• Title/Summary/Keyword: bonding material

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Thermodynamic Comparison of Silicon Carbide CVD Process between CH3SiCl3-H2 and C3H8-SiCl4-H2 Systems (탄화규소 CVD 공정에서 CH3SiCl3-H2과 C3H8-SiCl4-H2계의 열역학적 비교)

  • Choi, Kyoon;Kim, Jun-Woo
    • Korean Journal of Metals and Materials
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    • v.50 no.8
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    • pp.569-573
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    • 2012
  • In order to understand the difference in SiC deposition between the $CH_3SiCl_3-H_2$ and $C_3H_8-SiCl_4-H_2$ systems, we calculate the phase stability among ${\beta}$-SiC, graphite and silicon. We constructed the phase-diagram of ${\beta}$-SiC over graphite and silicon via computational thermodynamic calculation considering pressure (P), temperature (T) and gas composition (C) as variables. Both P-T-C diagrams showed a very steep phase boundary between the SiC+C and SiC region perpendicular to the H/Si axis, and also showed an SiC+Si region with a H/Si value of up to 6700 in the $C_3H_8-SiCl_4-H_2$, and 5000 in the $CH_3SiCl_3-H_2$ system. This difference in phase boundaries is explained by the ratio of Cl to Si, which is 4 for the $C_3H_8-SiCl_4-H_2$ system and 3 for the $C_3H_8-SiCl_4-H_2$ system. Because the C/Si ratio is fixed at 1 in the $CH_3SiCl_3-H_2$ system while it can be variable in the $C_3H_8-SiCl_4-H_2$ system, the functionally graded material is applicable for better mechanical bonding during SiC coating on graphite substrate in the $C_3H_8-SiCl_4-H_2$ system.

Mechanical properties of expanded polystyrene beads stabilized lightweight soil

  • Li, Mingdong;Wen, Kejun;Li, Lin;Tian, Anguo
    • Geomechanics and Engineering
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    • v.13 no.3
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    • pp.459-474
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    • 2017
  • To investigate the mechanical properties of Expanded Polystyrene (EPS) Beads Stabilized Lightweight Soil (EBSLS), Laboratory studies were conducted. Totally 20 sets of specimens according to the complete test design were prepared and tested with unconfined compressive test and consolidated drained triaxial test. Results showed that dry density of EBSLS ($0.67-1.62g/cm^3$) decreases dramatically with the increase of EPS beads volumetric content, while increase slightly with the increase of cement content. Unconfined compressive strength (10-2580 kPa) increases dramatically in parabolic relationship with the increase of cement content, while decreases with the increase of EPS beads volumetric content in hyperbolic relationship. Cohesion (31.1-257.5 kPa) increases with the increase of cement content because it is mainly caused by the bonding function of hydration products of cement. The more EPS beads volumetric content is, the less dramatically the increase is, which is a result of the cohesion between hydration products of cement and EPS beads is less than that between hydration products of cement and sand particles. Friction angle ($14.92-47.42^{\circ}$) decreases with the increase of EPS beads volumetric content, which is caused by the smoother surfaces of EPS beads than sand grains. The stress strain curves of EBSLS tend to be more softening with the increase of EPS beads content or the decrease of cement content. The shear contraction of EBSLS increases with the increase of $c_e$ or the decrease of $c_c$. The results provided quantitative relationships between physico-mechanical properties of EBSLS and material proportion, and design process for engineering application of EBSLS.

Evaluation of Adhesion Performance of High-Fireproofing Alumino-silicate Inorganic Mortar (알루미노 실리케이트계 고내화성 모르타르의 부착성능 평가)

  • Cho, Hyeon-Seo;Lee, Gun-Cheol
    • Journal of the Korea Institute of Building Construction
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    • v.18 no.6
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    • pp.569-576
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    • 2018
  • In modern society, a huge number of the buildings have been constructed with RC structure. RC structures have many structural instabilities due to earthquake, typhoon, construction fault, design phase errors. Therefore, many reinforcement methods are being implemented to solve this problem. In the reinforcement method, the organic epoxy adhesive used in the FRP reinforcing method is abruptly damaged when exposed to high temperature, which is directly connected to the fall of the reinforcing material. Therefore, the present study was conducted to develop inorganic refractory mortar with a certain level of adhesion ability to reduce the heat transferred to FRP reinforcement when exposed to high temperatures. As a result of the test, it showed high adhesion strength at room temperature condition with the inclusion of EVA resin, and showed no performance deterioration up to about $300^{\circ}C$ even under heating conditions. Also, it was confirmed that the backside temperature was lower as the thickness increased, and converged to a constant temperature of about $780^{\circ}C$ after 2 hours of heating.

