• Title/Summary/Keyword: bonding surface

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Constructability of a Waterproofing Sheet Joint Combining an Aluminum Thin-film and Viscosity Layer Using a High-frequency Inductive Heating Apparatus (고주파 유도가열 장치를 이용한 알루미늄 박판 점착 복합방수시트 조인트부의 시공성)

  • Chang, Sang Mook;Kim, Yun Ho;Choi, Sung Min
    • Journal of the Korea Institute of Building Construction
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    • v.14 no.2
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    • pp.163-169
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    • 2014
  • Engineers in the construction field have been using bonded waterproofing sheets in an attempt to resolve the imbalance in the quality, the risk of fire, safety of workers, and environmental pollution, as well as to eliminate separate use of organic adhesives on the surface of concrete. Recently, self-laminated waterproofing sheets have been developed. The purpose of this research is to find an appropriate processing speed according to the changes in physical properties, and visual observation of the waterproofing sheets laminated by the aluminum thin-film and viscosity layer that can be attached through self-adhesiveness on the surface of concrete and waterproofing sheets. Therefore, this research is conducted using a physical performance test. Based on the result of the test, when the high-frequency inductive heating apparatus was used, an improved adhesion and bonding stability effect were confirmed after the anti-hydrostatic pressure and bond strength in the temperature condition, and the surface observation in the processing speed condition.

Properties of ZnO thin film grown on $Al_2O_3$ substrate pretremented by nitrogen ion beam (이온빔으로 질화처리된 사파이어기판위에 성장한 ZnO박막의 특성)

  • Park, Byung-Jun;Jung, Yeon-Sik;Park, Jong-Young;Choi, Du-Jin;Choi, Won-Kook;Yoon, Seok-Jin
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2004.07a
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    • pp.413-416
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    • 2004
  • In this study, zinc oxide(ZnO) having large misfit(18.2%) with sapphire was tried to be grown on very thin nitride buffer layers. For the creation of various kinds of nitride buffer layer, sapphire surface was modified by an irradiation of nitrogen ion beam with low energy generated from stationary plasma thruster(SPT) at room temperature. After the irradiation of ion beam, Al-N and Al-O-N bonding was identified to be formed as nitride buffet layers. Surface morphology was measured by AFM and then ZnO growth was followed by pulsed laser deposition(PLD). Their properties are analyzed by XRD, AFM, TEM, and PL. We observed that surface morphology was improved and deep level emission related to defects was almost vanished in PL spectra from the ZnO grown on nitride buffer layer.

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Fabrication of Porous Electrodes for Zinc-Ion Supercapacitors with Improved Energy Storage Performance (아연-이온 전기화학 커패시터의 에너지 저장 성능향상을 위한 다공성 전극 제조)

  • An, Geon-Hyoung
    • Korean Journal of Materials Research
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    • v.29 no.8
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    • pp.505-510
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    • 2019
  • Zn-ion supercapacitors (ZICs) show high energy densities with long cycling life for use in electronic devices. Porous Zn electrodes as anodes for ZICs are fabricated by chemical etching process using optimized conditions. The structures, morphologies, chemical bonding states, porous structure, and electrochemical behavior are examined. The optimized porous Zn electrode shows a root mean square of roughness of 173 nm and high surface area of $153{\mu}m^2$. As a result, ZIC using the optimized porous Zn electrode presents excellent electrochemical performance with high specific capacitance of $399F\;g^{-1}$ at current density of $0.5A\;g^{-1}$, high-rate performance ($79F\;g^{-1}$ at a current density of $10.0A\;g^{-1}$), and outstanding cycling stability (99 % after 1,500 cycles). The development of energy storage performance using synergistic effects of high roughness and high surface area is due to increased electroactive sites by surface functionalization of Zn electrode. Thus, our strategy will lead to a rational design and contribute to next-generation supercapacitors in the near future.

