• Title/Summary/Keyword: chemical testing

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Development of Welding Quality Monitoring Method for TIG Cladding (TIG클래딩 공정에 대한 품질 모니터링기법의 개발)

  • Cho, Sang Myung;Son, Min Su;Park, Jung Hyun
    • Journal of Welding and Joining
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    • v.31 no.6
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    • pp.90-95
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    • 2013
  • Pipe inside clad welding is mainly used to the flow pipe of sub-sea or chemical plant. For the inside clad welding to the medium pipe with the diameter of about 12", TIG welding is frequently applied with filler metal. In this case, the clad welding has the very broad weld area over $10m^2$. And, the non-destructive test (NDT) such as ultrasonic test (UT) or radiographic testing (RT) should be conducted on the broad weld area, and it costs very high due to the time-consuming work. Therefore, the present study investigated the variation of arc voltage to develop the in-line quality monitoring system for the pipe inside TIG cladding. The 4 experimental parameters (current, arc length, wire feed position, and shield gas flow rate) varied to observe the change of arc voltage and to establish the model for the monitoring. The arc voltage was decreased when the wire was fed to the backward eccentric position(over 2mm), and the shield gas flow rate was insufficient under 10L/min. In the case of the backward eccentric position over 2mm, the bead appearance was not good and the dilution ratio was increased due to deep penetration. When the shield gas flow rate was lower than 10L/min, the bead surface was oxidized.

Studies on Situation and Utilization of Domestic Colostrum (국내산 초유의 현황과 이용에 관한 연구)

  • Bae, Hyung-Churl;Renchinthand, Gereltuya;Na, Seuk-Han;Choi, Seong-Hyun;Nam, Myoung-Soo
    • Food Science of Animal Resources
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    • v.27 no.4
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    • pp.517-521
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    • 2007
  • Questionnaire on utilization of colostrum was carried out in 33 farms. Highest milking cow numbers were 20-40 heads in 45.5% of the farms. Calf numbers were 20-40 heads in 39.4% of the dairy farms and 40-60 heads in 42.4% of the farms. The amount of colostrum production per day was 20-30 kg in 30.3% of the farms and 30-40 kg in 30.3% of the farms. Colostrum intake per calf per day was 4 kg in 45.5% farms. Surplus colostrum after intake by calf was farms (85%) was wasted in 67% of the farms. More than 90% of dairy farms recognize an necessity to use surplus colostrum. Selling price of surplus colostrum was below 1,000 won per kg at 15 dairy farms and 1,000-2,000 won per kg at 4 dairy farms. Colostrum collection and use should be done by the dairy farms of antibiotics free. Quality control of colostrum should be done by testing antibiotics, microbacterium, chemical composition, somatic cells and etc. The colostrum is subjected to cool down below $4^{\circ}C$ just after milking and process for the colostrum products.

A feasibility study on Introducing Reference Fuel(Diesel) for Testing Vehicles in South Korea (국내 차량 인증시험용 표준연료(경유) 도입 필요성 검토 연구)

  • Hwang, Inha;Kang, Hyungkyu;Seong, Sangrae;Song, Hoyoung;Ha, Jonghan;Na, Byungki
    • Journal of the Korean Applied Science and Technology
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    • v.34 no.4
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    • pp.974-985
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    • 2017
  • Although the number of registered cars in South Korea is about 22million but, there is no national standard for automobile reference fuel in South Korea. Reference fuel is the fuel used for certificating vehicle performance, emissions and fuel economy. Now, domestic market fuels are used as reference fuel. However, the quality of domestic market fuel is constantly changing by seasonal and fuel manufacturers. It may effect vehicle performance, emissions and fuel efficiency test result. On this study, market diesel fuel quality was monitored and reference fuel standard(draft) was set by reflecting market fuel monitoring result. Reference fuel standard(draft) was applied to CRDI engine.

Gas Permeation Study of Fuel Hose Composed as Inner Material of FKM Rubber (FKM 고무를 내층재료로 한 연료호스의 가스 투과성 연구)

  • Kim, Do-Hyun;Doh, Kyung-Hwan;Park, Hyun-Ho;Lee, Chang-Seop
    • Elastomers and Composites
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    • v.40 no.2
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    • pp.83-92
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    • 2005
  • To develop an automotive fuel hose suitable to the international environmental regulation, FKM rubber materials as an inner material of fuel hole were prepared with different chemical compositions. Measurement of the properties of thermal resistance, oil resistance, fuel resistance, gas permeability including fundamental properties were performed to investigate compatibility for a fuel hose material. Fundamental properties, thermal resistance, oil resistance, fuel resistance and permeability of FKM rubber materials were improved with fluorine content. When the carbon content was 20 phr, FKM compounds with fluorine contents of 66%, 09% and 71% were shown to satisfy the specification oi fuel hose. The gas permeability of NBR and FKM compounds was measured on the mixed fuel oils prepared with isooctane-toluene and gasoline-methanol. FKM rubber materials showed a small difference in penetrated amount of fuel and showed a permeability superior to NBR material. he permeability of FKM rubber materials was not influenced by the contents of fuel oil. Thermal properties of 69% FKM rubber experienced by permeability testing were not variated.

