• Title/Summary/Keyword: coated powder

Search Result 588, Processing Time 0.031 seconds

Thermally Stabilized Porous Nickel Support of Palladium Based Alloy Membrane for High Temperature Hydrogen Separation

  • Ryi, Shin-Kun;Park, Jong-Soo;Cho, Sung-Ho;Hwang, Kyong-Ran;Kim, Sung-Hyun
    • Corrosion Science and Technology
    • /
    • v.6 no.3
    • /
    • pp.133-139
    • /
    • 2007
  • Nickel powder was coated with aluminum nitrate solution to increase the thermal stability of a porous nickel support and control the nickel content in the Pd-Cu-Ni ternary alloyed membrane. Raw nickel powder and alumina coated nickel powder were uniaxialy pressed by home made press with metal cylindrical mold. Though the used nickel powder prepared by pulsed wire evaporation (PWE) method has a good thermal stability, the porous nickel support was too much sintered and the pores of porous nickel support was plugged at high temperature (over $800^{\circ}C$) making it not suitable for the porous support of a palladium based composite membrane. In order to overcome this problem, the nickel powder was coated by alumina and alumina modified porous nickel support resists up to $1000^{\circ}C$ without pore destruction. Furthermore, the compositions of Pd-Cu-Ni ternary alloy membrane prepared by magnetron sputtering and Cu-reflow could be controlled by not only Cu-reflow temperature but also alumina coating amount. SEM analysis and mercury porosimeter analysis evidenced that the alumina coated on the surface of nickel powder interrupted nickel sintering.

Characteristics of BGsome-Coated Illite as a Face Powder (BGsome이 코팅된 일라이트 및 이를 함유한 페이스 파우더의 특성)

  • Lim, Jin Kyong;Jin, Byung Suk
    • Applied Chemistry for Engineering
    • /
    • v.24 no.2
    • /
    • pp.126-131
    • /
    • 2013
  • BGsome coating on the surface of illite powder was attempted to impart skin affinity and improve various characteristics of the powder for makeup cosmetics. BGsome is a type of hydrated liquid crystalline vesicles prepared by the hydration of 1,3-butylene glycol (BG) dissolved lecithin. BGsome droplets were coated through wet process and the coated powders were analyzed by TGA, SEM, and particle size measurements. Effect of BGsome coating on the physical properties, such as flow-ability, dispersibility, spreadability, and adhesion, were examined. The repose angle of BGsome-coated illite was decreased, which means that BGsome coating improves the flowability of the powder. Dispersibility, spreadability, and adhesion of the coated illite were also improved remarkably. The result of adhesion tests showed that the BGsome-coated illite was evenly adhered onto artificial leather surface with almost no lumps. The flowability, dispersibility, spreadability and adhesion of face powders containing the BGsome-coated illite were also improved.

Non-electrolytic Deposition of Silver on Tungsten Powders for Functionally Gradient Composite Powder

  • Lee, Jae-Ho;Change, Gun-Ho
    • Proceedings of the Korean Powder Metallurgy Institute Conference
    • /
    • 2006.09b
    • /
    • pp.1225-1226
    • /
    • 2006
  • Particles of high strength material when coated with silver offer a means of obtaining desirable electrical properties and high strength. The coating process employed aqueous ammoniacal silver-nitrate electrolytes with a formaldehyde solution as the reductant. Modifying additives were also applied. The reduction and subsequent deposition of silver occurred selectively on the surface of the tungsten particles. The morphologies of the coated particles were assessed by SEM imaging. The silver was uniformed coated on tungsten powder and its thickness was estimated to be approximately 100nm on the basis of a mass account.

