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Magnetic Properties and Thermomagnetic Analysis of Cast and Hot-Pressed Pr, Nd-Fe-B Magnets (주조 및 열간압축된 Pr, Nd-Fe-B계 영구자석의 열자기 분석과 자기적 특성)

  • 김동엽;이동구;정원용
    • Journal of the Korean Magnetics Society
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    • v.2 no.1
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    • pp.37-43
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    • 1992
  • Minor phases in cast and hot-pressed R(R=Pr, Nd)-Fe-B magnet were investigated through thermomagnetic analysis. The relationship between minor phases and coercivities of R-Fe-B magnets was studied. ${\alpha}-Fe$ and $Nd_{2}Fe_{17}$ were precipitated in as-cast Pr-Fe-B and Nd-Fe-B alloys respectively. These phases were considered to deteriorate the magnetic properties of R-Fe-B magnets. During the heat treatment, ${\alpha}-Fe$ and $Nd_{2}Fe_{17}$ were annihilated and the magnetic properties of cast R-Fe-B magnet were improved. Hot-pressed Nd-Fe-B magnet showed better thermal stability than sintered magnet.

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Effect of Sr Addition on Mechanical and Corrosion Properties of Mg-Zn-Ca Alloy for Biodegradable Implant Material (생체 분해성 임플란트용 Mg-Zn-Ca 합금의 기계적 및 부식특성에 미치는 Sr 첨가의 영향)

  • Kong, Bo-Kwan;Cho, Dae-Hyun;Yun, Pil-Hwan;Lee, Jeong-Hun;Park, Jin-Young;Park, Ik-Min
    • Journal of Korea Foundry Society
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    • v.35 no.6
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    • pp.155-162
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    • 2015
  • The effect of Sr addition on mechanical and bio-corrosion properties of as-cast Mg-3wt.%Zn-0.5wt.%Ca-xwt.%Sr (x = 0.3, 0.6, 0.9) alloys were examined for application as biodegradable implant material. The microstructure, mechanical properties and corrosion resistance of the as-cast Mg-Zn-Ca-Sr alloys were characterized by using optical microscopy, scanning electron microscopy, tensile testing and electrochemical measurement in Hank's solution. The as-cast alloys contained ${\alpha}$-Mg and eutectic $Ca_2Mg_6Zn_3$ phases, while the alloys contained ${\alpha}$-Mg, $Ca_2Mg_6Zn_3$ and Mg-Zn-Ca-Sr intermetallic compound when the Sr addition was more than 0.3 wt.%. The yield strength, ultimate tensile strength and elongation increased with the increasing of Sr content up to 0.6 wt.% but decreased in the 0.9 wt.% Sr-added alloy, whereas the corrosion resistance of 0.3 wt.% Sr-added alloy was superior to other alloys. It was thought that profuse Mg-Zn-Ca-Sr intermetallic compound deteriorated both the mechanical properties and corrosion resistance of the as-cast alloy.

Analysis of Eutectic Reaction as a Function of Cooling Rate in High Manganese Flake Graphite Cast Irons (고 망간 편상흑연주철에서 냉각속도별 공정반응 분석)

  • Lee, Sang-Hwan;Lee, Hyun-Woo;Lee, Sang-Mok
    • Journal of Korea Foundry Society
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    • v.33 no.4
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    • pp.162-170
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    • 2013
  • The effects of Mn content and cooling rate on the eutectic reaction of flake graphite cast irons were studied by a combined analysis of macro/micro-structure and cooling curve data. The correlation between the eutectic reaction parameter and macro/microstructure was systematically investigated. Two sets of chemical compositions with different Mn contents were designed to cast. Three types of molds for cylindrical specimens with different diameters were prepared to analyze the cooling rate effect. The difference between undercooling temperature and cementite eutectic temperature (${\Delta}T_1=T_U-T_{E,C}$), which is decreased by increasing the Mn content or increasing the cooling rate, is considered to be a suitable eutectic reaction parameter for predicting graphite morphology. According to the criterion, A-type graphite is mainly suggested to form for ${\Delta}T_1$ over $20^{\circ}C$, and D-type graphite is mainly suggested to form for ${\Delta}T_1$ below $0^{\circ}C$. Eutectic reaction time (${\Delta}T$), which is increased by increasing the Mn content and decreased by increasing the cooling rate, is regarded as a suitable eutectic reaction parameter for predicting eutectic cell size. Eutectic cell size is found to decrease in proportion to the decrease of ${\Delta}T$.

