• Title/Summary/Keyword: changes of grain size

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Geomorphological Properties and Changes of Goreabul Sand Beach in Yeongdeok (영덕 고래불 모래해안의 지형 특성과 변화)

  • Bang, Hyun Ju;Lee, Gwang-Ryul
    • Journal of The Geomorphological Association of Korea
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    • v.18 no.3
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    • pp.83-92
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    • 2011
  • The properties and changes of geomorphic relief and coastal deposits were analyzed at Goreabul sand beach in Yeongdeok-gun, the largest that in east coast of Kyungsangbuk-do Province. As the result of grain size analysis, in almost season except summer, the sands mainly deposited in Goraebul sand beach because longshore current drift northward contrary to Gangwon-do east coast, and summer longshore current is weak or change direction to south ward. Sand beach mostly came form erosion owing to typoon and storm and was deposit more coarse sand in the summer, and was produced deposition actively in the fall and winter. Front side of sand dune came from deposition on sand every season by sea breeze, especially in the winter.

Dielectric and Piezoelectric Properties of Pb(Ni1/3Nb2/3)O3-PbTiO3-PbZrO3 Solid Solution Ceramics (Pb(Ni1/3Nb2/3)O3-PbTiO3-PbZrO3계의 유전 및 압전특성)

  • 손정호;남효덕;조상희
    • Journal of the Korean Ceramic Society
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    • v.25 no.5
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    • pp.523-531
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    • 1988
  • The dielectric and piezoelectric properties with compositions in Pb(Ni1/3Nb2/3)O3-PbTiO3-PbZrO3-(PNN-PT-PZ)solid solution ceramics were investigated. In this study, the compsition ranges were 30 PNN 45mole%, 20 PT 50mole% and 50 PZ5mole%. As PT fraction were increased the grain size was increased and the fired density was decreased, but the changes of PNN fraction had no effect on the grain size. The Curie temperature was increased when PT and PNN fraction were increased. The displacement was increased but had a great hysteresis loss when PT fraction was increased. In morphotropic phase boundary, the maximum piezoelectric and electromechanical coupling factor were indicated. Morphotropic phase boundary(MPB) was 34 PT 36mole% in chang of compositions.

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A Study on Dynamic and Static Recrystallization Behaviors and Microstructure Evolution Prediction of Die Steels (금형강의 동적 및 정적 재결정 거동과 미세조직 변화 예측에 관한 연구)

  • Jeong H. S.;Cho J. R.;Cha D. J.;Bae Y. B.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2001.05a
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    • pp.131-135
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    • 2001
  • Evaluation of microstructural changes during open die forging of heavy ingots is important for process control. The objective of the control of forging parameters, such as shape of the dies, reduction, temperature and sequence of passes, is to maximize the forging effects md to minimize inhomogeneities of mechanical properties. The hot working die steel is produced by using the multistage open die forging. The structure is altered during forging by subsequent processes of plastic deformation, recrystallization and grain growth. A numerical analysis using an rigid visco-plastic finite element model was performed to predict microstructural evolution of hot working die steel.

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A Study on Dynamic and Static Recrystallization Behaviors and Microstructure Evolution Prediction of a Die Steel (금형강의 동적 및 정적 재결정 거동과 미세조직 변화 예측에 관한 연구)

  • 정호승;조종래;차도진;배원병
    • Transactions of Materials Processing
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    • v.10 no.4
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    • pp.338-346
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    • 2001
  • Evaluation of microstructural changes is important for process control during open die forging of heavy ingots. The control of forging parameters, such as shape of the dies, reduction, temperature and sequence of passes, is to maximize the forging effects and to minimize inhomogeneities of mechanical properties. The hot working die steel is produced by using the multistage open die forging. The structure is altered during forging by subsequent Precesses of plastic deformation, recrystallization and grain growth. A numerical analysis using an rigid visco-plastic finite element model was performed to predict microstructural evolution of hot working die steel.

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Impedance Properties of Phase-Pure Titanium Dioxide Ceramics Sintered at Different Temperatures

  • Cui, Liqi;Niu, Ruifeng;Wang, Weitian
    • Korean Journal of Materials Research
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    • v.32 no.4
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    • pp.181-185
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    • 2022
  • In this study, phase-pure titanium dioxide TiO2 ceramics are sintered using standard high-temperature solid-state reaction technique at different temperatures (1,000, 1,100, 1,200, 1,300, 1,400 ℃). The effect of sintering temperature on the densification and impedance properties of TiO2 ceramics is investigated. The bulk density and average grain size increase with the increase of sintering temperature. Impedance spectroscopy analysis (complex impedance Z* and complex modulus M*), performed in a broad frequency range from 100 Hz to 10 MHz, indicates that the TiO2 ceramics are dielectrically heterogeneous, consisting of grains and grain boundaries. The complex impedance Z* -plane indicates the resistance of grains of the TiO2 ceramics increases with increasing sintering temperature, while that of grain boundaries develops in the opposing direction. The complex modulus M*-plane shows a grain capacitance that seems to be independent of the sintering temperature, while that of the grain boundaries decreases with increasing sintering temperature. These results suggest that different sintering temperatures have effects on the microstructure, leading to changes in the impedance properties of TiO2 ceramics.