  • PDF

High Temperature Oxidation Behavior of Plasma-sprayed Ti(Al,O)/$Al_2O_3$ Coatings on SS41 Steel (Ti(Al,O)/$Al_2O_3$ 플라즈마 코팅한 SS41의 고온산화 거동)

  • Choi, G.S.;Woo, K.D.;Lee, H.B.;Jeon, J.Y.
    • Journal of the Korean Society for Heat Treatment
    • /
    • v.20 no.5
    • /
    • pp.231-236
    • /
    • 2007
  • High velocity oxy-fuel (HVOF) spraying was used to coat Ti(Al,O)/$Al_2O_3$ powder onto the SS41 steel plate. Macrostructure of the coated specimen has been investigated by scanning electron micrograph (SEM). High temperature oxidation behavior of the coated specimen and SS41 steel have been studied. From the results of SEM observation, Ti(Al,O)/$Al_2O_3$ powder was coated well onto the substrate SS41 steel. Porosity onto the coated layer was only 0.38%. The oxidation results showed that Ti(Al,O)/$Al_2O_3$ powder coated SS41 steel have improved little oxidation resistance at $900^{\circ}C$ in air, but improved remarkably oxidation resistance at $800^{\circ}C $ in air compare to the substrate SS41 steel.

Fabrication of Cu-30 vol% SiC Composites by Pressureless Sintering of Polycarbosilane Coated SiC and Cu Powder Mixtures (Polycarbosilane이 코팅된 SiC와 Cu 혼합분말의 상압소결에 의한 Cu-30 vol% SiC 복합재료의 제조)

  • Kim, Yeon Su;Kwon, Na-Yeon;Jeong, Young-Keun;Oh, Sung-Tag
    • Korean Journal of Materials Research
    • /
    • v.26 no.6
    • /
    • pp.337-341
    • /
    • 2016
  • Cu-30 vol% SiC composites with relatively densified microstructure and a sound interface between the Cu and SiC phases were obtained by pressureless sintering of PCS-coated SiC and Cu powders. The coated SiC powders were prepared by thermal curing and pyrolysis of PCS. Thermal curing at $200^{\circ}C$ was performed to fabricate infusible materials prior to pyrolysis. The cured powders were heated treated up to $1600^{\circ}C$ for the pyrolysis process and for the formation of SiC crystals on the surface of the SiC powders. XRD analysis revealed that the main peaks corresponded to the ${\alpha}$-SiC phase; peaks for ${\beta}$-SiC were newly appeared. The formation of ${\beta}$-SiC is explained by the transformation of thermally-cured PCS on the surface of the initial ${\alpha}$-SiC powders. Using powder mixtures of coated SiC powder, hydrogen-reduced Cu-nitrate, and elemental Cu powders, Cu-SiC composites were fabricated by pressureless sintering at $1000^{\circ}C$. Microstructural observation for the sintered composites showed that the powder mixture of PCS-coated SiC and Cu exhibited a relatively dense and homogeneous microstructure. Conversely, large pores and separated interfaces between Cu and SiC were observed in the sintered composite using uncoated SiC powders. These results suggest that Cu-SiC composites with sound microstructure can be prepared using a PCS coated SiC powder mixture.

Fabrication and Thermophysical Properties of Nickel-coated Aluminum Powder by Electroless Plating (비전해 방법을 이용한 니켈 코팅 알루미늄 분말 제조 및 열물성 평가)

  • Lee, Sanghyup;Lim, Jihwan;Noh, Kwanyoung;Yoon, Woongsup
    • Journal of the Korean Society of Propulsion Engineers
    • /
    • v.18 no.4
    • /
    • pp.9-17
    • /
    • 2014
  • In this study, in order to improve the ignitability of high energy aluminum powder, natural oxide films (alumina) were chemically removed, and instead nickel coat was applied. We used an electroless plating for nickel coating and confirmed quantitatively and qualitatively a time-dependent degree of nickel coating through analysis of surface by SEM/EDS. We also conducted element analysis by XRD and thermal properties by TGA/DSC in air oxidizer environment. There results explained the ignition enhancement mechanism of the nickel-coated aluminum powder in air. The difference between coated and un-coated aluminum powder, the effectiveness of coated powder has better ignitability.

