• Title/Summary/Keyword: coating method

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Preparation of Hard Coating Films with High Refractive Index from Titania Nanoparticles (이산화티탄 나노입자로부터 고굴절 하드코팅 도막의 제조)

  • Kim, Nam Woo;Ahn, Chi Yong;Song, Ki Chang
    • Korean Chemical Engineering Research
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    • v.53 no.6
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    • pp.762-769
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    • 2015
  • The titania ($TiO_2$) nanoparticles with a diameter 2?3 nm were synthesized by controlling hydrolysis of titanium tetraisopropoxide (TTIP) in acid solution. Organic-inorganic hybrid coating solutions were prepared by reacting the titania nanoparticles with 3-glycidoxypropyl trimethoxysilane (GPTMS) by the sol-gel method. The hard coating films with high refractive index were obtained by curing thermally at $120^{\circ}C$ after spin-coating the coating solutions on the polycarbonate (PC) sheets. The coating films showed high optical transparency of 90% in the visible range and exhibited a pencil hardness of 2H. Also, the refractive index at 633 nm wavelength of coating films enhanced from 1.502 to 1.584 as the weight content of titania nanoparticles in the coating solutions increased from 4% to 25%.

MECHANICAL PROPERTIES OF TIN COATED FILM WITH VARIOUS COATING THICKNESS ON TITANIUM ALLOY (타이타늄 합금에 다양한 두께로 코팅된 TiN 피막의 기계적 성질)

  • Lee, Jae-Yun;Oh, Dong-Joon;Kim, Hee-Jung;Chung, Chae-Heon
    • The Journal of Korean Academy of Prosthodontics
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    • v.45 no.5
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    • pp.675-686
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    • 2007
  • Statement of problem: Titanium nitride(TiN) coatings are the most general and popular coating method and used to improve the properties of metallic surface for industrial purposes. When TiN coating applied to the abutment screw, frictional resistance would be reduced, as a results, the greater preload and prevention of the screw loosening could be expected. Purpose: The purpose of this study was to investigate mechanical properties of TiN coated film of various coating thickness on the titanium alloy surface and to evaluate proper coating thickness. Material and method: 95 Titanium alloy (Ti-6Al-4V) discs of 15 mm in diameter and 3 mm in thickness were prepared for TiN coating and divided into 7 groups in this study. Acceding to coating deposition time (CDT) with TiN by using Arc ion plating, were divided into 7 groups : Group A (CDT 30min), Group B (CDT 60min), Group C (CDT 90min), Group D (CDT 120min), Group E (CDT 150min), Group F(CDT 180min) and Group G (no CDT) as a control group. TiN coating surface was observed with Atomic Force Microscope(AFM), field emission scanning electron microscopy(FE-SEM) and examined with scratch tester, wear tester. Result: 1. Coating thickness fir each coated group was increased in proportion to coating deposition time. 2. Surface of all coated groups except Group A was homogeneous and smooth. However, surface of none coated Group G had scratch. 3. Adhesion strength for each coated group was increased in proportion to coating deposition time. 4. Wear resistance for each coated group was increased in proportion to coating deposition time. 5. Surface roughness in Group A, B, C was increased in proportion to coating deposition time. But, surface roughness in Group D, E, F was showed decreased tendency in proportion to coating deposition time. Conclusion: According to coating deposition time, mechanical properties of TiN coated film were changed. It was considered that 120 minutes coating deposition time ($1.32{\mu}m$ in coating thickness) is necessary.

Effect of Different Seed Coating Materials on Seedling Establishment and Growth in Direct Seeded Rice under Puddled Wet Soil Condition (벼 무논직파재배의 종자 코팅소재별 발아 및 유묘생육 특성)

  • Park, K.H;Kim, Y.S.;Chang, J.T.
    • Journal of Practical Agriculture & Fisheries Research
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    • v.15 no.1
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    • pp.63-73
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    • 2013
  • The research was conducted to determine a seed germination and seedling establishment of rice plant under seed coating materials such as iron, silicate, and phyllite and under covered with silicate and iron coated & silicate covered in the puddled wet hill seeding and wet line seeding methods. The seedling establishment was high in silicate and untreated control of 100%>phyllite coating of 91.5%>silicate coating of 88%>iron coating and silicate covered of 86%>silicate covered of 75.5% in the puddled wet hill seeding method, respectively. At 35days after treatment there was high in seedling height at silicate covered of 23.8cm>control of 23.6cm>silicate coating of 21.4cm>phyllite coating of 20.2cm>iron coating and silicate covered of 16.8cm>iron coating of 15.4cm. In puddle wet line seeding method rice seedling establishment was high at control and silicate covered of 100%>iron coating and silicate covered by 97.5%>phyllite coating by 94.8%>iron coating by 86%. Seedling height was high in silicate covered of 22.1cm>control of 21.2cm>silicate coating of 20.0cm>phyllite coating of 19.0cm>iron coating of 17.7cm>iron coating and silicate covered of 17.0cm, respectively.