Seasonal Variation of Surface Sediment Distribution and Transport Pattern Offshore Haeundae Beach Area (해운대 연안 표층퇴적물 분포의 계절변화와 이동)

  • Kim, Seok-Yun;Jeong, Joo-Bong;Lee, Byoung-Kwan
    • The Sea:JOURNAL OF THE KOREAN SOCIETY OF OCEANOGRAPHY
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    • v.17 no.1
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    • pp.16-24
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    • 2012
  • To study the seasonal pattern of sediment distribution and the transport tendency in Haeundae nearshore area; i) the grain size texture of surface sediment was examined in June, October, and December of 2007, and March and June of 2008, and secondary, ii) the transport tendency was studied by using a two-dimensional sediment transport model of Gao and Collins (1992), and finally, iii) the bathymetric changes were analyzed by using the data collected in February, May, August, and December of 2007 by Haeundae District Office. Spatial distribution of sediment texture, the tendency of sediment transport as well as the bathymetric change showed significant seasonal variations. From June to December of 2007, the eastern part of the Haeundae area, off Dalmaji Hill showed the coarsening of mean grain size with a prominent transport tendency toward the Haeundae beach. On the contrary, the western part of the area, off Dongbaek Island showed a fining trend of mean grain size, and the transport tendency toward the beach was relatively weakened. From December of 2007 to June of 2008, the mean grain size of Mipo Harbor became finer, and the transport tendency toward the central beach decreased. The mean grain size of Dongbaek Island became coarser, while the tendency increased in the direction of the beach. The areas of significant net accumulation and erosion were depicted based on the bathymetric changes between observation periods. During the period of February to May of 2007, net accumulation was observed on the eastern part of the study area, in front of Mipo Harbor. Erosion was generally occurred throughout the area from May to August of 2007. From August to December of 2007, erosion and accumulation was observed off Mipo Harbor and Dongbaek Island, respectively. The change of sediment facies also suggests the accumulation on the eastern coast during the spring, erosion around the entire coast during the summer, and accumulation on the western coast during the winter. The changes in the accumulation and erosion were most apparent during the summer when several typhoons have passed by, while unnoticeable during the spring.

Effect of Surface Morphology in ZnO:Al/Ag Back Reflectors for Flexible Silicon Thin Film Solar Cells on Light Scattering Properties (플렉서블 실리콘 박막 태양전지용 ZnO:Al/Ag 후면반사막의 표면형상에 따른 광산란 특성 변화)

  • Beak, Sang-Hun;Lee, Jeong-Chul;Park, Sang-Hyun;Song, Jin-Soo;Yoon, Kyung-Hoon;Wang, Jin-Suk;Lee, Hi-Deok;Cho, Jun-Sik
    • Korean Journal of Materials Research
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    • v.20 no.10
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    • pp.501-507
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    • 2010
  • Changes in surface morphology and roughness of dc sputtered ZnO:Al/Ag back reflectors by varying the deposition temperature and their influence on the performance of flexible silicon thin film solar cells were systematically investigated. By increasing the deposition temperature from $25^{\circ}C$ to $500^{\circ}C$, the grain size of Ag thin films increased from 100 nm to 1000 nm and the grain size distribution became irregular, which resulted in an increment of surface roughness from 6.6 nm to 46.6 nm. Even after the 100 nm thick ZnO:Al film deposition, the surface morphology and roughness of the ZnO:Al/Ag double structured back reflectors were the same as those of the Ag layers, meaning that the ZnO:Al films were deposited conformally on the Ag films without unnecessary changes in the surfacefeatures. The diffused reflectance of the back reflectors improved significantly with the increasing grain size and surface roughness of the Ag films, and in particular, an enhanced diffused reflectance in the long wavelength over 800 nm was observed in the Ag back reflectors deposited at $500^{\circ}C$, which had an irregular grain size distribution of 200-1000 nm and large surface roughness. The improved light scattering properties on the rough ZnO:Al/Ag back reflector surfaces led to an increase of light trapping in the solar cells, and this resulted in a noticeable improvement in the $J_{sc}$ values from 9.94 mA/$cm^2$ for the flat Ag back reflector at $25^{\circ}C$ to 13.36 mA/$cm^2$ for the rough one at $500^{\circ}C$. A conversion efficiency of 7.60% ($V_{oc}$ = 0.93, $J_{sc}$ = 13.36 mA/$cm^2$, FF = 61%) was achieved in the flexible silicon thin film solar cells at this moment.