Effect of Reductants and their Properties of Electric Resistivity on the Preparation of Ag coated Cu Powders by Chemical Reduction Method (화학환원법을 이용한 은 코팅 구리 분말 제조 시 환원제의 영향 및 전기비저항 특성)

  • Ahn, Jong-Gwan;Yoon, Chi-Ho;Kim, Dong-Jin;Cho, Sung-Wook;Park, Je-Shin
    • Korean Journal of Metals and Materials
    • /
    • v.48 no.12
    • /
    • pp.1097-1102
    • /
    • 2010
  • Silver coated copper powders were prepared by a chemical reduction method with controlling the deposition process variables such as the feeding rate of the silver ionic solution and concentration of the reductants at room temperature. The characteristics of the products were evaluated by scanning electron microscope (SEM), X-ray diffractometer (XRD), atomic absorption spectrophotometer (AA) and a 4 probe resistivity measurement system. The optimum condition of the preparation of Ag coated Cu powders was at 0.05 M of potassium sodium tartrate and 2 ml/min of the feeding rate of the silver ionic solution. Our method successfully produced dense, uniform, and well-dispersed Ag coated Cu powder of $2{\sim}2.5{\mu}m$ witha silver layer of 100~200 nm. Additionally, we found that thespecific resistivity of the 30 wt.% Ag coated Cu powder was similar to that of pure silver, so that the composite powder could be used as an alternative electromagnetic shielding material for silver.

Electromagnetic Properties of Siver Coated Iron based Alloy Powders Prepared by Chemical Reduction Method

  • Lee, Byoung-Yoon;Lee, Jae-Wook;Yun, Yeo-Chun;Jeong, In-Bum;Moon, Joo-Ho
    • Proceedings of the Korean Powder Metallurgy Institute Conference
    • /
    • 2006.09b
    • /
    • pp.1213-1214
    • /
    • 2006
  • The synthesis of silver coated iron base alloy (Sendust : Fe-Si-Al) powder having the both effects of shielding and suppressing of electromagnetic wave was studied. Depending on thickness of silver coating layer, the electromagnetic properties of the dispersed particles complexed with organic binder were examined. It is proposed that the silver coated sendust flake powders with controlled electrical properties and thickness can be used as thin microwave absorbers in quasi-microwave frequency band.

  • PDF

Synthesis of WS$_2$ Solid Lubricant and Its Application to the Ball Bearing (WS$_2$ 고체윤활제의 합성 및 구름베어링 적용)

  • 신동우;윤대현;최인혁;김경도
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
    • /
    • 1998.04a
    • /
    • pp.173-179
    • /
    • 1998
  • The processing conditions for the synthesis of platelet WS$_2$ lubricant powder through the solid-gas reaction were optimized. The tungsten and sulfur powders were sealed in a vacuum of 10$^{-6}$ torr, prior to heat-treating at 850$\circ$C for 8 days. The react~on product showed the well-developed platelet WS$_2$ powder with an average size of 3.8 $\mu$m. The synthesized WS$_2$ powder was coated on the commercial deep grooved ball bearing (No. 6203) to examine the effects of WS$_2$ coating layer on the noise and endurance of the ball bearing. The level of noise obtained from WS$_2$ coated-ball bearing was higher (56 dB) than the value occurred in the case of greece (37 dB). The life-time of the ball-bearing assembled after coating WS$_2$ powder increased 50 times compared to the non-coated bali-bearing.

  • PDF

The Shielding Effectiveness of Zn-Al Arc Thermal Metal Film Coated Cement-Mortar Using Copper Powder (Zn-Al 아크 금속용사 피막을 적용한 구리분말 혼입 시멘트 모르타르의 전자파 차폐 성능 평가)

  • Choi, Hyun-Jun;Choi, Hyun-Kuk;Kim, Hyeong-Cheol;Lee, Han-Seung
    • Proceedings of the Korean Institute of Building Construction Conference
    • /
    • 2017.05a
    • /
    • pp.124-125
    • /
    • 2017
  • In this study, the shielding effectiveness of the Zn-Al arc thermal metal film coated cement-mortar mixed with copper powder by reflection, absorption, multi-reflection loss in 2.25~2.65 GHz was reviewed. By enhancing the mixing ratio of copper powder, the shielding effectiveness by absorption and multi-reflection loss was increased, but shielding rate(%) based on 80 dB showed below 20%. The Zn-Al arc thermal metal film coated on specimen, the shielding rate increased 3.5 times by reflection loss.

  • PDF