication and characterization of Copper/Silicon Nitride composites

  • Ahmed, Mahmoud A.;Daoush, Walid M.;El-Nikhaily, Ahmed E.
    • Advances in materials Research
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    • v.5 no.3
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    • pp.131-140
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    • 2016
  • Copper/silicon nitride ($Cu/Si_3N_4$) composites are fabricated by powder technology process. Copper is used as metal matrix and very fine $Si_3N_4$ particles (less than 1 micron) as reinforcement material. The investigated powder were used to prepare homogenous ($Cu/Si_3N_4$) composite mixtures with different $Si_3N_4$ weight percentage (2, 4, 6, 8 and10). The produced mixtures were cold pressed and sintered at different temperatures (850, 950, 1000, $1050^{\circ}C$). The microstructure and the chemical composition of the produced $Cu/Si_3N_4$ composites were investigated by (SEM) and XRD. It was observed that the $Si_3N_4$ particles were homogeneously distributed in the Cu matrix. The density, electrical conductivity and coefficient of thermal expansion of the produced $Cu/Si_3N_4$ composites were measured. The relative green density, sintered density, electrical conductivity as well as coefficient of thermal expansion were decreased by increasing the reinforcement phase ($Si_3N_4$) content in the copper matrix. It is also founded that the sintered density and electrical conductivity of the $Cu/Si_3N_4$ composites were increased by increase the sintering temperature.

Development of Compressed-flattened Bamboo Impregnated with Low Molecular Weight PF Resin(1) (저농도 페놀수지 주입처리에 의한 평죽판 개발(1))

  • 이화형;김관의
    • Journal of the Korea Furniture Society
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    • v.12 no.2
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    • pp.29-38
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    • 2001
  • This study was carried out to develope a new process of flattening bamboo pieces(3 months old) by two steps of utilizing microwave oven and hot press. Internode bamboo pieces were impregnated with low molecular weight phenol formaldehyde resin (PF) under vacuum of 76 cmHg, heated in a household microwave oven in 1 minute, pressed on the temperature of $145^{\circ}C$ by the hot press for 10 minute, and then cooled by the cold press in their flattened form. The physical and mechanical . Properties of compressed flattened bamboo were as follows: 1) PF1(Mw:427) and PF2(Mw:246) sol. met the success of flattening of internode bamboo pieces in both of P. bambusoides and P. nigra var. PF2 showed the more plasticity to flatten the bamboo than PFI. The PF2 sol. with low molecular weight(Mw:246) gave the more weight gain than that of PF1 in the equal concentration. PF1 of 5% (NVC) and PF2 of 10% (NVC) sol. gave the best result for physical and mechanical properties and from a economical view point. 2) The PFI of 5% (NVC) sol. with low molecular weight decreased the water absorption of 62-63% and increased the bending strength (MaR) of 80-90%, compression strength of 43-54%. 3) The PF2 of 10% (NVC) sol. with low molecular weight decreased the water absorption of 56-57% and increased the bending strength (MaR) of 64-86%, compression strength of 39-63%.

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Delayed Operation Characteristics of Power Shuttle According to Hydraulic Oil Temperature in the Hydraulic Circuit of Agricultural Tractor

  • Park, Yoon-Na;Kim, Dae-Cheol;Park, Seung-Je
    • Journal of Biosystems Engineering
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    • v.40 no.2
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    • pp.95-101
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    • 2015
  • Purpose: During the start-up period, the response time of a hydraulic system increases in the winter because of the increased oil viscosity caused by the cold weather. The problems of delayed tractor starting and excessive wear of the clutch disk occur for these reasons. Therefore, this study develops an analysis model using the commercial hydraulic analysis program AMESim to examine the characteristics of delays in power shuttle starting at different oil temperatures. Methods: In the experiment, a tractor was stationary on a flat surface with the engine running at a constant speed of 1,080 rpm. The forward lever was then pressed to activate the power shuttle at three different oil temperatures, and the pressure changes were measured. The pressure on the forward clutch control valve was measured by a pressure gauge installed on the hydraulic line supplied to the transmission from the main valve. An analysis model was also developed and verified with actual tests. Results: The trend of the simulated pressures of the power shuttle is similar to that of the measured pressures, and a constant modulation period was observed in both the simulation and test results. However, the difference found between the simulation and test results was the initial pressure required to overcome the initial force of the clutch spring. Conclusions: This study also examines the characteristics of the delayed startup of the power shuttle at different oil temperatures through simulations.