Effect of Customized Fertilizer Application and Soil Properties on Amino Acids Composition in Rice Grain

  • Sung, Jwakyung;Lee, Yejin;Chun, Hyenjung;Ha, Sangkeun;Sonn, Yeonkyu;Lee, Jongsik
    • Korean Journal of Soil Science and Fertilizer
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    • v.48 no.5
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    • pp.464-468
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    • 2015
  • Our government has performed to support the nation-wide application of customized fertilizer based on soil-testing results and crop nutrient balance in order to promote the environment-friendly agriculture and to respond the global environment guide-line since 2010. This study was performed at the selected local paddy fields (Hwaseong-si, Uiseong-gun and Miryang-si) with different soil chemical properties in 2012. The contents of amino acids measured showed an increasing trend with fertilization, and glutamic acid was the most abundant amino acid followed by aspartic acid, leucine and alanine. However, valine, isoleusine, tyrosine and lysine were not significantly affected by fertilization. The significant differences in grain N, expressed as a crude protein, and amino acids dose was observed between experimental sites (p<0.001), treatments (p<0.01 to 0.001) and interaction of both factors (p<0.01 to 0.001). In our experiment the following order of carbon skeleton backbones to produce amino acids was observed irrespective of experiment sites and fertilization: ${\alpha}$-ketoglutarate > oxalate > pyruvate > 3-phosphoglycerate > phosphoenolpyruvate. In conclusion, customized fertilizer had no difference in amino acids compared to the conventional-NPK practice which was higher than in no fertilization, and also the normal paddy represented slightly higher amino acids compared to the reclaimed. Further study based on the present results is required to investigate what is main factor to amino acids between genetic and environmental factors.

Sequential use of real-time polymerase chain reaction and enzyme-linked immunosorbent assay techniques verifies adulteration of fermented sausages with chicken meat

  • Benli, Hakan;Barutcu, Elif
    • Animal Bioscience
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    • v.34 no.12
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    • pp.1995-2002
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    • 2021
  • Objective: Detection of adulteration in processed meats is an important issue for some countries due to substitution of beef with a cheaper source of protein like poultry. In this study, the presence of chicken meat was investigated using real-time polymerase chain reaction (real-time PCR) and enzyme-linked immunosorbent assay (ELISA) techniques to verify adulteration of fermented sausage samples. Methods: A total of 60 commercial samples were collected from 20 establishments in three replicates including 10 fermented sausage manufacturers and 10 butchers to investigate the presence of chicken meat with the sequential use of real-time PCR and ELISA techniques. In addition, pH, moisture content, water activity and color values of the samples were determined. Results: Both real-time PCR and ELISA showed agreement on the presence or absence of chicken meat in 55 out of 60 fermented sausage samples and chicken meat was identified with both methods in 16 samples. Five samples produced inconsistent results for the presence of chicken meat in the first run. Nevertheless, the presence of chicken meat was verified with both methods when these samples were analyzed for the second time. In addition, the average physico-chemical values of the fermented sausage samples tested positive for chicken meat were not significantly different from some of those fermented sausage samples tested negative for the chicken meat. Conclusion: The sequential use of real-time PCR and ELISA techniques in fermented sausages could be beneficial for the government testing programs to eliminate false negatives for detection of adulteration with chicken meat. Furthermore, consumers should not rely on some of the quality cues including color to predict the adulteration of fermented sausages with chicken meat since there were no statistical differences among some of the samples tested positive and negative for chicken meat.

Effect of the Properties of Diesel Engine Oil and Aging on Exhaust Gases and DPF (경유엔진용 윤활유의 성상 및 열화가 배출가스 및 후처리 장치에 미치는 영향 연구)

  • Kim, JeongHwan;Kim, KiHo;Lee, JungMin
    • Tribology and Lubricants
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    • v.34 no.6
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    • pp.292-299
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    • 2018
  • The objective of this research is to investigate the impact of engine oil aging on PM(Particulate Matter), exhaust gases, and DPF. It is widely known that the specification of a lubricant and its consumption in an ICE considerably influences the release of regulated harmful emissions under normal engine operating conditions. Considering DPF clogging phenomena associated with lubricant-derived soot/ash components, a simulated aging mode is designed for DPF to facilitate engine dynamometer testing. A PM/ash accumulation cycle is developed by considering real-world engine operating conditions for the increment of engine oil consumption and natural DPF regeneration for ash accumulation. The test duration for DPF aging is approximately 300 h with high- and low-SAPs engine oils. Detailed engine lubricant properties of new and aged oils are analyzed to evaluate the effect of engine oil degradation on vehicle mileage. Furthermore, physical and chemical analyses are performed using X-CT, ICP, and TGA/DSC to quantify the engine oil contribution on the PM composition. This is achieved by sampling with various filters using specially designed PM sampling equipment. Using high SAPs engine oil causes more PM/ash accumulation compared with low SAPs engine oils and this could accelerate fouling of the EGR in the engine, which results in an increase in harmful exhaust gas emissions. These test results on engine lubricants under operating conditions will assist in the establishment of regulated and unregulated toxic emissions policies and lubricant quality standards.

