• Title/Summary/Keyword: ceramic processing

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Selective Laser Sintering of Alumina Using an Inorganic Binder Monoclinic $HBO_2$ and Post-Processing

  • 이인섭
    • Journal of Powder Materials
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    • v.5 no.3
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    • pp.199-209
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    • 1998
  • A new low melting inorganic binder, monoclinic $HBO_2$, has been developed for Selective Laser Sintering (SLS) of alumina powder by dehydration process of boron oxide powder in a vacuum oven at $120^{\circ}C$. It led to better green SLS parts and higher bend strength far green and fired parts compared to other inorganic binders such as aluminum and ammmonium phosphate. This appeared to be due to its low viscosity and better wettability of the alumina particle surface. A low density single phase ceramic, aluminum borate ($Al_{18}B_4O_{33}$), and multiphase ceramic composites, $A_{12}O_3-A_{14}B_2O_9$, were successfully developed by laser processing of alumina-monoclinic $HBO_2$ powder blends followed by post-thermal processing; both $Al_{18}B_4O_{33}$ and $A_{14}B_2O_9$ have whisker-like grains. The physical and mechanical properties of these SLS-processed ceramic parts were correlated to the materials and processing parameters. Further densification of the $A_{12}O_3-A_{14}B_2O_9$ ceramic composites was carried out by infiltration of colloidal silica, and chromic acid into these porous SLS parts followed by heat-treatment at high temperature ($1600^{\circ}C$). The densities obtained after infiltration and subsequent firing were between 75 and 80% of the theoretical densities. The bend strengths are between 15 and 33 MPa.

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Low Temperature Processing of Porous Silicon Carbide Ceramics by Carbothermal Reduction (탄소열환원 공정을 사용한 다공질 탄화규소 세라믹스의 저온 제조공정)

  • Eom, Jung-Hye;Jang, Doo-Hee;Kim, Young-Wook;Song, In-Hyuck;Kim, Hai-Doo
    • Journal of the Korean Ceramic Society
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    • v.43 no.9 s.292
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    • pp.552-557
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    • 2006
  • A low temperature processing route for fabricating porous SiC ceramics by carbothermal reduction has been demonstrated. Effects of expandable microsphere content, sintering temperature, filler content, and carbon source on microstructure, porosity, compressive strength, cell size, and cell density were investigated in the processing of porous silicon carbide ceramics using expandable microspheres as a pore former. A higher microsphere content led to a higher porosity and a higher cell density. A higher sintering temperature resulted in a decreased porosity because of an enhanced densification. The addition of inert filler increased the porosity, but decreased the cell density. The compressive strength of the porous ceramics decreased with increasing the porosity. Typical compressive strength of porous SiC ceramics with ${\sim}70%$ porosity was ${\sim}13 MPa$.

Fabrication of Concrete Containing Mechanochemically Surface Treated(MST) Fly Ash (Mechanochemical 표면처리한 Fly Ash 혼화 Concrete의 제조)

  • Lee, Hyung-Jik;Koo, Ja-Hun;Yoo, In-Sang;Song, Doo-Gyoo;Joung, Hae-Kyoung;Kwon, Hyouk-Byoung;Yoon, Sang-Ok;Lee, Hyung-Bock;Lee, Hong-Lim
    • Journal of the Korean Ceramic Society
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    • v.39 no.2
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    • pp.135-144
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    • 2002
  • Fabrication of high strength structural concrete was investigated by using a mechanochemically Surface Treated Fly Ash(MSTFA) induced by mechanochemical processing through ball-milling of (90 wt% As Recevied Fly Ash(ARFA) + 10wt% cement) mixture, which was compared to the specimen fabricated by using As Received Fly Ash(ARFA) in terms with compressive strength and microstructures. The compressive strength of concrete specimen fabricated by using MSTFA represented 10-20% and 2-7% higher value than that for the case of using ARFA and BPFA in each cases. Increased compressive strength as above mentioned is considered to be caused by mutually increased affinity generated between cement and fly ash during mechanochemical processing.