The effects of custom tray material on the accuracy of master cast reproduction

  • Kim Hyun-Kyung;Chang Ik-Tae;Heo Seong-Joo;Koak Jai-Young
    • The Journal of Korean Academy of Prosthodontics
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    • v.39 no.3
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    • pp.282-296
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    • 2001
  • The accuracy of master cast reproduction by a polyvinylsiloxane impression material using two visible-light curing resin and autopolymerizing polymethyl methacrylate resin custom tray material was investigated. Custom trays were fabricated from a master cast that had three index points marked on both inner and outer vestibules and then poured in yellow stone. The distance between the reproduced index points were measured to be ${\pm}0.001mm$ with a measuring microscope and the algebraic norms calculated for each tray material. No differences were found in the algebraic norms of inner and outer dimensions for upper tray impressions by ANOVA(p>0.05). However, T-test revealed that there were differences between upper and lower impressions and Tukey's hsd test revealed that in lower tray impressions, the Palatray in inner, the Lightplast in outer dimensions respectively were different from other materials. The index points reproduced on the casts compared with the master cast, were closer together for upper tray impressions. All four tray materials produced acceptable casts, 1. Algebraic norms of inner and outer dimensions of the test casts for upper trays were not statistically different irrespective of materials.(P>0.05) 2. T-test showed that there were differences between means with upper and lower trays especially in outer dimension.(P>0.05) 3. But, algebraic norms of inner and outer dimensions of the test casts for lower trays were statistically different between materials. 4. Palatray XL in inner, Lightplast-platten in outer dimensions respectively for lower trays were different from other materials, but, the nearest to the original model.

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THE DIMENSIONAL CHANGE OF CAST IMPLANT BARS AFTER LABORATORY PROCEDURE

  • Kwon, Ji-Yung;Kim, Chang-Whe;Lim, Young-Jun;Kim, Myung-Joo
    • The Journal of Korean Academy of Prosthodontics
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    • v.45 no.3
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    • pp.354-361
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    • 2007
  • Statement of Problems. The precision of fit between the bearing surfaces of implant abutments and the prosthesis framework has been considered fundamental to implant prosthodontic protocol. Purpose. The study aimed to investigate the effect of laboratory procedure on the dimensional accuracy of cast implant bars. Material and methods Thirty implant bars were fabricated on a metal master model. The gap distances were measured at the right implant abutment replica-gold cylinder interface after casting procedure. The bar length data of precasting and postcasting state were collected and analyzed. Results. The mean gap distance found after casting was $106.3{\mu}m$ for buccal side, $122.1{\mu}m$ for distal side and $117.1{\mu}m$ for the lingual side. The mean bar length was $17964.7{\mu}m$ at precasting measurement, $17891.6{\mu}m$ at postcasting measurement. The mean change of bar length was $-73.1{\mu}m$. Conclusion. Even though the techniques used in this study strictly followed the guidelines established in the literature, the 30 cast implant bars evaluated all yielded gap distances that were beyond acceptable accuracy. There was a statistically significant difference between precasting and postcasting bar length (P<0.01). There was a decreasing tendency in bar length after casting procedure. It was necessary to correct this dimensional change from laboratory procedure by some corrective methods.

Diagnosis of Insulation Deterioration in Cast Resin Transformer Using Method of AE Measurement (음향 방출 측정법을 이용한 몰드변압기 열화진단)

  • Lee, Sang-Woo;Gu, Kyung-Chul;Kim, Seung-Gyu;Kim, In-Sik;Lee, Dong-In;Kim, Ki-Chai;Park, Won-Zoo;Lee, Kwang-Sik
    • Proceedings of the KIEE Conference
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    • 2000.07c
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    • pp.1936-1938
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    • 2000
  • In this paper, a frequency spectra of AE (acoustic emission) signals detected from the partial discharges of an epoxy resin void and a cast resin transformer in operating were analyzed to offer the proper frequency range of AE signals from the corona discharge for the purpose of AE sensor selection, From these results, a frequency spectra of AE signals emitted from the corona discharges in the void of an epoxy resin sample were about 190[kHz] to 220[kHz] by the FFT(fast fourier transform), A frequency spectra of AE signals emitted from a cast. resin transformer with non-load were appeared to be downward of about 140[kHz] by the FFT, and then a frequency spectra of AE signals emitted from the above of cast resin transformer with load were appeared to increase from about 190[kHz] to 220[kHz] by the FFT.

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Maxillomandibular arch width differences at estimated centers of resistance: Comparison between normal occlusion and skeletal Class III malocclusion

  • Koo, Yun-Jin;Choi, Sung-Hwan;Keum, Byeong-Tak;Yu, Hyung-Seog;Hwang, Chung-Ju;Melsen, Birte;Lee, Kee-Joon
    • The korean journal of orthodontics
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    • v.47 no.3
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    • pp.167-175
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    • 2017
  • Objective: To evaluate the differences in maxillomandibular transverse measurements at either the crown or the estimated center of resistance (CR), and to compare values between normal occlusion and Class III malocclusion groups. Methods: Dental casts and computed tomography (CT) data from 30 individuals with normal occlusion and 30 with skeletal Class III malocclusions were evaluated. Using the casts, dental arch widths (DAWs) were measured from the cusp tips, and basal arch widths (BAWs-cast) were measured as the distance between the points at the mucogingival junction adjacent to the respective cusp tips. The BAWs determined from CT (BAWs-CT) images were measured from the estimated CRs of the teeth. Results: None of the DAW measurements or maxillomandibular DAW differences showed statistically significant intergroup differences. In contrast, the maxillary BAWs-CT and BAWs-cast were lesser in the Class III malocclusion group than in the normal occlusion group. The mandibular BAWs-CT were significantly greater in the Class III malocclusion group than in the normal occlusion group. Moreover, the maxillomandibular BAW differences on both CT and cast showed significant intergroup differences in all transverse measurements. Conclusions: The maxillomandibular DAW differences showed no significant intergroup differences. In contrast, the maxillomandibular BAW differences on both CT and cast showed significant intergroup differences in all transverse measurements. The maxillomandibular BAW differences at the estimated CRs, measured using CT or casts, can reveal underlying transverse maxillary basal arch deficiencies in patients with skeletal Class III malocclusions.

