• Title/Summary/Keyword: carbonized

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Development of Carbon-Ceramic Composites using Fly Ash and Carbon Fibers as Reinforcement

  • Manocha, S.;Patel, Rakesh
    • Carbon letters
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    • v.7 no.1
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    • pp.27-33
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    • 2006
  • Carbon-ceramic composites were fabricated by using fly ash and PANOX fibers as reinforcement. Fly ash, because of its small size particles e.g. submicron to micron level can be effectively dispersed along with fibrous reinforcements. Phenolic resin was used as carbon precursor. Both dry as well as wet methods were used for forming composites. The resulting composites were characterized for their microstructure, thermal and mechanical properties. The microstructure and mechanical properties of composites are found to be dependent on type of the fly ash, fibrous reinforcements as well as processing parameters. The addition of fly ash improves hardness and the fibers, which get co-carbonized on heat treatment, increase the flexural strength of the carbon-ceramic composites. Composites with dual reinforcement exhibit about 30-40% higher strength as compared to the composites made with single reinforcement, either with fly ash as filler or with chopped fibers.

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Preparation of Activated Carbon Fiber from Chemically Modified Coal-tar Pitch

  • Lee, Dong-Jun;Yang, Gap-Seung;Ryu, S.K.;Kim, Y.J.
    • Proceedings of the Korean Fiber Society Conference
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    • 1996.10a
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    • pp.117-123
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    • 1996
  • Cabon fiber of general purpose was prepared from coal tar pitch modified with 10% benzoquinine(BQ) at 380C for 3 hours. Such a modified pitch raised the softening of the pitch from 85C to 271C at the yield of 40%. The modified pitch was spun smoothly at a rate of 480m/min into a fiber of 20um diameter. The fiber was stabilized stepwise at 236C (5C/min) and 312C (1C/min) for 3 hours each. Both carbonized and graphitized fibers exhibited tensile strength of 570MPa which appears large enough as a precursor for active carbon fiber. The activated carbon fiber prepared exhibited relatively high surface area of 2062m2/g at 76% burn-off and rather narrow distribution pore size of 20A.

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Electrochemical Properties of Coal Tar Pitch based MCMB

  • Suh, Jeong-Kwon;Hong, Ji-Sook;Lee, Jung-Min
    • Carbon letters
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    • v.5 no.3
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    • pp.118-126
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    • 2004
  • MCMB (Mesocarbon microbeads) is a kind of anode material for lithium-ion secondary battery. MCMB charge/discharge cycle stability is one of the important criterion at lithium-ion battery operation. In this study, the cycling stability of a lithium-ion secondary battery has been examined. MCMB was made by the direct solvent extraction method. After the MCMB was carbonized and graphitized, the measurement of charge/discharge capacity and efficiency were carried out. In the result, discharge capacity of MCMB in the initial cycle was above 290.0 mAh/g. After the second cycle, efficiency of charge/discharge MCMB was about 98%. These results were similar to the commercial MCMB product.

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Cellulose-based carbon fibers prepared using electron-beam stabilization

  • Kim, Min Il;Park, Mi-Seon;Lee, Young-Seak
    • Carbon letters
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    • v.18
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    • pp.56-61
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    • 2016
  • Cellulose fibers were stabilized by treatment with an electron-beam (E-beam). The properties of the stabilized fibers were analyzed by scanning electron microscopy, Fourier transform infrared spectroscopy, X-ray photoelectron spectroscopy, and thermogravimetric analysis. The E-beam-stabilized cellulose fibers were carbonized in N2 gas at 800℃ for 1 h, and their carbonization yields were measured. The structure of the cellulose fibers was determined to have changed to hemicellulose and cross-linked cellulose as a result of the E-beam stabilization. The hemicellulose decreased the initial decomposition temperature, and the cross-linked bonds increased the carbonization yield of the cellulose fibers. Increasing the absorbed E-beam dose to 1500 kGy increased the carbonization yield of the cellulose-based carbon fiber by 27.5% upon exposure compared to untreated cellulose fibers.

Copper Oxide Growing Characteristics of PVC Insulated Wire and Application to the Fire Investigation (비닐절연전선의 산화물 성장 특성과 화재조사에의 적용)

  • Kim, Hyang-Kon;Choi, Chung-Seog;Kim, Dong-Ook;Choi, Hyo-Sang
    • The Transactions of the Korean Institute of Electrical Engineers P
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    • v.56 no.1
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    • pp.37-44
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    • 2007
  • This paper describes characteristics for copper oxide growth of polyvinyl chloride(PVC) insulated wires by series arc. In this experiment, 600V IV wires were used, and characteristics of oxide growth and ignition process were analyzed in case load was 300W, 460W and 600W, respectively. In the result of experiment, covering materials were molten, carbonized and ignited, whereas, oxidized materials were grown in conducting material. During copper oxide was growing, contact voltages and power dissipations increased. When there is copper oxide growth, the waveform of current showed sinusoidal waveform, and the waveform of voltage showed modified waveform. Oxidized materials were heated at about $905^{\circ}C$, surface structure showed irregular shapes, and cross-section showed multiple cracks. And, the results of this experiment were applied to the fire cause analysis of fire evidence collected at the fire scene.

