• Title/Summary/Keyword: cold-pressed

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Enhancement of Microstructural Homogeneity of W-Cu Pseudo-alloy by Adding W-Cu Composite Powder in Infiltration Process

  • Hong, Moon-Hee;Choi, Jae-Ho;Lee, Seong;Kim, Eun-Pyo;Noh, Joon-Woong;Lee, Sung-Ho;Kim, Young-Moo
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.948-949
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    • 2006
  • An infiltration technique using W-Cu composite powder has been developed to enhance microstructural uniformity of W-Cu pseudo-alloy. W-Cu composite powder, manufactured by reduction from $WO_3$ and CuO powder mixtures, were blended with W powder and then cold iso-statically pressed into a cylindrical bar under 150 MPa. The pressed samples were pre-sintered at $1300^{\circ}C$ for 1 hour under hydrogen to make a skeleton structure. This skeleton structure was more homogeneous than that formed by using W and Cu powder mixtures. The skeleton structures were infiltrated with Cu under hydrogen atmosphere. The infiltrated W-Cu pseudo-alloy showed homogeneous microstructure without Cu rich region

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Analysis of nutrients and antioxidants of sterilized and non-heat-pressed perilla oil (살균 및 비가열압착한 들깨오일의 영양성분 및 항산화 분석)

  • Kim, Yang-Hee;Chang, Ji-Hwe;Ha, Seo-Yeong;Park, Su-Jin;Park, Seon-Young;Jung, Tae-Hwan;Hwang, Hyo-Jeong;Shin, Kyung-Ok
    • Korean Journal of Food Science and Technology
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    • v.54 no.3
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    • pp.264-271
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    • 2022
  • In this study, the nutritional properties of sterilized and non-heat-pressed raw perilla oil (SRPO) were studied and its potential as a functional food was evaluated. The copper, cobalt, and calcium levels were high in sterilized and SRPO. The total polyphenol content and ABTS radical scavenging activity were the highest in SRPO, whereas nitrite scavenging activity was the highest in 45℃ cold pressed perilla oil (CPPO). The above results confirmed that sterilized and non-heat-pressed perilla oil had high mineral and total polyphenol contents, as well as ABTS radical scavenging activity and nitrite scavenging ability. The peroxide value of SRPO decreased as the storage period increased, and the acid value of low-temperature pressed perilla oil over 65℃ (LPPO) significantly increased. This work also provided an opportunity to develop a new method for manufacturing perilla oil, and it is hoped that these experiments will form a basis for the commercialization of perilla oil.

Effect of Cold Rolling on Fatigue Crack Propagation of TiNi/A16061 Shape Memory Composite (TiNi/A16061 형상기억복합재료의 피로균열진전에 대한 냉간압연효과)

  • Lee Jin-Kyung;Park Young-Chul;Lee Kyu-Chang;Lee Sang-Pill;Cho Youn-Ho;Lee Joon-Hyun
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.29 no.10 s.241
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    • pp.1315-1320
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    • 2005
  • TiNi alloy fiber was used to recover the original shape of materials using its shape memory effect. The shape memory alloy plays an important role within the metal matrix composite. The shape memory alloy can control the crack propagation in metal matrix composite, and improve the tensile strength of the composite. In this study, TiNi/A16061 shape memory alloy(SMA) composite was fabricated by hot press method, and pressed by a roller for its strength improvement. The four kinds of specimens were fabricated with $0\%,\;3.2\%,\;5.2\%\;and\;7\%$ and volume fraction of TiNi alloy fiber, respectively. A fatigue test has performed to evaluate the crack initiation and propagation for the TiNi/A16061 SMA composite fabricated by かis method. In order to study the shape memory effect of the TiNi alloy fiber, the test has also done under both conditions of the room temperature and high temperature. The relationship between the crack growth rate and the stress intensity factor was clarified for the composite, and the cold rolling effect was also studied.

Try out and Analytical Researches on Quenching Process of Coupled Torsion Beam Axle using Boron Steel Tube (보론강을 이용한 CTBA의 후열처리 공정 실험 및 해석)

  • Yoon, S.J.;Park, J.K.;Kim, Y.S.;Suh, C.H.;Lee, K.H.;Kim, R.Y.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2009.10a
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    • pp.181-184
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    • 2009
  • The hot press farming process, which is the press hardening of steel parts using cold dies, can utilize both ease of shaping and high strength due to the hardening effect of rapid quenching during the pressing. In this study, a thermo-elastoplastic analysis of the hot press forming process using the finite element method was performed in order to investigate the deformation behavior and temperature history during the process and the mechanical properties of the pressed parts.

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Fatigue Strength Evaluation of Adhesive Bonded and Mechanical Pressed Joints of Cold Rolled Steel Sheet (냉간압연강판 접착 및 기계적 프레스 접합부의 피로강도 평가)

  • Kim, Ho-Kyung
    • Journal of the Korean Society of Safety
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    • v.25 no.1
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    • pp.1-8
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    • 2010
  • The tensile and fatigue experiments were conducted with tensile-shear specimens for investigating the strength of adhesive bonded and mechanical press joints of SPCC steel sheet used in the field of the automobile industry. The optimal punch press force was evaluated 50kN for combining epoxy adhesive bonding and mechanical press joining with a diameter of 8.3mm using SPCC sheet with a thickness of 0.8mm. The combining epoxy adhesive bonding and mechanical press joining exhibits the maximum tensile force of 750N. The fatigue strengths of the combination of adhesive bond and mechanical press joint and pure adhesive joint were evaluated 370N and 320N at 106cycles, respectively. These values correspond to 22% and 20% of their maximum tensile forces, respectively. However, the fatigue strength of the combination of adhesive bond and mechanical press joining was much lower than that of pure mechanical press joining.