Prediction of Bending Fatigue Life of Cracked Out-of-Plane Gusset Joint Repaired by CFRP Plates

  • Matsumoto, Risa;Komoto, Takafumi;Ishikawa, Toshiyuki;Hattori, Atsushi;Kawano, Hirotaka
    • International journal of steel structures
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    • v.18 no.4
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    • pp.1284-1296
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    • 2018
  • Carbon fiber reinforced polymer (CFRP), plates bonding repair method is one of the simple repair methods for cracked steel structures. In this study, the influence of width of CFRP plates on bending fatigue life of out-of-plane gusset joint strengthened with CFRP plates was investigated from the experimental and numerical point of view. In the bending fatigue test of cracked out-of-plane gusset joint strengthened with CFRP plates, the effect of width of CFRP plates on crack growth life was clarified experimentally. Namely, it was revealed that the crack growth life becomes larger with increasing the width of CFRP plates. In the numerical approach, the stress intensity factor (SIF) at the surface point of a semi-elliptical surface crack was estimated based on the linear fracture mechanics. Furthermore, the extended fatigue life of cracked out-of-plane gusset joint strengthened with CFRP plates was evaluated by using the estimated SIF at the surface point and the empirical formula of the aspect ratio of semi-elliptical crack. As the results of numerical analysis, the estimated fatigue life of the specimen strengthened with CFRP plates showed the good agreement with the test results.

Analysis of Wafer Cleaning Solution Characteristics and Metal Dissolution Behavior according to the Addition of Chelating Agent (착화제 첨가에 따른 웨이퍼 세정 용액 특성 분석 및 금속 용해 거동)

  • Kim, Myungsuk;Ryu, Keunhyuk;Lee, Kun-Jae
    • Journal of Powder Materials
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    • v.28 no.1
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    • pp.25-30
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    • 2021
  • The surface of silicon dummy wafers is contaminated with metallic impurities owing to the reaction with and adhesion of chemicals during the oxidation process. These metallic impurities negatively affect the device performance, reliability, and yield. To solve this problem, a wafer-cleaning process that removes metallic impurities is essential. RCA (Radio Corporation of America) cleaning is commonly used, but there are problems such as increased surface roughness and formation of metal hydroxides. Herein, we attempt to use a chelating agent (EDTA) to reduce the surface roughness, improve the stability of cleaning solutions, and prevent the re-adsorption of impurities. The bonding between the cleaning solution and metal powder is analyzed by referring to the Pourbaix diagram. The changes in the ionic conductivity, H2O2 decomposition behavior, and degree of dissolution are checked with a conductivity meter, and the changes in the absorbance and particle size before and after the reaction are confirmed by ultraviolet-visible spectroscopy (UV-vis) and dynamic light scattering (DLS) analyses. Thus, the addition of a chelating agent prevents the decomposition of H2O2 and improves the life of the silicon wafer cleaning solution, allowing it to react smoothly with metallic impurities.

A Study on Non-contact Surface Temperature Field Measurement of a Body Immerged in Water Using Thermographic Phosphor Thermometry (열감지인광온도계를 이용한 물에 잠긴 물체 표면 온도장의 비접촉식 측정에 관한 연구)

  • Park, Yoonseong;Cai, Tao;Kim, Kyung Chun
    • Journal of the Korean Society of Visualization
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    • v.18 no.3
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    • pp.61-68
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    • 2020
  • Thermographic phosphor (TP) thermometry is a noncontact optical measurement method and has been applied in many fields such as combustion and heat transfer. However, due to the limitation of bonding technology and measurement method, most TP thermometry studies were conducted only on the air environment with water-soluble binders. In this paper, a temperature measurement technology in water using TP is proposed by coatings of manganese activated magnesium fluorogermanate (Mg4FGeO6:Mn4+, MFG) with Polydimethylsiloxane (PDMS). Four MFG-PDMS coatings with different thicknesses were prepared. The lifetime of MFG was not affected by the thickness of the coating as a result of the experiment and analysis of phosphor intensity using a photomultiplier tube. To measure the surface temperature field of an immerged body in water, a cylinder-type cartridge heater was coated with MFG doped PDMS. Transient surface temperature field was successfully measured even the initial temperature is higher than the boiling point of water.