Mechanical behaviour of waste powdered tiles and Portland cement treated soft clay

  • Al-Bared, Mohammed A.M.;Harahap, Indra S.H.;Marto, Aminaton;Abad, Seyed Vahid Alavi Nezhad Khalil;Mustaffa, Zahiraniza;Ali, Montasir O.A.
    • Geomechanics and Engineering
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    • v.19 no.1
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    • pp.37-47
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    • 2019
  • The main objective of this study is to evaluate and compare the efficiency of ordinary Portland cement (OPC) in enhancing the unconfined compressive strength of soft soil alone and soft soil mixed with recycled tiles. The recycled tiles have been used to treat soft soil in a previous research by Al-Bared et al. (2019) and the results showed significant improvement, but the improved strength value was for samples treated with low cement content (2%). Hence, OPC is added alone in this research in various proportions and together with the optimum value of recycled tiles in order to investigate the improvement in the strength. The results of the compaction tests of the soft soil treated with recycled tiles and 2, 4, and 6% OPC revealed an increment in the maximum dry density and a decrement in the optimum moisture content. The optimum value of OPC was found to be 6%, at which the strength was the highest for both samples treated with OPC alone and samples treated with OPC and 20% recycled tiles. Under similar curing time, the strength of samples treated with recycled tiles and OPC was higher than the treated soil with the same percentage of OPC alone. The stress-strain curves showed ductile plastic behaviour for the untreated soft clay and brittle behaviour for almost all treated samples with OPC alone and OPC with recycled tiles. The microstructural tests indicated the formation of new cementitious products that were responsible for the improvement of the strength, such as calcium aluminium silicate hydrate. This research promotes recycled tiles as a green stabiliser for soil stabilisation capable of reducing the amount of OPC required for ground improvement. The replacement of OPC with recycled tiles resulted in higher strength compared to the control mix and this achievement may results in reducing both OPC in soil stabilisation and the disposal of recycled tiles into landfills.

Study on the Degradaion Behavior of Acrylonitrile Rubber(NBR) O-ring by Intermittent CSR and Time-Temperature Superposition Principle (간헐 압축응력완화 시험법과 시간-온도 중첩 이론을 이용한 NBR 오링의 노화 거동 분석 연구)

  • Lee, Jin Hyok;Bae, Jong Woo;Choi, Myung Chan;Yun, Yu Mi;Kim, Wonho;Park, Sung Han;Jo, Nam-Ju
    • Journal of the Korean Society of Propulsion Engineers
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    • v.23 no.1
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    • pp.46-51
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    • 2019
  • Intermittent CSR testing was used to investigate the degradation of a NBR O-ring, and also the prediction of its life-time. An intermittent CSR jig was designed taking into consideration the O-ring's environment under use. Degradation of O-rings by thermal aging was observed between $40^{\circ}C$ and $120^{\circ}C$. O-rings showed non-linear degradation behavior under $80^{\circ}C$. At 20% of failure condition, predicted life-times were 32.5 years by Arrhenius plot and 22.6 years by WLF plot.

Effect of yttrium additives on the shear bond strength of porcelain fused to Ni-Cr alloy for porcelain fused metal crown (도재용착용 Ni-Cr계 합금의 이트륨 첨가물이 도재전단결합강도에 미치는 영향)

  • Woo, Je-Seung;Noh, Se-Ra;Noh, Hyeong-Rok;Lim, Chung-Ha;Lee, Jung-Hwan
    • Journal of Technologic Dentistry
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    • v.41 no.2
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    • pp.71-80
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    • 2019
  • Purpose: In this study, to evaluate the effect of oxide changes on the shear bond strength according to the composition of Ni-Cr alloys for porcelain fused matal crown, T-4 alloys, Zeroy alloys and Zeroy-X alloys were selected. Methods: 20 specimens were fabricated using selected Ni-Cr alloys and porcelain powders. A Ni-Cr alloy having a diameter of 5 mm and a height of 25 mm was produced and the metal surface was polished. Porcelain powder was fired on the polished metal surface to a diameter of 5 mm and a height of 3 mm. The experiment group consisted of three groups, T-4(TNA), Zeroy(ZNA) and Zeroy-X(ZXA). The fabricated specimens were mounted on a jig of a universal testing machine(UTM) and fracture strength was measured by applying a shear force at a UTM crosshead speed of 0.5 mm/min. The fracture strength was calculated as the bond strength between the porcelain and the alloy. The surface of the fractured alloy was analyzed by X-ray diffraction(XRD) and scanning electron microscopy(SEM), and the components of the oxide were measured by energy dispersive X-ray spectroscopy(EDX) line profile method. Results: In SEM, XRD and EDX analysis, yttrium tended to increase the mechanical and chemical bonding forces. The shear bond strength of ZXA group containing yttrium showed the highest value at 27.53 MPa. Conclusion: Based on the results of this study, it is considered that the yttrium-added Ni-Cr alloy is clinically acceptable in porcelain shear bond strength.