Lubrication of Space Systems by Tribo-coating

  • Kato, Koji
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 2002.10b
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    • pp.7-8
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    • 2002
  • It is a time to introduce a concept of lubrication to space systems. Minimum amount of lubricant should be supplied to a contact interface instead of preparing too much lubricant on surfaces of the earth. In situ controllable lubrication method is wanted to overcome unexpected tribo-troubles in space. Tribo-coating, which forms a thin solid film in nm-scale by vacuum deposition during friction, is a promising lubrication method for space.

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Treatment Results of Intracranial Aneurysms by Wrapping and Coating (포장술을 시행한 뇌동맥류의 치료 성적)

  • Kwon, Taek Hyun;Chung, Hung Seob;Park, Youn Kwan;Cho, Tai Hyoung;Lim, Dong Jun;Park, Jung Yul;Chung, Yong Gu;Lee, Hoon Kap;Lee, Ki Chan;Suh, Jung Keun
    • Journal of Korean Neurosurgical Society
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    • v.30 no.7
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    • pp.891-895
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    • 2001
  • Objective : Although surgical clipping of intracranial aneurysm is the definite method of treatment, there remains a small number of patients in whom surgical clipping is not technically possible. In such difficult cases, surgeon has to consider other therapeutic alternatives. In this report, we analyze our aneurysmal cases treated by wrapping and coating method and evaluate their surgical outcome and follow-up results. Method : Among the total of 877 patients operated from 1990 to 1999 for intracranial aneurysms at our hospital, 40 cases(4.6%) were treated by wrapping and coating method. They included 24 cases of single ruptured aneurysms and 16 with unruptured ones in multiple aneurysms. Wrapping with temporalis muscle and/or muslin gauze and coating with bioadhesive agent such as fibrin glue were performed. Result : Wrapping and coating method was performed mostly to the anterior communicating artery aneurysm (35%), and mostly because of the broad-based neck of an aneurysm(43%). At the time of discharge, 30 out of 40 patients(80%) showed favourable outcome and three cases died. The patients were monitored for average of 37 months(3-75 months). Among 24 cases with single ruptured aneurysm, 4 cases(17%) had early rebleeding within 6 months from the initial hemorrhage, and such rebleeding occurred within the first postoperative month in 3 cases. However, there was no rebleeding after the 6 months. Among 16 patients whose aneurysms were unruptured ones, none of them showed bleeding episode. Conclusion : It seems likely that the wrapping and coating method would be some help to prevent the rebleeding of an intracranial aneurysm. In order to obtain more accurate results regarding the efficacy of such method, it will be necessary to perform a multi-center study for longer follow-up periods and various wrapping and coating materials.

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Emission Properties of Electro luminescent Devices using Poly(3-hexylthiophene) Deposited by LB Method (LB법으로 첨가한 Poly(3-hexylthiophene)을 발광층으로 사용한 전계발광소자의 발광특성)

  • 김주승;이경섭;구할본
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.14 no.9
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    • pp.757-761
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    • 2001
  • We studied emitting properties of organic electroluminescent devices fabricated using the spin-coating and Langmuir-Blodgett(LB) technique. The LB technique has the advantage of precise control of the thickness better than spin-coating method. LB monolayer of poly(3-hexylthiophene)(P3HT) was deposited 27 layers onto the indium-tin-oxide(ITO) substrate as Y-type films by the vertical dipping method. In the absorption spectra, the λ$\_$max/ of P3HT-AA LB films and of spin-coating films showed about at 510, 545 and 590 nm corresponding to 2.43, 2.28, 2.10eV. And we observed that the turn-on voltage of devices deposited by LB method(10V) was higher than that of spin-coating method(8.5V) in voltage-current-luminance characteristic. In the logV-logJ characteristics of ITO/P3HT-AA LB/Al device, we confirmed that El device fabricated by LB method follows three conduction mechanisms: ohmic, space-charge-limited current(SCLC) conduction and trapped-carrier-limited space-charge current(TCLC) conduction.