Carbonization Behavior due to Surface Tracking (연면 트래킹에 의한 탄화 거동)

  • Jung, Yeon-Ha;Jang, Tae-Jun;Shong, Kil-Mok;Roh, Young-Su;Kwak, Hee-Ro
    • Journal of the Korean Institute of Illuminating and Electrical Installation Engineers
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    • v.21 no.2
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    • pp.28-33
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    • 2007
  • In this paper, we are studied on the direction and formation of carbonized conductive path according to surface leakage current between electrodes. The characteristics of the tracking as surface is broken down between exposed live parts. Using the HSIS(high speed imaging system. 100,000[fps], redlake ltd., USA), it took photographs by arc growth mechanism occurred in on/off surge, ground fault and discharge between electrodes. Then the results was analyzed. Hereafter, it expected effects that application of energy utility technology through the arc control.

Vacuum Carbonization of Nanometer Tungsten Powder with Carbon Black

  • Luo, Ji;Lin, Tao;Guo, Zhi-meng;Jia, Chengchang
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.442-443
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    • 2006
  • Vacuum carbonization of nanometer tungsten powder was investigated in a simple designed apparatus. An X-Y recorder was used to plot differential thermal analysis (DTA) curves to determine starting temperature of carbonization of four samples with different specific surface area. The product was detected by X-ray Diffraction (XRD) and small angle X-ray scattering (SAXS). The results show that finer tungsten powder has lower starting temperature of carbonization. Tungsten powder, which BET surface area is $32.97m^2/g$, is completely carbonized to tungsten carbide at $1050^{\circ}C$, although the starting temperature is $865^{\circ}C$. Particle grows sharply before carbonization.

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Electrochemical Properties of Carbonized Phenol Resin (탄화된 페놀레진의 전기화학적 성질)

  • 김한주;박종은;홍지숙;류부형;박수길
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1999.11a
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    • pp.629-632
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    • 1999
  • For replacing Li metal ai Lithium ton Bakery(LIB) system. we used carbon powder material which prepared by pyrolysis of phenol resin as starting material. It became amorphous carbon by pyrolysis through it\`s self condensation by thermal treatment. Amorphous carbon can be doped with Li intercalation and deintercalation because it has wide interlayer. however it has a problem with structural destroy causing weak carbon-carbon bond. So. we used ZnCl$_2$ as the pore-forming agent. This inorganic salt used together with the resin serves not only as the pore-forming agent to form open pores, which grow Into a three-dimensional network structure in the cured material, foul also as the microstructure-controlling agent to form a loose structure dope with bulky dopants. We analyzed SEM in order to find to different of structure. and can calculate distance of interlayer. CV test showed oxidation and reduction

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A Study on the Discrimination of Fire Pattern by the Phenomenological Observation (Focused on the Fire Cases) (현상학적 관찰에 의한 연소패턴의 식별에 관한 연구(사례를 중심으로))

  • Choi, Don-Mook;Choi, Sung-Bok;Choi, Jae-Soung
    • Fire Science and Engineering
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    • v.23 no.6
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    • pp.98-110
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    • 2009
  • The burned patterns of fire are changed very diversely according to the direction of wind, conditions of combustibles, shape of buildings and so on in the fire scenes. And careful attentions are required on the determining of ignition point and fire causes. In this study, we examined that the burned pattern of fuel controlled fires and ventilation controled fires that impose a heavy burden on fire investigators, carbonized marks of floor, formed by flammable liquids, and combustion marks of falling firing materials through the fire cases. We suggest a proper fire investigation method.

iDENTIfyme Informative Campaign: Raising Forensic Dental Identification Awareness in the Community

  • Nuzzolese, Emilio
    • Journal of Preventive Medicine and Public Health
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    • v.54 no.3
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    • pp.218-219
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    • 2021
  • The identification of human remains can be performed visually through families and next-of-kin, but it is not advisable to rely only on visual recognition; instead, it is preferable to conduct a forensic comparison of antemortem and postmortem data for primary identifiers (fingerprints, DNA, and dental data). A dental autopsy is particularly valuable in the identification process of skeletonized, carbonized, saponified, and fragmented human remains. The principal challenge in the identification process is the search and collection of antemortem data. To this end, all dental information held on a missing person can represent a precious source of individualizing information that families should share with the police or investigating agencies after reporting a disappearance.