• The Journal of Korean Academy of Prosthodontics
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• v.45 no.2
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• pp.169-181
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• 2007

Statement of problem: Titanium is well known as a proper metal for the dental restorations, because it has an excellent biocompatibility, resistance to corrosion, and mechanical property. However, adhesion between titanium and dental porcelains is related to the diffusion of oxygen to the reaction layers formed on cast-titanium surfaces during porcelain firing and those oxidized layers make the adhesion difficult to be formed. Many studies using mechanical, chemical and physical methods to enhance the titanium-ceramic adhesion have been actively performed. Purpose: This study meant to comparatively analyse the adhesion characteristics depending on different titanium surface coatings after coating the casts and wrought titanium surfaces with Au and TiN. Material and method: In this study, the titanium specimens (CP-Ti, Grade 2, Kobe still Co. Japan) were categorized into cast and wrought titanium. The wrought titanium was cast by using the MgO-based investment(Selevest CB, Selec). The cast and wrought titanium were treated with Au coating($ParaOne^{(R)}$., Gold Ion Sputter, Model PS-1200) and TiN coating(ATEC system, Korea) and the ultra low fusing dental porcelain was fused and fired onto the samples. Biaxial flection test was done on the fired samples and the porcelain was separated. The adhesion characteristics of porcelain and titanium after firing and the specimen surfaces before and after the porcelain fracture test were observed with SEM. The atomic percent of Si on all sample surfaces was comparatively analysed by EDS. In addition, the constituents of specimen surface layers after the porcelain fracture and the formed compound were evaluated by X-ray diffraction diagnosis. Result: The results of this study were obtained as follows : 1. The surface characteristics of cast and wrought titanium after surface treatment(Au, TiN, $Al_2O_3$ sandblasting) were similar and each cast and wrought titanium showed similar bonding characteristics. 2. Before and after the biaxial flection test, the highest atomic weight change of Si component was found in $Al_2O_3$ sandblasted wrought titanium(28.6at.% $\rightarrow$ 8.3at.%). On the other hand, the least change was seen in Au-Pd-In alloy(24.5at.% $\rightarrow$ 9.1at.%). 3. Much amount of Si components was uniformly distributed in Au and TiN coated titanium, but less amount of Si's was unevenly dispersed on Al2O3 sandblasting surfaces. 4. In X-ray diffraction diagnosis after porcelain debonding, we could see $Au_2Ti$ compound and TiN coating layers on Au and TiN coated surfaces and $TiO_2$, typical oxide of titanium, on all titanium surfaces. 5. Debonding of porcelain on cast and wrought titanium surface after the biaxial flection is considered as a result of adhesion deterioration between coating layers and titanium surfaces. We found that there are both adhesive failure and cohesive failure at the same time. Conclusion: These results showed that the titanium-ceramic adhesion could be improved by coating cast and wrought titanium surfaces with Au and TiN when making porcelain fused to metal crowns. In order to use porcelain fused to titanium clinically, it is considered that coating technique to enhance the bonding strength between coating kKlayers and titanium surfaces should be developed first.

• Journal of Mechanical Science and Technology
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• v.20 no.1
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• pp.13-18
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• 2006

Ti-8Ta-3Nb, as a new biomaterial, was prepared by cast and swaging process. Their deformation behavior of Ti-8Ta-3Nb alloy has been characterized on the basis of its flow stress variation obtained from the true strain rate compression testing in the temperature of $700-900^{\circ}C$ and strain rate of $0.001-10\;s^{-1}$. At the strain rates lower than $0.1\;s^{-1}$ and the all temperature ranges which consist of two phase ${\alpha}+{\beta}$ as well as single ${\beta}$ phase fields, the flow curves show a small degree of flow softening behavior. In contrast, the shapes of the flow curves at other strain rates indicate unstable behavior. The shapes of the flow curves were similar in both as-cast and swaged specimen as well as in both ${\alpha}+{\beta}$ phase and ${\beta}$ phase. The flow stress data did not obey the kinetic rate equation over the entire regime of testing but a good fit has been obtained in the intermediate range of temperatures ($750-850^{\circ}C$). In this range, a stress exponent value of about 7.7 in as-cast specimens and about 6.2 in swaged specimens with an apparent activation energy of about 300 kJ/mol and about 206 kJ/mol respectively have been evaluated.