A Study of High Temperature Filtration Performance Test on Low Density Cylindrical Ceramic Filters (저밀도 원통형 세라믹 필터의 고온 여과 성능시험 연구)

  • 이동섭;홍민선;최종인
    • Journal of Korean Society for Atmospheric Environment
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    • v.17 no.2
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    • pp.213-222
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    • 2001
  • Cylindrical type ceramic filers, that is 60 O.D$\times$10t$\times$600L and 60 O.D$\times$10t$\times$1,000L were manufactured by vacuum forming processes using ceramic ray materials. For cylindrical type ceramic filters, porosity and bulk density were measured for, 80 to 90% and 0.3 to 0.4 g/㎤, respectively at uniform pore size of 41 to 45${\mu}{\textrm}{m}$. Bench scale candle filters (60$\psi$ $\times$10t$\times$600L) were tested using different dusts collected from many industries including chemical processing, glass processing and metal manufacturing pants. Collection efficiencies found out to range from 99.87% to 99.90%, while resistance coefficients from 1.1$\times$10(sup)11/$m^2$ to 1.7$\times$10(sup)11/$m^2$ . Full scale low density ceramic filters (60$\psi$ $\times$10t$\times$1,000L) were also tested at 1 atm, $600^{\circ}C$ to reveal the filtration efficiency, conditioning, and resistance coefficients using two different types of dust as chemical processing and metal refined processing. Darcys law resistance coefficients were measured to range 1.44$\times$10(sup)11/$m^2$ to 2.74$\times$10(sup)11/$m^2$, and collection efficiencies on the range 99.84 to 99.96%, Finally, results of long term performance test showed that filters were conditioned after 170hrs. Experimental conditions for effective filtration were examined under the condition 10 cm/sec face velocity, 3kg/$\textrm{cm}^2$ pulsing pressure, 5 min filtration cycle, and 300msec pulse opening time.

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Ceramic Stereolithography: Additive Manufacturing for 3D Complex Ceramic Structures

  • Bae, Chang-Jun;Ramachandran, Arathi;Chung, Kyeongwoon;Park, Sujin
    • Journal of the Korean Ceramic Society
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    • v.54 no.6
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    • pp.470-477
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    • 2017
  • Ceramic processing to fabricate 3D complex ceramic structures is crucial for structural, energy, environmental, and biomedical applications. A unique process is ceramic stereolithography, which builds ceramic green objects from CAD files from many thin liquid layers of powder in monomer, which are solidified by polymerization with a UV laser, thereby "writing" the design for each slice. This approach directly writes layers in liquid ceramic suspension and allows one to fabricate ceramic parts and products having more accurate, complex geometries and smooth surfaces. In this paper, both UV curable materials and processes are presented. We focus on the basic material principles associated with free radical polymerization and rheological behavior, cure depth and broadening of cured lines, scattering at ceramic interface and their corresponding simulation. The immediate potentials for ceramic AM to change industry fabrication are also highlighted.

Sodium titanate as an infrared reflective material for cool roof application

  • Ullah, Mahboob;Kim, Hee Jung;Heo, Jae Gu;Roh, Dong Kyu;Kim, Dae-Sung
    • Journal of Ceramic Processing Research
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    • v.20 no.spc1
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    • pp.86-91
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    • 2019
  • A solid-state route was used to prepare sodium titanium oxide (NTO, Na2Ti3O7) as a solar heat protecting material with an impressive solar reflectance (TSR = 94.3%) using a high refractive index rutile TiO2. The solar reflectance of the synthesized NTO was measured using UV-Vis-NIR spectrophotometer. Solar reflectance property of the synthesized compound depends on the calcination temperature. The solar reflectance property of the synthesized NTO powder was compared with commercial rutile TiO2. The compound synthesized at 900 ℃ for 24 hrs had remarkable solar reflectance 94.3% than that calcined below 900 ℃. Crystalline nature, structural property, morphology and optical properties of NTO powders were characterized and analyzed using XRD, FE-SEM, EDS and UV-Vis-NIR spectrophotometer. From the results, we guessed that NTO would be a suitable "solar heat protecting candidate" for energy-saving applications in coating industries.

Novel CAD/CAM hybrid blocks: PICN and RNC (새로운 CAD/CAM 블록의사용 : PICN and RNC)

  • Ko, Kyung-Ho
    • The Journal of the Korean dental association
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    • v.56 no.3
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    • pp.167-174
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    • 2018
  • The development of dental materials has widened the scope of materials by changes in processing methods. CAD/CAM processing enables the use of zirconia as a dental material. Recent esthetic materials development has been made. For aesthetic purposes, a block for CAD/CAM processing by mixing polymer and ceramic materials are fabricated. However there is no guideline of how these materials should be used in actual clinical practice. Mechanical properties, wear and clinical studies were reviewed.

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