Evaluation of biogeneric design techniques with CEREC CAD/CAM system

  • Arslan, Yeliz;Nemli, Secil Karakoca;Gungor, Merve Bankoglu;Tamam, Evsen;Yilmaz, Handan
    • The Journal of Advanced Prosthodontics
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    • v.7 no.6
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    • pp.431-436
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    • 2015
  • PURPOSE. The aim of this study was to evaluate occlusal contacts generated by 3 different biogeneric design modes (individual (BI), copy (BC), reference (BR)) of CEREC software and to assess the designs subjectively. MATERIALS AND METHODS. Ten pairs of maxillary and mandibular casts were obtained from full dentate individuals. Gypsum cast contacts were quantified with articulating paper and digital impressions were taken. Then, all ceramic crown preparation was performed on the left first molar teeth and digital impressions of prepared teeth were made. BI, BC, and BR crowns were designed. Occlusal images of designs including occlusal contacts were superimposed on the gypsum cast images and corresponding contacts were determined. Three designs were evaluated by the students. RESULTS. The results of the study revealed that there was significant difference among the number of contacts of gypsum cast and digital models (P<.05). The comparison of the percentage of virtual contacts of three crown designs which were identical to the contacts of original gypsum cast revealed that BI and BR designs showed significantly higher percentages of identical contacts compared with BC design (P<.05). Subjective assessment revealed that students generally found BI designs and BR designs natural regarding naturalness of fissure morphology and cusp shape and cusp tip position. For general occlusal morphology, student groups generally found BI design "too strong" or "perfect", BC design "too weak", and BR design "perfect". CONCLUSION. On a prepared tooth, three different biogeneric design modes of a CAD/CAM software reveals different crown designs regarding occlusal contacts and morphology.

Management of Earthworm Casts using Pesticides and Tea Tree (Camellia oliefera) Extracts in Turfgrass of Golf Courses (골프장에서 차나무류 추출물과 화학 방제제를 이용한 지렁이 분변토 발생 관리)

  • Shin, Chong Chang;Kim, Jong Kyung;Choi, Sung Hwan;Jeon, Byungduk;Lee, Dong Woon
    • Weed & Turfgrass Science
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    • v.5 no.1
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    • pp.35-41
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    • 2016
  • Earthworm cast is a harmful factor which reduces the uniformity of management of turfgrass and play quality in golf courses and playground. This research was conducted to carry out the efficacy of some pesticide (bifenthrin GR + clothianidin GR, ethoprophos GR, imidacloprid SC, picoxystrobin WG, thiophanate-methyl WP) and tee tree (Camellia oliefera) extracts against reducing earthworm cast in golf courses. All tested materials were acted reducing earthworm cast, thiophanate-methyl among them showed the highest effect reducing earthworm casts in golf courses. Tea tree extracts was occurred similar efficacy among tested chemical pesticides. However, pellet type byproduct of tea seed extract and liquid formulation of tea tree extract were better than granule formulation of them. Byproduct of tea seed and tea tree extract can be used for alternative biological management material for reducing earthworm cast in heavily casting occurrence area.

The Solidification Microstructure of X%C-5%Cr-5%V-5%Mo-5%W-5%Co Multi-Component White Cast Iron (X%C-5%Cr-5%V -5%Mo-5%W-5%Co 다합금계백주철의 응고조직에 관한 연구)

  • Yu, Sung-Kon;Yasuhiro Matsubara
    • Korean Journal of Materials Research
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    • v.11 no.6
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    • pp.472-476
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    • 2001
  • Type and three-dimensional morphology of carbides precipitated in the X(X= 1.70, 1.92, 2.21, 2.50, 2.86)%C-5%Cr-5%V-5%Mo-5%W-5%Co multi-component white cast iron were investigated using an optical microscope and SEM. The types of carbides precipitated were MC, M$_2$C and M$_{7}$C$_{3}$. Morphology of the MC carbide took three forms, that it petal-like, nodular and coral-like. MC carbide seemed to change its morphology from petal-like through nodular, and finally to coral-like with an increase in carbon content. M7C carbide was classified into lamellar and plate-like type. The lamellar M$_2$C arbide precipitated in the iron with low molybdenum and tungsten contents, and higher contents of both elements in the iron were needed to form the plate-like M$_2$C carbide. The morphology of M$_{7}$C$_{3}$ was rod-like similar to that observed in high chromium white cast iron. However, cobalt does not affect the type and morphology of precipitated carbides.des.

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