• Journal of Korea Foundry Society
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• v.24 no.1
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• pp.52-59
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• 2004

Microstructure and mechanical properties of ductile cast iron were investigated in terms of diameter change of samples that gives rise to modify the microstructure due to different cooling rate in the continuous casting process. The chemical composition used in this study was GCD 400 grade. From the microstructural observation, we have found a large number of graphite with small size in diameter which is comparable to the microstructure of the sample produced by conventional sand casting. The major reason of this would he due to high cooling rate. In the sample with 26 mm in diameter, the microstructure was composed of pearlite, iron carbide, and graphite. In the samples with 60 and 100 mm in diameter, however, we have observed a dissimilar microstructure that consisting of ferrite and graphite. Concerning the mechanical property, the sample with 26 mm in diameter showed higher hardness and strength compared to those samples with 60 and 100 mm in diameter. The result obtained for ductility appeared a reversal. Much more works such as inoculation, process design and chemical composition would be required in order to have a sound product even in a small diameter of samples.

• Journal of Korea Foundry Society
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• v.15 no.2
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• pp.146-155
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• 1995

This study was performed to investigate the effect of austempering temperature on the mechanical properties and fracture characteristics of the ductile cast iron with Cu, Mo and Cu, Mo, Ni. The results obtained from this study are summarized as follows; Microstructures of Cu-Mo and Cu-Mo-Ni ductile cast iron by austempering were obtained low bainite with some martensite at $250^{\circ}C$, mixture structure of upper and low bainite obtained at $300^{\circ}C$ and upper bainite obtained at $350^{\circ}C$. Tensile, impact and fracture toughness properties were remarkably controlled by retained austenite. With increasing austempering temperature, tensile and yield strength, hardness decreased, while the elongation and impact absorption energy, fracture toughness increased. With adding Ni, tensile and yield strength increased and elongation, facture toughness and impact absorption energy decreased. Retained austenite increased with increasing austempering temperature and the fracture surface were shown mixture structure of fibrous and dimple.

• Geomechanics and Engineering
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• v.5 no.2
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• pp.119-142
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• 2013

Pile load tests using Osterberg cells (O-cell) were conducted on cast-in-place concrete piles founded in oil sand fill and in situ oil sand at an industrial plant site in Fort McMurray, Alberta, Canada. Interpreted pile test results show that very high pile shaft resistance (with the Bjerrum-Burland or Beta coefficient of 2.5-4.5) against oil sand could be mobilized at small relative displacements of 2-3% of shaft diameter. Finite element simulations based on linear elastic and elasto-plastic models for oil sand materials were used to analyze the pile load test measurements. Two constitutive models yield comparable top-down load versus pile head displacement curves, but very different behaviour in mobilization of pile shaft and end bearing resistances. The elasto-plastic model produces more consistent matching in both pile shaft and end bearing resistances whereas the linear elastic under- and over-predicts the shaft and end bearing resistances, respectively. The mobilization of high shaft resistance in oil sand under pile load is attributed to the very dense and interlocked structure of oil sand which results in high matrix stiffness, high friction angle, and high shear dilation.

• Journal of Korea Foundry Society
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• v.37 no.6
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• pp.199-206
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• 2017

In this study, the variations of microstructures and tensile properties of Ti-(44-54)at.%Al binary alloys were investigated. The heat-treated microstructure depended greatly on their solidification structure and annealing temperature. We measured the variations of volume fractions of primary and secondary lamellar structure as a function of the heat treatment temperature in a Ti-47at.%Al alloy. The variation of ductility as a function of Al content was in good agreement with the change of fracture mode in the tensile fracture surface. It can be inferred that the variations of yield stress and hardness of ${\gamma}$ phase in a single ${\gamma}$-phase field region are enhanced by anti-site defects created by deviations from the stoichiometric composition. In a Ti-47at.%Al alloy within the (${\alpha}_2+{\gamma}$) two-phase field, the yield stress tended to be the maximum at a near equal volume fraction of lamellar and ${\gamma}$ grains. The ductility depended sensitively on the overall grain size and Al content. The calculation of fracture strain using Chan's model indicated that the change of ductility as a function of annealing temperature was primarily determined by the variations in the overall grain size and lamellar volume fraction.