Development of the Splint Manufacturing Process Using Indirect Coating and Roll Bonding (간접 코팅과 롤 접합을 이용한 의료용 스플린트 제작 및 공정기술 개발)

  • Ha, Kyoung-Ho;Kang, Dae-Min;Lee, Jung-Hee;Kwak, Jae-Seob
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.18 no.2
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    • pp.1-6
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    • 2019
  • With the increase in number of the athletic population and elderly demographic, the demand for orthopedic splints, which are used to support a damaged body, has rapidly increased. Current splints mainly consist of inner and outer parts, which are multiple fabrics covered with polyurethane and nonwoven fabrics, respectively. However, the laminated materials with directly applied pre-polymer coating lead to a high defect rate because of the uneven thickness on the surface. Thus, this study proposes an indirect coating method using a precise clearance controller, which enables the even application of the coating material on multiple inner parts while maintaining a constant thickness. In addition, a roll-to-roll (R2R) technique is applied instead of the sewing mechanism to bond the inner and outer materials together and enhance the productivity in the final stage. In the advanced methods, there is a storage tank that contains polyurethane, a clearance controller, and pairs of rollers in the upper and lower rows. To improve the quality of the products and optimize the equipment, three controllable factors are determined: the viscosity of polyurethane, angle of the gap controller and number of pairs of rollers in the R2R system.

Development of Ply-Lam Composed of Japanese Cypress Laminae and Korean Larch Plywood

  • FUJIMOTO, Yoshiyasu;TANAKA, Hiroshi;MORITA, Hideki;KANG, Seog Goo
    • Journal of the Korean Wood Science and Technology
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    • v.49 no.1
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    • pp.57-66
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    • 2021
  • In recent years, the use of cross laminated timber (CLT) has been evolving. In addition, CLT manufactured with various species such as Japanese cedar has been developed to utilize the local resources in each country. However most factories in Japan produce CLT by bonding the laminae in width direction for orthogonal layers, where grain of element is perpendicular to the grain of outer layer, and this process is considered to be one of the factors that reduce productivity. A new wood based material (hereinafter referred to as Ply-lam) using wooden panel such as plywood for the orthogonal layer was developed in order to improve productivity in CLT manufacturing and improve quality. Japanese cypress lamina was used for the parallel layer, where grain of element is parallel to the grain of outer layer, of CLT and Korean larch plywood was used for the orthogonal layer, in order to effectively use Korean larch and expand the utilization of Japanese cypress. The cross-sectional construction of the Ply-lam was 5-layers 5-plies, and the dimensions were 1000 mm (width) × 150 mm (depth) × 4000 mm (length). As a performance evaluation of the manufactured Ply-lam, strength tests such as out-of-plane bending, in-plane bending, out-of-plane shearing and in-plane shearing tests were carried out. As the result of this study, Ply-lam composed of Japanese cypress lamina panels and Korean larch plywood showed very higher out-of-plane bending strength compared to the standard strength of CLT. And the result obtained in other tests seems to show a sufficiently high value.

Tensile Strength Application Using a Definitive Screening Design Method in Friction Stir Welding of Dissimilar Cast Aluminum and High-Strength Steel with Pipe Shape (파이프 형상의 이종 주조알루미늄-고장력강의 마찰교반용접에서 확정선별설계법에 의한 인장강도 응용)

  • Choy, Lee-jon;Park, Seong-Hwan;Lee, Myung-Won;Park, Jae-Ha;Choi, Byeong-Joon
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.19 no.10
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    • pp.98-104
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    • 2020
  • Recently, friction stir welding of dissimilar materials has become one of the biggest issues in lightweight and eco-friendly bonding technology. In this study, a lightweight torsion beam axle, which is an automobile chassis component, was used in the welding to cast aluminum material. The friction stir welding process of A357 cast aluminum and FB590 high-strength steel as well as the effects of the process parameters were investigated and optimized using a novel definitive screening design (DSD). ANOVA was used to predict the importance of the process parameters with 13 degradation experiments using the proposed DSD. Also, FSWed experiments were conducted using an optical microscope analysis to investigate the tensile strength behavior in the weld area. In addition to determining the interaction between the tool's rotational speed and the plunge speed, results indicate that the influence of the plunge depth was the most significant.

