• 제목/요약/키워드: bonding surface

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A Study on the Adaptability and Cytotoxicity of Porcelain Bonded Ni-Cr Alloy (도재소부용 Ni-Cr합금의 적합성과 세포독성에 관한 연구)

  • Choi, Boo-Byung;Shin, Myung-Chull
    • The Journal of Korean Academy of Prosthodontics
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    • v.20 no.1
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    • pp.7-17
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    • 1982
  • In order to investigate the internal adaptability and cytotoxicity for porcelain fused to metal Ni-Cr alloy, two commercial alloys (Generic Gold-R alloy, Aalba Dent- Valloy)were employed and compared with new developed beryllium free Ni-Cr alloy (KIST-K alloy). After cementation of each crown to abutment die before and after ceramic bonding respectively, dies were mounted to epoxy resin and the internal space was measured between crown and die of each point on sagittal section. The results were as follows: 1) The results show that the space between the crown and the die was largest at the incisal edge, followed by the shoulder or the bevel and chamfer. The least was to be in the axial surface. 2) There were no significant difference in the adaptability of the compared alloys. 3) On day 2 of the experiment the cell multiplication was slightly inhibited by R and K alloys. However, observations taken at day 4 and 7 showed normal cell multiplication process compared to control group. 4) Alloy V exhibited the most severe cell toxicity among the alloys tested on day 2. By day 4 and 7 it showed a decrease level in toxicity, however it did not exhibit normal cell growth as compared to control group.

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Guided wave field calculation in anisotropic layered structures using normal mode expansion method

  • Li, Lingfang;Mei, Hanfei;Haider, Mohammad Faisal;Rizos, Dimitris;Xia, Yong;Giurgiutiu, Victor
    • Smart Structures and Systems
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    • v.26 no.2
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    • pp.157-174
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    • 2020
  • The guided wave technique is commonly used in structural health monitoring as the guided waves can propagate far in the structures without much energy loss. The guided waves are conventionally generated by the surface-mounted piezoelectric wafer active sensor (PWAS). However, there is still lack of understanding of the wave propagation in layered structures, especially in structures made of anisotropic materials such as carbon fiber reinforced polymer (CFRP) composites. In this paper, the Rayleigh-Lamb wave strain tuning curves in a PWAS-mounted unidirectional CFRP plate are analytically derived using the normal mode expansion (NME) method. The excitation frequency spectrum is then multiplied by the tuning curves to calculate the frequency response spectrum. The corresponding time domain responses are obtained through the inverse Fourier transform. The theoretical calculations are validated through finite element analysis and an experimental study. The PWAS responses under the free, debonded and bonded CFRP conditions are investigated and compared. The results demonstrate that the amplitude and travelling time of wave packet can be used to evaluate the CFRP bonding conditions. The method can work on a baseline-free manner.

Evaluation of AR Characteristics on Microscopic Fracture Mechanism of A17075/CERP Hybrid Composite (Al 7075/CFRP 하이브리드 복합재료의 미시적 파괴특성에 대한 AE특성평가)

  • 이진경;이준현;윤한기
    • Composites Research
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    • v.15 no.5
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    • pp.1-6
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    • 2002
  • When compared to other composite materials such as FRP and MMC, hybrid composite material is more attractive one due to the high specific strength and the resistance to fatigue. However, the fracture mechanism of hybrid composite material is extremely complicated because of the bonding structure of metals and FRP. Recently, nondestructive technique has been used to evaluate the fracture mechanism of these composite materials. In this study. AE technique has been used to clarify the fracture mechanism and the degree of damage for Al 7075/CFRP hybrid composite material. It was found that AE event, energy and amplitude among AE parameters were effective to evaluate fracture process of Al 7075/CFRP composite material. In addition, the relationship between the AE signal and the characteristics of failure surface using optical microscope was discussed.

Fatigue Life Prediction of Composite Patch for Edge Cracked Aluminum Plate (모서리균열이 있는 알루미늄판의 복합재 패치보수시 수명예측 연구)

  • Kim, Wie-Dae
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.35 no.1
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    • pp.52-57
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    • 2007
  • One of the hot issues in composite patching is to reduce the thermal residual stresses between composite patch and aluminum surface which occurs after bonding of composite patch. In this study, the edge crack patching is adopted for different curing cycles. For the analysis, three layer Mindlin plate elements are used, and Paris' law is adopted to predict the fatigue life of composite patch plate. The analysis results show a good agreement with the experimental fatigue life and this technique can be applied for the prediction of fatigue life of aircraft structures.