Fundamental Properties of Composite Board Made with Oriented Strand Board and Three Different Species of Veneer

  • Yanti, Hikma;Massijaya, Muh Yusram;Cahyono, Tekat Dwi;Novriyanti, Eka;Iswanto, Apri Heri
    • Journal of the Korean Wood Science and Technology
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    • v.47 no.2
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    • pp.239-248
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    • 2019
  • This research presents an improvement of the physical and mechanical properties of composite board (com-ply) made of Oriented Strand Board (OSB) coated with wood veneer of Pine (Pinus merkusii), Avocado (Persea Americana) and Mahogany (Swietenia mahogany). 1.5 mm thick veneers of those three wood types were adhered to the surface of OSB using two adhesive types: epoxy and isocyanate. The adhesive with the glue spread of $250g\;m^{-2}$ applied using single glue line was spread and then cold pressed with the pressure of $15kg\;cm^{-2}$ for 3 hours. The research result showed an improving dimension stability of com-ply, but not found on all parameters of physical property test. The moisture content seemed to be influenced by the com-ply type, yet not related to its thickness swelling, water absorption and linear expansion. The exception took place in the parallel linear expansion when immersed for 2 hours. The highest to the lowest increases of MOE and MOR were consecutively found on OSB coated with wood veneer of Pine, Mahogany and Avocado. However, the increases were statistically insignificant. The highest increasing screw hold power was found at the com-ply type AE (avocado veneer and epoxy adhesive) that was by 28%.

Solid state reactive sintering of cold pressed thermoelectric Mg3Sb2 (냉간 압축 성형한 Mg3Sb2 열전재료의 고상 반응 소결)

  • Kim, In-Ki;Jang, Kyung-Wook;Oh, Han-Jun
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.24 no.4
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    • pp.176-182
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    • 2014
  • We intended to prepare $Mg_3Sb_2$ compound bodies through solid state reactive sintering after cold-pressing mixtures of elementary Mg and Sb powders and investigated the crystal phases of the sintered bodies according to Mg/Sb mole ratios and reaction temperatures. The $Mg_3Sb_2$ bodies sintered at the temperatures of 773~843 K showed typical crystalline phases of $Mg_3Sb_2$ compounds, but their diffraction angles in XRD patterns were slightly different along with the vertical axis of the bodies obtained. All the bottom parts of the sintered $Mg_3Sb_2$ bodies were composed of the typical crystalline phases of $Mg_3Sb_2$ compounds and their diffraction angles were completely in accord with those of the ${\alpha}-Mg_3Sb_2$ phase, when Mg : Sb = 3.15 : 1.85 at 823 K, or when the Mg moles were greater than or equal to 3.10 at 843 K. It was considered that the slightly remaining Mg phases were formed by precipitation from ${\alpha}-Mg_3Sb_2$ phases during the solidification process of liquid phase.

Effects of Pre-synthesized $BaTiO_3$ Addition on the Microstructure and Dielectric/ Piezoelectric Properties of $(Bi_{0.5}Na_{0.5})_{0.94}Ba_{0.06}TiO_3$ Piezoelectric Ceramics

  • Khansur, Neamul Hayet;Yoon, Man-Soon;Kweon, Soon-Yong;Lee, Young-Geun;Ur, Soon-Chul
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2008.11a
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    • pp.189-189
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    • 2008
  • Due to the environmental issue vast research is going on to replace the widely used lead contented piezoelectric materials. Bismuth sodium titanate (abbreviated as BNT) based bismuth sodium titanate-barium titanate (abbreviated as BNBT) ceramic was prepared by using modified method rather than conventional mixed oxide method. This modification was made to improve the properties of BNT based ceramic. In this procedure $BaTiO_3$ (abbreviated as BT) was prepared using conventional mixed oxide method. Analytical grade raw materials of $BaCO_3$ and $TiO_2$ were weighted and ball milled using ethanol medium. The mixed slurry was dried and sieved under 80 mesh. Then the powder was calcined at $1100^{\circ}C$ for 2 hours. This calcined BT powder was used in the preparation of BNBT. Stoichiometric amount of $Bi_2O_3$, $Na_2CO_3$, $TiO_2$ and BT were weighted and mixed by using ball mill. The used calcination temperature was $850^{\circ}C$ for 2 hours. Calcined powder was taken for another milling step. BNBT disks were pressed to 15 mm of diameter and then cold isostatical press (CIP) was used. Pressed samples were sintered at $1150^{\circ}C$ for 2 hours. The SEM microstructure analysis revealed that the grain shape of the sintered ceramic was polyhedral and grain boundary was well matched where as the sample prepared by conventional method showed irregular arrangement and grain boundary not well matched. And sintered density was better (5.78 g/cc) for the modified method. It was strongly observed that the properties of BNBT ceramic near MPB composition was found to be improved by the modified method compare to the conventional mixed oxide method. The piezoelectric constant dB of 177.33 pC/N, electromechanical coupling factor $k_p$ of 33.4%, dielectric constant $K_{33}^T$ of 688.237 and mechanical quality factor $Q_m$ of 109.37 was found.