Phase Transformation and Mechanical Properties on Sintering Temperature of $\alpha$-SiC Manufactured by Pressureless Sintering ($\beta$-SiC의 상압소결시 소결온도에 따른 상전이와 기계적 특성 변화)

  • Ju, Jin-Young;Shin, Yong-Deok
    • Proceedings of the KIEE Conference
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    • 2001.07c
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    • pp.1433-1435
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    • 2001
  • The mechanical and phase transformation of the cold isostatically pressed $\beta$-SiC ceramic were investigated as a function of the sintering temperature. The result of phase analysis revealed 6H, 4H, 3C and phase transformation between 3C and 4H showed over 2000$^{\circ}C$ and the $\beta$ ${\rightarrow}$ $\alpha$ phase transformation was in saturation at 2200$^{\circ}C$. The relative density and the mechanical properties of $\alpha$-SiC ceramic was increased with increased sintering temperature. The flexural strength showed the highest value of 230 MPa at 2200$^{\circ}C$. This reason is because crack was propagated through surface flaw. The fracture toughness showed the highest value of 4.2 $MPa{\cdot}m^{1/2}$ at 2200$^{\circ}C$.

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Preparation of Cube-textured Nickel-alloy Tape using Metal Powders

  • Lee, Hee-Gyoun;Oh, Hyun-Suk;Hong, Gye-Won
    • Progress in Superconductivity
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    • v.1 no.2
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    • pp.120-124
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    • 2000
  • Ni-13%Cr and Ni-70%Cu alloy tapes were prepared by using high purity metal powders as starting materials. The Ni-13%Cr and the Ni-70%Cu mixtures were isostatically pressed, sintered, rolled and texture-annealed. SEM EDS analysis showed that copper and nickel atoms were completely mixed, while the alloying between the chromium powders and the nickel powders was incomplete. In spite of incomplete alloying between nickel and chromium powders, sharp cube-texture was developed for the Ni-13%Cr tape as well as the Ni-70%Cu tape.

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Fabrication Process and Mechanical Properties of High Volume Fraction SiC Particle Preform (고부피분율 SiC분말 예비성형체의 제조공정과 기계적특성)

  • 전경윤
    • Journal of Powder Materials
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    • v.7 no.1
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    • pp.27-34
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    • 2000
  • The fabrication process and mechanical properties of SiC particle prefrrms with high volume fraction ranged 50∼71% were investigated to make metal matrix composites for possible applications as heat sinks in electronic packares. The SiC particle preforms with 50∼71vol% of reinforcement were fabricated by a new modified process named ball milling and pressing method. The SiC particle performs were fabricated by ball milling of SiC particles with single sized of 48${\mu}$m in diameter or two different size of 8${\mu}$m and 48${\mu}$min diameter, with collodal SiO2 as inorgnic binder in distilled water, and the mixed slurries were cold pressed for consolidation into final prefom. The compressive strengths og calcined SiC particle prefoms increased from 20MPa to 155MPa with increasing the content of inorganis binder, temperature and time for calcination. The increase of compressive strength of SiC particle bridge the interfaces of two neighboring SiC particles.

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Effect of Repeated Quenching Heat Treatment on Microstructure and Dry Sliding Wear Behaviour of Low Carbon PM Steel

  • Gural, Ahmet;Tekeli, Suleyman;Ozyurek, Dursun;Guru, Metin
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.570-571
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    • 2006
  • The mixed atomized iron powders with 0.3% graphite and 1% Ni powders were cold pressed and sintered at $1200^{\circ}C$ for 30 min under pure Ar gas atmosphere. Some of the sintered specimens were intercritically annealed at $760^{\circ}C$ and quenched in water (single quenching). The other sintered specimens were first fully austenized at $890^{\circ}C$ and water quenched. These specimens were then intercritically annealed at $760^{\circ}C$ and re-quenched in water. The experimental results showed that the wear coefficient effectively decreased in the double quenched specimen.

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Pressureless Sintering and Microstructure of Pure Tungsten Powders Prepared by Ultrasonic Spray Pyrolysis (초음파 분무 열분해법으로 제조한 텅스텐 분말의 상압소결과 미세조직)

  • Heo, Youn Ji;Lee, Eui Seon;Oh, Sung-Tag;Byun, Jongmin
    • Journal of Powder Materials
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    • v.29 no.3
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    • pp.247-251
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    • 2022
  • This study demonstrates the effect of the compaction pressure on the microstructure and properties of pressureless-sintered W bodies. W powders are synthesized by ultrasonic spray pyrolysis and hydrogen reduction using ammonium metatungstate hydrate as a precursor. Microstructural investigation reveals that a spherical powder in the form of agglomerated nanosized W particles is successfully synthesized. The W powder synthesized by ultrasonic spray pyrolysis exhibits a relative density of approximately 94% regardless of the compaction pressure, whereas the commercial powder exhibits a relative density of 64% under the same sintering conditions. This change in the relative density of the sintered compact can be explained by the difference in the sizes of the raw powder and the densities of the compacted green body. The grain size increases as the compaction pressure increases, and the sintered compact uniaxially pressed to 50 MPa and then isostatically pressed to 300 MPa exhibits a size of 0.71 m. The Vickers hardness of the sintered W exhibits a high value of 4.7 GPa, mainly due to grain refinement.