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A Study on Hydrophobic Surface Treatment for Microfluidic System Fabrication Based on SLA 3D Printing Method (SLA 3D 프린팅 방식 기반의 미세 유체 시스템 제작을 위한 소수성 표면 처리 연구)

  • Jae Uk Heo;Seo Jun Bae;Do Jin Im
    • Korean Chemical Engineering Research
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    • v.62 no.1
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    • pp.105-111
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    • 2024
  • The SLA (Stereolithography Apparatus) method is a type of 3D printing technique predicated on the transformation of liquid photocurable resin into a solid form through UV laser exposure, and its application is increasing in various fields. In this study, we conducted research to enhance the hydrophobicity and transparency of SLA 3D printing surfaces for microfluidic system production. The enhancement of surface hydrophobicity in SLA outputs was attainable through the application of hydrophobic coating methods, but the coating durability under different conditions varied depending on the type of hydrophobic coating. Additionally, to simultaneously achieve the required transparency and hydrophobic properties for the fabrication of microfluidic systems, we applied hydrophobic coatings to the proposed transparency enhancement method from prior research and compared the changes in contact angles. Teflon coating was proposed as a suitable hydrophobic coating method for the fabrication of microfluidic systems, given its excellent transparency and high coating durability in various environmental conditions, in comparison to titanium dioxide coating. Finally, we produced an Electrophoresis of Charged Droplet (ECD) chip, one of the digital microfluidics systems, using SLA 3D printing with the proposed Teflon coating method (Fluoropel 800). Droplet manipulation was successfully demonstrated with the fabricated chip, confirming the potential application of SLA 3D printing technology in the production of microfluidic systems.

Fabrication of Carbon Fiber Reinforced Reaction Bonded SiC Composite Fabricated by a Molten Si Infiltration Method; I. The Effect of Carbon Fiber Coating Process (용융 Si 침윤법에 의해 제조된 반응소결 탄소 섬유강화 탄화규소 복합체 제조; I. 탄소 섬유 코팅 방법에 따른 영향)

  • Yun, Sung-Ho;Tan, Phung Nhut;Cho, Gyung-Sun;Cheong, Hun;Kim, Young-Do;Park, Sang-Whang
    • Journal of the Korean Ceramic Society
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    • v.45 no.9
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    • pp.531-536
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    • 2008
  • Reaction bonded silicon carbide (RBSC) composite for heat-exchanger was fabricated by molten Si infiltration method. For enforcing fracture toughness to reaction bonded silicon carbide composite, the surface of carbon fiber has coating layer by SiC or pyro-carbon. For SiC layer coating, CVD method was used. And for carbon layer coating, the phenol resin was used. In the case of carbon layer coating, fracture toughness and fracture strength were enhancing to 4.4 $MPa{\cdot}m^{1/2}$ and 279 MPa.

Analysis on Enameled Container with Different Coating Thicknesses of Enamel in Pyrolysis Process (법랑공정에서 Enamel 도포두께에 따른 강판 용기의 변형 메커니즘 분석)

  • Park, Sang-Hu;Kang, Dong-Suk;Yu, Jae-Hyun
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.19 no.5
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    • pp.67-74
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    • 2020
  • To predict the thermal deformation of an oven cabinet during the enamel process, we propose a simple finite element analysis method comprising two steps: heating and cooling. To this end, the basic mechanical and thermal properties such as thermal expansion of the enamel and steel plate were experimentally studied, and the mechanical properties of four different stainless steel (SUS) plates were evaluated to select the target material for the oven at high temperature conditions from 400 ℃ to 700 ℃. In the first analysis step of the enamel process, the SUS plate was heated to 850 ℃ and was then thermally expanded without considering the enamel coating. Next, assuming the perfect bonding of two materials (enamel coating and metal plate), the enamel plate was allowed to cool to room temperature till 22 ℃. From the results of comparing the experimental and analytical data, we can make a conclusion that the proposed method can be applied to evaluate the thermal deformation of enamel products. Especially, the thermal deformation of the oven can be predicted with different enamel coating conditions, such as uniform and nonuniform coating thickness.