• Title/Summary/Keyword: coating properties

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Properties of Sol-Gel Thin Films Containing Colloidal Silica and Alkoxysilanes (콜로이드 실리카 알콕시실란을 함유한 졸겔반응 경화박막 특성연구)

  • Myung, In-Hye;Ahn, Myeong-Sang;Kang, Young-Taec;Kang, Dong-Pil
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2006.06a
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    • pp.230-231
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    • 2006
  • We synthesized sol according to kinds(particle size/stabilized ion) of colloidal silica(CS), content ratio of alkoxysilane versus CS and reaction degree in sol solution and studied the surface property of coated gel materials. The contact angle of the thin films prepared from LHSA/N1030 CS/tetramethoxysilane(TMOS)/methyltrimethoxysilane(MTMS) sol-gel reaction system showed a little good relationship with content ratio of TMOS/MTMS silanes. The surface roughness of LHSA CS/TMOS/MTMS reaction system showed flatter than that of LHSA/N1030 CS. The thermal degradation of LHSA CS/TMOS/MTMS coating flim occurred at $550^{\circ}C$.

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Experimental Study on Spin Coated Thin Cover Layer for High Numerical Aperture Optical Disc

  • Dohoon Chang;Myongdo Ro;Duseop Yoon;Park, Insik;Dongho Shin;Kim, Jinhwan
    • Macromolecular Research
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    • v.9 no.6
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    • pp.313-318
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    • 2001
  • The present study relates to a method of manufacturing 100$\mu\textrm{m}$ thick cover layer for the high density digital versatile disc system (HD-DVD), which uses a high numerical aperture of 0.85 at 405 nm wavelength. Spin coating technique was investigated as means for manufacturing the cover layer within sufficient margins of thickness variation and with good mechanical properties including small radial and tangential tilts. The influence of processing variables such as spinning speed, spinning time, and dispensing position was investigated. The effect of viscosity of UV-curable resin was also investigated.

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Friction and wear properties of plasma-sprayed $Cr_2$$O_3$/$MoO_3$ composite coatings ($MoO_3$가 첨가된 $Cr_2$$O_3$ 플라스마 용사코팅의 마찰 마멸 특성)

  • 여인웅;안효석;임대순
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 2001.06a
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    • pp.22-29
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    • 2001
  • Plasma-sprayed coatings were prepared using by spray-dried Cr$_2$O$_3$ powder with and without MoO$_3$ addition. A reciprocal type tribe-tester was employed to examine friction and wear behavior of the specimens at room temperature. The worn surfaces of plasma spray coated specimens were observed by SEM. The results showed that friction coefficient of the MoO$_3$-added coatings were lower than those without MoO3 addition. However pure Cr$_2$O$_3$ coating showed the lowest wear loss at the self-mated test. The larger protecting layers were observed at the worn surface of plasma spray coated specimens with MoO$_3$ addition.

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Effect of Gradient Plasma Power on TiN, TiCN Coating Deposited by PECVD Process (PECVD법에 의한 TiN, TiCN 증착 시 gradient plasma power가 코팅층에 미치는 영향)

  • Kim, D.J.;Shin, C.H.;Hur, J.;Nam, T.W.
    • Journal of the Korean Society for Heat Treatment
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    • v.17 no.4
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    • pp.236-240
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    • 2004
  • Effect of plasma power on PECVD process were investigated in this study. TiN and TiCN films were deposited on nitrided STD11 steel with 600W, 1,200W and 1,600W plasma power. As the plasma power was increased, the preferred orientation was reinforced from (200) to (111) and the hardness of films was improved. The low plasma power was, however, effective for improving of adhesion force of films. Regarding above properties, TiN and TiCN films were deposited by gradient plasma power. It was possible to get high hardness as well as adhesion force through gradient plasma power.

Characteristics of Zn-Ni Electrodeposition of 60 kgf/$\textrm{mm}^2$ Grade Transformation Induced Plastic Steel Sheets for Automotive Body (60 kgf/$\textrm{mm}^2$급 자동차용 변태유기소성강화강 Zn-Ni 전기도금 특성 연구)

  • Kim D. H.;Kim B. I.;Jeon Y. T.;Jeong Y. S.
    • Journal of Surface Science and Engineering
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    • v.37 no.5
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    • pp.263-272
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    • 2004
  • High strength steels such as transformation induced plastic steel, dual phase and solid solution Hardening have been developed and continuously improved due to the intensified needs in the automotive industry. But silicon and manganese in transformation induced plastic steels were known to exhibit harmful effects on galvannealing reaction by oxide film formed during heat treatment. Therefore, in this work, the applicability of Zn-Ni electrodeposition instead of hot dip galvannealed coating to transformation induced plastic steels was evaluated and optimum electroplating condition was investigated. Based on these investigations optimized electroplating conditions were proposed and Zn-Ni electrogalvanized steel sheet was produced by EGL (electrogalvanized line). Its perfomance properties for automotive steel was evaluated.