Experimental study on damage and debonding of the frozen soil-concrete interface under freeze-thaw cycles

  • Liyun Tang;Yang Du;Liujun Yang;Xin Wang;Long Jin;Miaomiao Bai
    • Structural Engineering and Mechanics
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    • v.86 no.5
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    • pp.663-671
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    • 2023
  • Freeze-thaw cycles induce strength loss at the frozen soil-concrete interface and deterioration of bonding, which causes construction engineering problems. To clarify the deterioration characteristics of the interface under the freeze-thaw cycle, a frozen soil-concrete sample was used as the research object, an interface scanning electron microscope test under the freeze-thaw cycle was carried out to identify the micro index information, and an interface shear test was carried out to explore the loss law of interface shear strength under the freeze-thaw cycle. The results showed that the integrity of the interface was destroyed, and the pore number and pore size of the interface increased significantly with the number of freeze-thaw cycles. The connection form gradually deteriorates from surface-to-surface contact to point-to-surface contact and point-to-point contact, and the interfacial shear strength decreases the most at 0-3 freeze-thaw cycles, with small decreases from to 3-8 cycles. After 12 freeze-thaw cycles, the interfacial shear strength tends to be stable, and shear the failure occurs internally in the soil.

Study on the effect of vacuum fusion infiltration technology on the properties of tungsten/copper joining interface

  • Hao-Jie Zhang;Xue-qin Tian;Xiao-Yu Ding;Hui-Yun Zheng;Lai-Ma Luo;Yu-Cheng Wu;Jian-Hua Yao
    • Nuclear Engineering and Technology
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    • v.56 no.6
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    • pp.2367-2374
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    • 2024
  • In this paper, based on the need for high-strength connections between all-tungsten-oriented plasma materials and thermal sinking materials of copper and its alloys in nuclear fusion devices, a study on the effect of tungsten surface laser micro structuring on the interfacial bonding properties of W/Cu joints was carried out. In the experiment, the connectors were prepared by vacuum fusion infiltration technology, and the effects of microgroove structure on the mechanical and thermal conductivity of W/Cu connectors were investigated under different parameters (including microgroove pitch, microgroove depth, and microgroove taper). The maximum shear strength is 126.0 MPa when the pitch is 0.15 mm and the depth is 34 ㎛. In addition, the negative taper structure, i.e., the width of the entrance of the microstructure is smaller than the width of the interior of the microstructure, is also investigated. The shear tests show that there is an approximately linear relationship between the shear strength of W/Cu and taper. Compared with the positive taper, the shear strength of the samples with the same morphological density and depth of the tungsten surface is significantly higher.

Evaluation of Adhesion Characteristics of Crack Sealants Used in Asphalt Concrete Pavement (아스팔트 콘크리트 포장용 균열실링재의 부착특성 평가)