Development of MEMS based Piezoelectric Inkjet Print Head and Its Applications

  • Shin, Seung-Joo;Lee, Hwa-Sun;Lee, Tae-Kyung;Kim, Sung-Jin
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2010.05a
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    • pp.20.2-20.2
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    • 2010
  • Recently inkjet printing technology has been developed in the areas of low cost fabrication in environmentally friendly manufacturing processes. Although inkjet printing requires the interdisciplinary researches including development of materials, manufacturing processes and printing equipment and peripherals, manufacturing a printhead is still core of inkjet technology. In this study, a piezoelectric driven DOD (drop on demand) inkjet printhead has been fabricated on three layers of the silicon wafer in MEMS Technology because of its chemical resistance to industrial inks, strong mechanical properties and dimensional accuracy to meet the drop volume uniformity in printed electronics and display industries. The flow passage, filter and nozzles are precisely etched on the layers of the silicon wafers and assembled through silicon fusion bonding without additional adhesives. The piezoelectric is screen-printed on the top the pressure chamber and the nozzle plate surface is treated with non-wetting coating for jetting fluids. Printheads with nozzle number of 16 to 256 have been developed to get the drop volume range from 5 pL to 80 pL in various industrial applications. Currently our printheads are successfully utilized to fabricating color-filters and PI alignment layers in LCD Flat Panel Display and legend marking for PCB in Samsung Electronics.

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A study on etch Characteristics of $CeO_2$ thin Film in an $Ar/CF_{4}/Cl_{2}$ Plasma ($Ar/CF_{4}/Cl_{2}$ 플라즈마에 의한 $CeO_2$ 박막의 식각 특성 연구)

  • Chang, Yun-Seong;Chang, Eui-Goo;Kim, Chang-Il;Lee, Cheol-In;Kim, Tae-Hyung;Eom, Joon-Chul
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2001.11b
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    • pp.217-220
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    • 2001
  • The possibility of cerium dioxide $(CeO_2)$ thin films as insulators of metal erroelectric insulator semiconductor (MFIS) structures have been studied. The etching $CeO_2$ thin films have been perfonned in an inductively coupled $Cl_{2}/CF_{4}/Ar$ plasma. The high etch rate of the $CeO_2$ thin film was $250\AA /m$ at a 10 % addition of $Cl_2$ into the $Ar(80)/CF_{4}(20)$. The surface reaction of the etched $CeO_2$ thin films was investigated using X-ray photoelectron spectroscopy (XPS) analysis. There are Ce-Cl and Ce-F bonding by chemical reaction between Cl, F and Ce. These products can be removed by the physical bombardment of incident Ar ions.

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Mechanical Properties of Carbon Fiber/Nylon 6 Composite Introducing Coupling Agent (II) -Increasing Interfacial Strength of Composite- (카플링제를 도입한 탄소섬유/나일론 6 복합재료의 기계적 성질(II) -복합재료의 계면강도 증가-)

  • Park, Chan Hun;Lee, Yang Hun;Shin, Eun Joo
    • Textile Coloration and Finishing
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    • v.9 no.4
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    • pp.47-53
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    • 1997
  • To improve the interfacial bonding of carbon fiber-nylon 6 composite, carbon fiber(CF) were oxidized by nitric acid treatment, and two types of graft polymer(GP) of nylon 6-g-polyacrylamide (PAAm) -water dispersable GP(WDGP) and m-cresol solu ble GP(CSGP) were treated as coupling agents. Introduction of polar groups such as -COOH, -OH, etc, on the surface of the oxidized CF was confirmed by IR spectra. The stem polymer of nylon 6 in the coupling agent (GP) could be compatible with'matrix nylon 5, and the grafted branch of PAAm on GP could react to the polar groups on the oxidized CF in composite. The interfacial strength was measured by the transverse tensile test to the fiber direction for single CF embedded nylon 6 film especially prepared and by the pull-out test method. The interfacial strength of the composite reinforced with oxidized CF is greater than that reinforced with unoxidized CF. The interfacial strength of the composite was increased by treatment of coupling agents(GPs) considerably, and the increasing tendency by the WDGP is greater than that by the CSGP. The optimum conditions of coupling agent treatment are as follows: the concentration, adsorption tlme of GP, and curing temperature are 2%, 20 minutes, and $170^{\circ}$, respectively.