Effect of Skinpassing Conditions on the Surface Characteristics of Hot-dip Galvanized Steel Sheets (용융아연도금강판의 표면특성에 미치는 조질압연 조업조건의 영향)

  • 전선호
    • Journal of Surface Science and Engineering
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    • v.34 no.4
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    • pp.327-336
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    • 2001
  • The skinpassing conditions such as roll type, roll force and roll roughness of the work roll were evaluated to give the surface properties of the galvanized steel sheets that were required for automotive and to get rid of the surface defects that caused with the bad control of galvanized coating process parameters. The surface defects of the galvanized steel sheets such as the ripple mark and the scratch were completely removed as the roll force of SPM work roll was increased and the amount of the transfer of roll surface texture to the strip was also gained a lot. The image clarity of electro discharge textured (EDT) coated steel sheets before and after painting was higher than that of the bright (BRT) and shot blasted (SBT) coated steel sheets because of higher PPI value, lower waviness and uniform surface pattern. Since micro-craters transferred on the surface of the galvanized steel sheets played a role of nucleation sites of chromate reaction, Increase of micro-craters was bring to better corrosion resistance with the increase of the roll force and the use of EDT roll at the skin pass mill.

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A Study of Structure & Composition Characteristics of the(Ti, Al) N Coating on the STS 304 by D.C. Magnetron Sputtering (D.C. Magnetron Sputter를 이용한 (Ti, Al) N 피막의 조성 및 조직특성연구)

  • 최장현;이상래
    • Journal of Surface Science and Engineering
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    • v.25 no.5
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    • pp.223-233
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    • 1992
  • (Ti, Al)N films were deposited on 304 stainless steel by D.C. magnetron sputtering using Al target and Ti plate. The properties of (Ti, Al)N films such as composition, microhardness, grain size, crystal structure were investigated. The chemical composition of (Ti, Al)N films was similar to the sputter area ratio of titanium to aluminum target by means of EDS and AES survey. The higher bias voltage to substrate and the smaller input of N2 gas showedthe increased microhardness and the finer grain size of the films. The results obtained from this study show, it is belived, that the (Ti, Al)N film by D.C.magne-tron sputtering is promising in the wear resistance use.

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Synthesis and mechanical properties of $CrAlC_xN_{1-x}$ coatings by a hybrid coating system (하이브리드 코팅 시스템을 이용한 $CrAlC_xN_{1-x}$ 코팅의 합성과 기계적 특성)

  • Choi, Ji-Hwan;Hong, Yeong-Su;Kim, Kwang-Ho
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2009.10a
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    • pp.200-200
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    • 2009
  • 아크이온플래이팅 기술과 DC 마그네트론 스퍼터링 기술이 결합된 하이브리드 코팅 시스템을 이용하여 STS 304와 Si 기판에 4성분계 CrAlCxN1-x 코팅을 증착하였다. 합성된 CrAlCxN1-x 코팅은 주로 유도결합형로 f구성되었다. CrAlCxN1-x 코팅의 carbon 함량이 0.17 at.%일 때 약 34 GPa을 나타내었으며 마찰계수는 carbon 함량이 0에서 1 at.%로 증가함에 따라 0.82에서 0.38까지 크게 감소하였다. 이는 코팅 표면과 steel 볼 사이에 amorphous carbon layer가 형성되어 고체윤활제로 작용한 것으로 사료된다.

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Syntheses and mechanical properties of Cr-Mo-Si-N coatings by a hybrid coating system (하이브리드 코팅시스템을 이용한 Cr-Mo-Si-N 코팅의 합성 및 기계적 특성)

  • Yun, Ji-Hwan;An, Seong-Gyu;Lee, Ju-Hui;Kim, Gwang-Ho
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2007.04a
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    • pp.103-104
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    • 2007
  • Cr-Mo-Si-N 코팅막은 AISI D2 모재와 Si 모재위에 $Ar/N_2$ 혼합기체를 사용하여 AIP (arc ion plating) 방법과 마그네트론 스퍼터링 (DC magnetron sputtering) 방법을 결합시킨 하이브리드 코팅시스템을 이용하여, 증착하였다. XRD, HRTEM, XPS 등의 분석장비를 이용하여 Cr-Mo-Si-N 코팅의 미세구조를 관찰하였다. Cr-Mo-Si-N 코팅의 경도는 Si함량이 12.1 at.%에서 약 50 GPa의 최고치를 나타냈으며, 평균 마찰계수는 Si 함량이 증가할수록 감소하였다.

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Effect of the atmospheric plasma etching preprocessing on properties of silica coating (대기압플라즈마 에칭 전처리 공정이 실리카 코팅의 특성에 미치는 영향)

  • O, Seung-Cheon;Sin, Jung-Uk;Kim, Sang-Sik
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2012.05a
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    • pp.200-200
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    • 2012
  • 대기압 플라즈마 에칭 전처리 공정이 실리카 코팅의 특성에 미치는 영향을 연구하였다. 접촉각 특성, aging 효과, 광투과도 변화를 분석 하였다. 대기압 플라즈마 에칭 전처리를 통해 실리카 코팅의 특성은 접촉각 $13^{\circ}$에서 $6^{\circ}$로 변하였으며 aging 시험 결과 에칭 전 $6^{\circ}$ 증가에서 에칭 후 $2^{\circ}$로 친수특성 유지도가 향상되었다. 광 투과도는 89.8 %에서 90.67% 로 0.61 % 향상되었다.

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