• Title/Summary/Keyword: calorimeter

Search Result 732, Processing Time 0.035 seconds

Effect of Ohmic Heating on Characteristics of Heating Denaturation of Soybean Protein (옴 가열이 대두 단백질의 열변성에 미치는 영향)

  • Cha, Yun-Hwan
    • The Korean Journal of Food And Nutrition
    • /
    • v.24 no.4
    • /
    • pp.740-745
    • /
    • 2011
  • Ohmic heating uses electric resistance heat which occurs equally and rapidly inside food when an electrical current is passed throught. In this study, we observed the physical & chemical characteristics changes which occurs in soybean protein during heating denaturation by using ohmic and conventional heating. After the ohmic heating process, we could not find any change of the primary protein structure in the denaturated soy protein samples. However, the rate of imbibed water(RIW) of the ohmic samples was 2 times faster than that of the conventional samples. Also the ANS-surface hydrophobicity was decreased, which is very closely related to RIW. In the differential scanning calorimeter(DSC) analysis result, all 7S soyprotein fraction samples were completely denaturated by ohmic and conventional heating. However, the 11S samples were completely denatured only by ohmic heating. According to the DSC result, we decided that soyprotein was damaged by temperature and electrical current during ohmic heating. The damage of electrical current was a cause of the characteristic changes.

열량계 채널에 대한 3차원 열전달 해석

  • Park, Tae-Seon;Seol, Woo-Seok
    • Aerospace Engineering and Technology
    • /
    • v.2 no.2
    • /
    • pp.142-150
    • /
    • 2003
  • Turbulent flows and related heat transfer in a square heated duct is investigated by a turbulence model and a large eddy simulation. The cooling channel of calorimeter is modeled to the square duct. The nonlinear k-ε-fμ model of Park et al. [3] is slightly modified and their explicit heat flux model is employed. The Reynolds number is varied in the range 4000≤Reb≤20000. The heat transfer is closely linked to the secondary flows which driven by the turbulent motion. Its magnitude is 1~3% of the mean streamwise velocity. The relation of Nu~Re0.8Pr0.34 is validated by comparing with the predicted Nu of k-ε-fμ model. Finally, the coherent structures and thermal fluctuations are scrutinized.

  • PDF

Comparative Analysis of Gross Calorific Value by Determination Method of Lignocellulosic Biomass Using a Bomb Calorimeter

  • Ju, Young Min;Ahn, Byung-Jun;Lee, Jaejung
    • Journal of the Korean Wood Science and Technology
    • /
    • v.44 no.6
    • /
    • pp.864-871
    • /
    • 2016
  • This study was conducted to compare and analyze gross calorific values from measurement methods of lignocellulosic biomass and calculation data from calorific value prediction models based on the elemental content. The deviation of Liriodendron tulipifera (LT) and Populus euramericana (PE) was shown 7.7 cal/g and 7.4 cal/g respectively in palletization method, which are within repeatability limit 28.8 cal/g of ISO FDIS 18125. In the case of Thailand charcoal (TC), nontreatment method and palletization method was satisfied with repeatability limit as 22.8 cal/g and 8.8 cal/g respectively. Seowon charcoal (SC) was shown deviation of 11.4 cal/g in nontreatment method, because the density and chemical affinity of sample increases as the carbon content increases from heat treatment at high temperature in the case of TC and SC. In addition, after applying the elemental content of each of these samples to the calorific value prediction models, the study found that Model Equation (3) was relatively consistent with measured calorific values of all these lignocellulosic biomass. Thus, study about the correlation between the density and size of particle should be conducted in order to select the measurement method for a wide range of solid biofuels in the future.

Ignition Characteristics and Combustion Gas Analysis of the Plastics Foam (발포 프라스틱의 착화특성 및 연소가스 분석)

  • 이근원;김관응
    • Journal of the Korean Society of Safety
    • /
    • v.16 no.1
    • /
    • pp.48-52
    • /
    • 2001
  • This study was undertaken to investigate fire risk characteristics of the plastics foam that is used an insulating materials in workplaces. The ignition characteristics and combustion gas of the plastics foam were carried out using the ISO self-Ignition tester, the Cone Calorimeter, and NES combustion analyzer. The experimental materials used were commercial samples and their composition is not disclosed by the manufacturer. As the experimental results, the self-ignition temperature of the plastics foam ranges from $410^{\circ}C$ to $510^{\circ}C$, and the flash-ignition temperature of plastics foam ranges from $370^{\circ}C$ to $450^{\circ}C$. The difference of ignition temperature on density with plastics foam type was smaller since the amount of combustible gas to ignite is not caused enough. The time to ignition of the polyethylene foam in samples of the plastics foam was shorter, and its of polyethylene foam was longer. The concentration of carbon dioxide of the polyethylene foam shows higher in samples of the plastics foam. It is found that the concentration values of carbon monoxide of the plastics foam show very fatality on people during exposure of 30 minutes in fire.

  • PDF

Study on Flame Retardancy and Thermal Resistance Properties of Phenolic Foam and Polyurethane Foam (페놀 폼과 폴리우레탄 폼의 난연 및 내열성 연구)

  • Lee, Ju-Chan;Seo, Jung-Seok;Kim, Sang Bum
    • Journal of the Korean Institute of Gas
    • /
    • v.17 no.1
    • /
    • pp.35-41
    • /
    • 2013
  • In this study, flame retardancy of polyurethane foam and phenolic foam were investigated by addition of phosphorous flame retardants. The thermal degradation behavior of polyurethane foam and phenolic foam in the presence of flame retardants has been studied by thermogravimetric analysis(TGA). Heat release rate(HRR), mean HRR, mass loss rate(MLR), total smoke released(TSR) and limited oxygen index(LOI) were tested by cone calorimeter. From the test results, Phenolic foam showed low HRR, MLR and TSR than polyurethane foam.