  • Lee, Jae-Jun;Kim, Seung-Hoon;Baek, Jong-Eun;Lim, Jae-Kyu;Kim, Yong-Joo
    • International Journal of Highway Engineering
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    • v.17 no.2
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    • pp.55-62
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    • 2015
  • Cracking is an inevitable fact of asphalt concrete pavements and plays a major role in pavement deterioration. Pavement cracking is one of the main factors determining the frequency and method of repair. Cracks can be treated with a number of preventative maintenance actions, including overlay surface treatments such as slurry sealing, crack sealing, or crack filling. Pavement cracks can show up as one or all of the following types: transverse, longitudinal, fatigue, block, reflective, edge, and slippage. Crack sealing is a frequently used pavement maintenance treatment because it significantly extends the pavement service life. However, crack sealant often fails prematurely due to a loss of adhesion. Because current test methods are mostly empirical and only provide a qualitative measure of the bond strength, they cannot accurately predict the adhesive failure of the sealant. This study introduces a laboratory test aimed at assessing the bonding of hot-poured crack sealant to the walls of pavement cracks. A pneumatic adhesion tensile testing instrument (PATTI) was adopted to measure the bonding strength of the hot-poured crack sealant as a function of the curing time and temperature. Based on a limited number of test results, the hot-poured crack sealants have very different bonding performances. Therefore, this test method can be proposed as part of a newly developed performance-based standard specification for hot-poured crack sealants for use in the future. PURPOSES : The purpose of this study was to evaluate both the adhesion and failure performance of a crack sealant as a function of its curing time and curing temperature. METHODS: A pneumatic adhesion tensile testing instrument (PATTI) was adopted to measure the adhesion performance of a crack sealant as a function of the curing time and curing temperature. RESULTS: With changes in the curing time, curing temperature, and sealant type, the bond strengths were found to be significantly different. Also, higher bond strengths were measured at lower temperatures. Different sealant types produced completely different bond strengths and failure behaviors. CONCLUSIONS: The bonding strength of an evaluated crack sealant was shown to differ depending on various factors. Two sealant types, which were composed of different raw materials, were shown to perform differently. The newly proposed test offers the possibility of evaluating and differentiating between different crack sealants. Based on alimited number of test results, this test method can be proposed as part of a newly developed performance-based standard specification for crack sealants or as part of a guideline for the selection of hot-poured crack sealant in the future.

A STUDY ON THE EFFECTS OF THE TEMPERATURE AND HUMIDITY TO THE TENSILE BOND STRENGTH BETWEEN GLASS-IONOMER CEMENT AND COMPOSITE RESIN (온도 및 습도가 Glass-ionomer cement와 Composite resin의 접착강도에 미치는 변화에 관한 연구)

  • Chung, Inn-Gyo;Min, Byung-Soon
    • Restorative Dentistry and Endodontics
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    • v.16 no.1
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    • pp.60-73
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    • 1991
  • The purpose of this study is to evaluate the effects of etching time, environmental temperature and humidity on the adhesion of composite resin to glass-ionomer cement. Two chemical cure composite resins (Clearfil F II and Microrest AP) and two glass-ionomer cements (Fuji ionomer Type I and KET AC-CEM) were used as the experimental materials. The experiment is performed in 3 stages: The first stage is to bond composite resins to glass-ionomer cements, and the surface was not etched, and etched for 20 seconds, 40 seconds, and 60 seconds. Then specimens are stored in distilled water at $37^{\circ}C$ for 24 hours to measure tensile strength. The second stage is to choose the one group that had the highest tensile strength from the first stage and prepare two experimental groups: One group with composite resin bonded to glass-ionomer cement without etching and bonding agent application and the other with composite resin bonded to glass-ionomer cement with etching but without any bonding agent application. The specimens are stored in distilled water at $37^{\circ}C$ for 24 hours and tensile strength is measured. The third stage is to choose group that had the highest tensile strength from the first stage experiment, and bond composite resin to glass-ionomer cement at $24^{\circ}C$ 44%, $30^{\circ}C$ 44%, $30^{\circ}C$ 80%, and $32^{\circ}C$ 92%. The storage time of specimens is to bond immediately after storage, then changed to 30 sec., 60 sec., and 120 sec.. Specimens are stored in distilled water at $37^{\circ}C$ for 24 hours and their tensile strength are measured again. The following results were obtained: 1. As the etching time increases, the tensile bond strength between glass-ionomer cement and composite resin increase, and the tensile bond strength is the highest when acid etched for 60 minutes (P < 0.05). 2. After acid etching for 60 minutes, the tensile strength of the group with bonding agent was stronger than that without bonding agent application (P < 0.05). 3. The tensile strength of Clearfil F II was stronger than that of Microrest AP. 4. It was observed that the tensile bond strength is not affected by different storage time with different temperature and humidity. 5. As the humidity was increased, the tensile bond strength between glass-ionomer cement and composite resin decreased (P < 0.05).

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