The Changes of Physical Properties of Barley Grain at Various Polishing Yields during Hydration Process (도정수율별(搗精收率別) 보리의 수화공정중(水和工程中) 물성변화(物性變和)에 관(關)한 연구(硏究))

  • Mok, Chul-Kyoon;Nam, Young-Joong
    • Applied Biological Chemistry
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    • v.26 no.1
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    • pp.47-52
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    • 1983
  • The size distribution and changes of volume and grain hardness of ‘Sedohadaka', waked barley of various polishing yields during hydration process at various temperatures were investigated, and were analyzed kinetically, Both major and minor diameter of barley grain decreased linearly during polishing, and the decreasing rate of major diameter was greater than that of minor diameter. The volume change of barley grain could be expressed as a power of hydration time, and a break point was found in case of non-polished barley. The changing rate of grain hardness followed the equation of a first-order reaction, and the reaction rate constant increased with decreasing polishing yields and at higher temperature in the range of $20{\sim}60^{\circ}C$. The activation energy of hardness change reaction of polished barley during hydration were ranged $5.1{\sim}7.8Kcal/mole$, and 13.3Kcal/mole of non-polished barley.

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A Study on the Characteristics and Burial Ages of Sediment Deposits at Jiduri, Daecheong Island (대청도 지두리 해안의 모래 퇴적층의 특성과 매몰연대에 대한 연구)

  • Kim, Jong Yeon
    • Journal of The Geomorphological Association of Korea
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    • v.25 no.1
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    • pp.1-17
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    • 2018
  • The characteristics and burial ages of sand sediments on the Jiduri coast in Daechung-myeon, Ongjin-gun, Incheon were investigated. Daecheong Island is the area where the characteristics of the rocky coast and sand coast are shown. Various studies have been conducted on the Okjukdong sand dune that appears in the north of the island. However, there has been no study on the sandy sedimentary topography of the Jiduri and Moraewul area in the south. The sandy sedimentary terrain of Jiduri is divided into sandy beaches, sand dunes and sand deposits along the slope including climbing dune. Overall, the depth of sandy sediments in Jiduri is not deep. The characteristics of sandy sediments and burial ages were investigated at an elevation of about 23 m above sea level at the back of Jiduli Beach and 46 m above sea level at the ridge line between Jiduri and Moraewol. From the Jiduri coast to the hillside behind, the average grain size decreases and the sorting becomes better as it moves from the intertidal zone to the beach and the foredune. This indicates the selective sand transport by the wind and can be judged by the terrain formed under the current sedimentation environment. The average grain size at the upper part of the section of JD-1 (elevation of about 23m MSL) was $1.6918{\varphi}$ of medium sand. The sorting was $0.4584{\varphi}$, skewness was -1.0491 and kurtosis was -1.2411, respectively. Particularly, the average particle size of the crosssection issomewhat uniform, but the color of the constituent material changes from brown to black. In the case of JD-2 (about 46 m MSL), the mean grain size of the section was $1.7943{\varphi}$, the sorting was 0.4931, the skewness was -1.1163, and the kurtosis was 1.2133. On the other hand, the brown and black layers of JD-1 exhibited a burial age of $0.1{\pm}0.0ka$ and the JD-2 had a burial age of $0.7{\pm}0.0ka$.

Application of Automated Microscopy Equipment for Rock Analog Material Experiments: Static Grain Growth and Simple Shear Deformation Experiments Using Norcamphor (유사물질 실험을 위한 자동화 현미경 실험 기기의 적용과 노캠퍼를 이용한 입자 성장 및 단순 전단 변형 실험의 예)

  • Ha, Changsu;Kim, Sungshil
    • Economic and Environmental Geology
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    • v.54 no.2
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    • pp.233-245
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    • 2021
  • Many studies on the microstructures in rocks have been conducted using experimental methods with various equipment as well as natural rock studies to see the development of microstructures and understand their mechanisms. Grain boundary migration of mineral aggregates in rocks could cause grain growth or grain size changes during metamorphism or deformation as one of the main recrystallization mechanisms. This study suggests improved ways regarding the analog material experiments with reformed equipment to see sequential observations of these grain boundary migration. It can be more efficient than the existing techniques and carry out an appropriate microstructure analysis. This reformed equipment was implemented to enable optical manipulation by mounting polarizing plates capable of rotating operation on a stereoscopic microscope and a deformation rig capable of experimenting with analog materials. The equipment can automatically control the temperature and strain rate of the deformation rig by microcontrollers and programming and can take digital photomicrographs with constant time intervals during the experiment to observe any microstructure changes. The composite images synthesized using images by rotated polarizing plates enable us to see more accurate grain boundaries. As a rock analog material, norcamphor(C7H10O) was used, which has similar birefringence to quartz. Static grain growth and simple shear deformation experiments were performed using the norcamphor to verify the effectiveness of the equipment. The static grain growth experiments showed the characteristics of typical grain growth behavior. The number of grains decreases and the average grain size increases over time. These case experiments also showed a clear difference between the growth curves with three temperature conditions. The result of the simple shear deformation experiment under the medium temperature-low strain rate showed no significant change in the average grain size but presented the increased elongation of grain shapes in the direction of about 53° regarding the direction perpendicular to the shearing direction as the shear strain increases over time. These microstructures are interpreted as both the plastic deformation and the internal recovery process in grains are balanced by the deformation under the given experimental conditions. These experiments using the reformed equipment represent the ability to sequentially observe changing the microstructure during experiments as desired in the tests with the analog material during the entire process.