Characteristics of Thermal Hazard in Methylthioisocyanate Synthesis Reaction Process (Methylthioisocyanate 합성반응 공정의 열적위험 특성)

  • Han, In-Soo;Lee, Keun-Won;Lee, Joo-Yeob
    • Journal of the Korean Society of Safety
    • /
    • v.27 no.5
    • /
    • pp.77-87
    • /
    • 2012
  • Compared to a batch reactor, where all reactants are initially charged to the reactor, the semi-batch reactor presents serious advantages. The feed of at least one of the reactants provides an additional way of controlling the reaction course, which represents a safety factor and increases the constancy of the product quality. The aim of this study was to investigate the characteristics of thermal hazard such as a feed time, catalysis concentration and solvent concentration in methylthioisocyanate(MTI) synthesis reaction process. The experiments were carried out by the Multimax reactor system and Accelerating rate calorimeter(ARC). The MTI synthesis reaction process has many reaction factors and complicated reaction mechanism of multiphase reaction. Through this study, we can use as a tool for assessment of thermal hazard of other reaction processes by applying experiment method provided.

A Study on the Combustion Characteristics of Useful Imported Wood for Building Materials - Focusing on the North American species (Douglas-fir, Western Red cedar) and African species(Makore, Padauk, Bubinga) - (국내 유용 건축자재용 수입 목재의 연소특성에 관한 연구 - 북미 산재(Douglas-fir, Western Red cedar)와 아프리카 산재 (Makore, Padauk, Bubinga)를 중심으로 -)

  • Seo, Hyun Jeong;Baek, Jong Kyo;Lee, Min Chul
    • Journal of the Korean Society of Safety
    • /
    • v.32 no.3
    • /
    • pp.8-14
    • /
    • 2017
  • This study examined the combustion and thermal characteristics of imported woods for building materials in Korea. Wooden specimens were confirmed by a cone calorimeter according to the KS F ISO 5660-1 standard. The combustion properties of the wooden specimens were measured in terms of the heat release rate (HRR), total heat released (THR), mass lose rate (MLR), and ignition time (time to ignition; TTI). The optical microscope was used for determine the anatomical characteristics of wood pit and structure. Also, the thermal properties were measured by thermogravimetric analysis (TGA) to determine the thermal stability of wooden specimens. The result of this experiment would be useful for fundamentals of guiding the combustion properties and thermal stability using wood application.

A Study for the Fire Retardant-Characteristics of Expandable Graphite Composite Materials (팽창흑연을 사용한 복합재료의 난연 특성에 관한 연구)

  • Chun, Kwan-Ok;Rie, Dong-Ho
    • Journal of the Korean Society of Safety
    • /
    • v.32 no.3
    • /
    • pp.28-33
    • /
    • 2017
  • In this study, the composite material of expandable graphite was made to the material development for improving such as a composite material of the sandwich panels or material properties of a fire door and was tested by the ISO 1182, ISO 5660-1(Cone calorimeter Method). For the test, the composite material of expandable graphite, what the expandable graphite ratio was increased by respectively 0g~30g, was classified A1,A2, A3, A4, and made to the test specimens. Through cone calorimeter test, peak heat release rate(HRR) and total heat release(THR), expanded thickness and expansion rate of each composite material of expandable graphite, and fire prone crack and mass loss rate after burning was measured. Thus, the effect of the addition of the expandable graphite and whether is suitable for reference as a fire retardant, was analyzed. Consequently the correlation of THR and fire retardant performance rate was confirmed.

Determination of Enthalpy in the High Temperature Test Facility (고온 시험장치에서의 엔탈피 결정)

  • Na, Jae-Jeong;Lee, Jung-Min;Kang, Kyung-Taik
    • Proceedings of the Korean Society of Propulsion Engineers Conference
    • /
    • 2011.11a
    • /
    • pp.224-227
    • /
    • 2011
  • In order to determine the enthalpy profile in the high temperature transpiration cooling test facility for the air-breating engine compartments, theoretical calculation and measurement for the flow of the test section are performed. The mass averaged enthalpy value determined by the heat balance and sonic throat methods is 10 MJ/kg. The centerline enthalpy value measured using the slug type copper calorimeter is 15 MJ/kg. Typically, the ratio of centerline and mass averaged enthalpy should be varies from 1.4 to 4. This facility has lower bound of enthalpy profile. It will be effective in testing of high temperature transpiration cooling.

  • PDF

Controlled Release of Retinol Containing Microcapsules Prepared by Solvent Evaporation Method (액중건조법으로 제조한 Retinol 함유 마이크로캡슐의 방출 거동)

  • Kim, Se Ra;Shin, Young Jae;Lee, Chun Il;Pyo, Hyeong Bae;Shin, Jae Sup
    • Journal of Adhesion and Interface
    • /
    • v.9 no.2
    • /
    • pp.1-7
    • /
    • 2008
  • Using biodegradable polycaprolactone, the microcapsules were prepared by solvent evaporation method. Retinol was selected as a core material, which was used as an important ingredient material in cosmetic fields. Poly(vinyl alcohol) was used as a stabilizer. The shape and property of the microcapsules were characterized by scanning electron microscope and differential scanning calorimeter, and the release rate of the microcapsule was measured by UV spectrophotometer. The microcapsules were prepared, changing the concentration of wall material, the stirring rate, and the concentration of stabilizer. Under the optimum condition, the microcapsules were formed, which showd 5~6 um in diameter and got the homogeneous sphere shape.

  • PDF