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Effect of Particle Pre-Treatment on Properties of Jatropha Fruit Hulls Particleboard

  • Iswanto, Apri Heri;Febrianto, Fauzi;Hadi, Yusuf Sudo;Ruhendi, Surdiding;Hermawan, Dede;Fatriasari, Widya
    • Journal of the Korean Wood Science and Technology
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    • v.46 no.2
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    • pp.155-165
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    • 2018
  • The objective of the research was to evaluate the effect of particle pre-treatment on physical, mechanical, and durability of jatropha fruit hulls (JFH) particleboard. The pre-treatments included were immersing in cold water, hot water, and acetic acid solution. After each treatment, the particles were dried up to 3% moisture content. Urea-formaldehyde (UF) resin was used to fabricate particleboards with board size, thickness and density target of 25 cm by 25 cm, 0.80 cm, and $0.70g/cm^3$, respectively. Board pressed at $130^{\circ}C$ for 10 minutes, and $25kg/cm^2$ pressure. The evaluation of particleboard followed the JIS A 5908-2003. Whilist their resistance to subterranean termite test (mass loss, mortality, antifeedant value and feeding rate) refers to the Indonesian standard (SNI 01.7207-2006). The physical and mechanical properties of particleboards showed that all pre-treatments decreased the pH of particles. Overall, all particle immersing treatments resulted of better physical and mechanical properties of particleboard than those of untreated ones. The acetic acid treatment resulted the best physical and mechanical properties of particleboard. Based on the mass loss of JFH particleboard, hot water and acetic acid treated particleboards were classified into weak resistance to subterranean attack. The other two treatments were classified into very weak resistance. Hot water treated particleboard provided the highest mortality and antifeedant as much as 87.40% and 34.20%, respectively. Based on antifeedant classification, hot water treated particleboards were classified into moderately strong resistance, while other treatments were categorized into weak resistance. The lowest feeding rate value ($45.30{\mu}g/termite/day$) was attained by hot water treatment.

Physical-Mechanical Properties of Laminated Board Made from Oil Palm Trunk (Elaeis guineensis Jacq.) Waste with Various Lamina Compositions and Densifications

  • PRABUNINGRUM, Dita Sari;MASSIJAYA, Muh Yusram;HADI, Yusuf Sudo;ABDILLAH, Imam Busyra
    • Journal of the Korean Wood Science and Technology
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    • v.48 no.2
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    • pp.196-205
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    • 2020
  • The purpose of this study was to investigate a method for improving the physical and mechanical properties of laminated board made from oil palm trunk (OPT). The effects of pretreating the lamina with heat-pressure and altering the lamina composition of the laminated board were investigated. The outer third of OPT in cross-section had high-density wood, while the underlying third had low to medium density. The hot press was applied to pretreat the lamina that had low to medium density. The lamina were 1.5 cm in thickness, 5 cm in width, and 65 cm in length. The hot press was applied at 2.94 MPa or 4.41 MPa at 150 ℃ for 60 minutes, and the target thickness of the lamina was 1 cm. The three layers of the laminated board samples were bonded with isocyanate adhesive at a glue spread of 300 g/㎡ and cold pressed at 0.98 MPa for 3 h. The laminated board samples were tested according to Japanese Agricultural Standard (JAS) 234-2003. The results showed that the densification of the inner lamina did not significantly affect the physical-mechanical properties of the laminated board produced. However, the laminated board made with high-density laminas for the outer layers fulfilled the JAS 234-2003 standard for the modulus of elasticity and the modulus of rupture.

Development and Luminescent Characteristics of $CaSiN_2$ Based Phosphors ($CaSiN_2$를 모체로 하는 형광체의 개발 및 발광 특성)

  • Lee, Soon-Seok;Lim, Sung-Kyoo
    • Journal of the Korean Institute of Telematics and Electronics D
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    • v.36D no.10
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    • pp.31-36
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    • 1999
  • The $CaSiN_2:Eu$ and $CaSiN_2:Tb$ phosphors were synthesized and analyzed to develop new nitride compound phosphors. $Ca_3N_2$, $Si_3N_4$ and $EuF_3$(or $TbF_3$) powders were mixed, cold-pressed, and sintered to synthesize $CaSiN_2:Eu$ and $CaSiN_2:Tb$ phosphors. Photoluminescence(PL) and electroluminescence(EL) characteristics of the synthesized phosphors were measured and found to be similar to general emission spectra of 뗘 and Tb ion, respecticely. Threshold voltage($V_{th)$) and luminance of the $CaSiN_2:Eu$ TFEL device fabricated by sputtering were 90 V and 1.62 $cd/m^2$ at 280 V, respectively. The charge-voltage(Q-V) and transferred charge-phosphor field($Q_t-F_p$) characteristics of the TFEL devices were also measured.

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