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Electrochemical Behavior of Well-dispersed Catalysts on Ruthenium Oxide Nanofiber Supports (루테늄 산화물 나노 섬유 지지체에 담지된 고 분산성 촉매의 전기화학적 거동)

  • An, Geon-Hyoung;Ahn, Hyo-Jin
    • Journal of Powder Materials
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    • v.24 no.2
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    • pp.96-101
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    • 2017
  • Well-dispersed platinum catalysts on ruthenium oxide nanofiber supports are fabricated using electrospinning, post-calcination, and reduction methods. To obtain the well-dispersed platinum catalysts, the surface of the nanofiber supports is modified using post-calcination. The structures, morphologies, crystal structures, chemical bonding energies, and electrochemical performance of the catalysts are investigated. The optimized catalysts show well-dispersed platinum nanoparticles (1-2 nm) on the nanofiber supports as well as a uniform network structure. In particular, the well-dispersed platinum catalysts on the ruthenium oxide nanofiber supports display excellent catalytic activity for oxygen reduction reactions with a half-wave potential ($E_{1/2}$) of 0.57 V and outstanding long-term stability after 2000 cycles, resulting in a lower $E_{1/2}$ potential degradation of 19 mV. The enhanced electrochemical performance for oxygen reduction reactions results from the well-dispersed platinum catalysts and unique nanofiber supports.

Structure & Mechanical Behavior of TiCN Thin Films by rf Plasma Deposition (RF Plasma법으로 증착된 TiCN박막의 구조 및 기계적 거동에 관한 연구)

  • Baeg, C.H.;Park, S.Y.;Hong, J.W.;Wey, M.Y.;Kang, H.J.
    • Journal of the Korean Society for Heat Treatment
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    • v.13 no.2
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    • pp.91-97
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    • 2000
  • The structure and mechanical properties of TiN and TiCN thin films deposited on STD61 steel substrates by the RF-sputtering methods has been studied by using XPS, XRD, micro-hardness tester, scratch tester, and wear-resistance tester. XPS results showed that the TiCN thin film formed with chemical bonding state. The TiN thin films grew with (111) orientation having the lowest strain energy by compressive stress, whereas the TiCN thin films grew with both (111) and (200) orientation, but (200) orientation having the lowest surface energy becomes dominant as carbon contents increase. The pre-etching treatment of substrate did not affect on the preferred orientation of thin films, but it played an important role in improving mechanical properties of thin films such as the hardness, adhesion and wear- resistance. Especially, the TiCN thin films showed the superior wear resistances due to high hardness and low friction coefficient compared with TiN thin films.

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Flexural Characteristics of Coir Fiber Reinforced Cementitious Composites

  • Li Zhi-Jian;Wang Li-Jing;Wang Xungai
    • Fibers and Polymers
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    • v.7 no.3
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    • pp.286-294
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    • 2006
  • This study has examined the flexural properties of natural and chemically modified coir fiber reinforced cementitious composites (CFRCC). Coir fibers of two different average lengths were used, and the longer coir fibers were also treated with a 1% NaOH solution for comparison. The fibers were combined with cementitious materials and chemical agents (dispersant, defoamer or wetting agent) to form CFRCC. The flexural properties of the composites, including elastic stress, flexural strength, toughness and toughness index, were measured. The effects of fiber treatments, addition of chemical agents and accelerated ageing of composites on the composites' flexural properties were examined. The results showed that the CFRCC samples were 5-12 % lighter than the conventional mortar, and that the addition of coir fibers improved the flexural strength of the CFRCC materials. Toughness and toughness index, which were associated with the work of fracture, were increased more than ten times. For the alkalized long coir fiber composites, a higher immediate and long-term toughness index was achieved. SEM microstructure images revealed improved physicochemical bonding in the treated CFRCC.