• Steel and Composite Structures
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• v.21 no.5
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• pp.981-997
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• 2016

To avoid the cracks of cast-in-place concrete in shear pockets and seams in the traditional composite beam with precast decks, this paper proposed a new type of prefabricated steel truss-concrete composite beam (ab. PSTC beam) with pre-embedded shear studs (ab. PSS connector). To study the initial cracking load of concrete deck, the development and distribution laws of the cracks, 3 PSTC beams were tested under hogging moment. And the crack behavior of the deck was compared with traditional precast composite beam, which was assembled by shear pockets and cast-in-place joints. Results show that: (i) the initial crack appears on the deck, thus avoid the appearance of the cracks in the traditional shear pockets; (ii) the crack of the seam appears later than that of the deck, which verifies the reliability of epoxy cement mortar seam, thus solves the complex structure and easily crack behavior of the traditional cast-in-place joints; (iii) the development and the distribution laws of the cracks in PSTC beam are different from the conventional composite beam. Therefore, in the deduction of crack calculation theory, all the above factors should be considered.

• Journal of the Korea Concrete Institute
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• v.12 no.2
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• pp.3-11
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• 2000

There is a possibility of poor-state concrete filling condition due to segregation and interlocking of aggregate and paste when a high performance concrete is used at reinforced concrete structure without compaction. This study was conducted to evaluate the flexural behavior of high performance concrete beams with design parameters such as c, t and different concrete filling conditions. Different concrete filling conditions were intentionally made such that the first type specimen was soundly cast to obtain the perfect concrete filling condition. Second type was cast in such a way that up to the longitudinal tensile reinforcement from the top, good concrete was filled while poor concrete was poured for the bottom part to simulate the poor strength, workability and unsatisfactory compaction. Third type was cast in such a was that up to the neutral axis of the beam section from the top, good concrete was filled while so did for the bottom part as the second type. The test results were analyzed in terms of load-displacement response, failure pattern, crack width and crack spacing. The test results indicate that have no effect of concrete filling conditions on the yielding strength of structures. But, have a grate influence on the stiffness and ductility of structures.

• Journal of the Korean Society of Manufacturing Technology Engineers
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• v.7 no.6
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• pp.90-96
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• 1998

The ductile cast iron is austempered at 300, 350 and 40$0^{\circ}C$ temperature in order to investigate the basic factors for monitoring drill wear in automatic production process, and cutting force and AE RMS signals are measured with changing cutting condition for ADI(Austempered Ductile Cast Iron) with different mechanical properties. The signals of cutting force were influenced by cutting speed and feedrate greatly. On the other hand AE RMS signals are influenced by cutting speed where as it is not related with feedrate. As the depth of drilling increases, cutting force shows a slow increase and the value of AE RMS increases until the range of h/d=4. But over the range it increases greatly due to an amount of chip discharge and friction with inner wall of drilling hole, etc. As the drill diameter increases at a constant depth of drilling. Cutting force increases linearly, but the level of AE RMS does not increases linearly due to circumferential velocity and great influence of h/d.

• Journal of the Korean Society for Heat Treatment
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• v.8 no.3
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• pp.197-204
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• 1995

In recent work, we reported that a hot-rolled Fe-18wt%Mn alloy exhibited high damping capacity as well as excellent mechanical properties. It was also proposed that damping capacity of the alloy was proportional to the ${\gamma}/{\varepsilon}$ boundary area. In the present study, the effects of homogenization(12hrs at $1100^{\circ}C$) and solution treatment(1hr at $1050^{\circ}C$ before air cooling) on damping capacity and mechanical properties were investigated for as-cast and heat treated Fe-18wt%Mn alloy. The specimen subjected to both homogenization and solution treatment was found to show superior damping capacity and mechanical properties to the as-cast state due to removal of segregation and increase in ${\gamma}/{\varepsilon}$ boundary area.