A Study on Selective Transfer and Reflow Process of Micro-LED using Micro Stamp (마이크로 스탬프를 이용한 Micro-LED 개별 전사 및리플로우 공정에 관한 연구)

  • Han, Seung;Yoon, Min-Ah;Kim, Chan;Kim, Jae-Hyun;Kim, Kwang-Seop
    • Tribology and Lubricants
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    • v.38 no.3
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    • pp.93-100
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    • 2022
  • Micro-light emitting diode (micro-LED) displays offer numerous advantages such as high brightness, fast response, and low power consumption. Hence, they are spotlighted as the next-generation display. However, defective LEDs may be created due to non-uniform contact loads or LED alignment errors. Therefore, a repair process involving the replacement of defective LEDs with favorable ones is necessitated. The general repair process involves the removal of defective micro-LEDs, interconnection material transfer, as well as new micro-LED transfer and bonding. However, micro-LEDs are difficult to repair since their size decreases to a few tens of micron in width and less than 10 ㎛ in thickness. The conventional nozzle-type dispenser for fluxes and the conventional vacuum chuck for LEDs are not applicable to the micro-LED repair process. In this study, transfer conditions are determined using a micro stamp for repairing micro-LEDs. Results show that the aging time should be set to within 60 min, based on measuring the aging time of the flux. Additionally, the micro-LEDs are subjected to a compression test, and the result shows that they should be transferred under 18.4 MPa. Finally, the I-V curves of micro-LEDs processed by the laser and hot plate reflows are measured to compare the electrical properties of the micro-LEDs based on the reflow methods. It was confirmed that the micro-LEDs processed by the laser reflow show similar electrical performance with that processed by the hot plate reflow. The results can provide guidance for the repair of micro-LEDs using micro stamps.

Experimental study of graphene oxide on wollastonite induced cement mortar

  • Sairam, V.;Shanmugapriya, T.;Jain, Chetan;Agrahari, Himanshu Kumar;Malpani, Tanmay
    • Advances in concrete construction
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    • v.12 no.6
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    • pp.479-490
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    • 2021
  • Present research is mainly focused on, microstructural and durability analysis of Graphene Oxide (GO) in Wollastonite (WO) induced cement mortar with silica fume. The study was conducted by evaluating the mechanical properties (compressive and flexural strength), durability properties (water absorption, sorptivity and sulphate resistance) and microstructural analysis by SEM. Cement mortar mix prepared by replacing 10% ordinary portland cement with SF was considered as the control mix. Wollastonite replacement level varied from 0 to 20% by weight of cement. The optimum replacement of wollastonite was found to be 15% and this was followed by four sets of mortar specimens with varying substitution levels of cementitious material with GO at dosage rates of 0.1%, 0.2%, 0.3% and 0.4% by weight. The results indicated that the addition of up to 15%WO and 0.3% GO improves the hydration process and increase the compressive strength and flexural strength of the mortar due to the pore volume reduction, thereby strengthening the mortar mix. The resistance to water penetration and sulphate attack of mortar mixes were generally improved with the dosage of GO in presence of 15% Wollastonite and 10% silica fume content in the mortar mix. Furthermore, FE-SEM test results showed that the WO influences the lattice framework of the cement hydration products increasing the bonding between silica fume particles and cement. The optimum mix containing 0.3% GO with 15% WO replacement exhibited extensive C-S-H formation along with a uniform densified structure indicating that calcium meta-silicate has filled the pores.

A machine learning-based model for the estimation of the critical thermo-electrical responses of the sandwich structure with magneto-electro-elastic face sheet

  • Zhou, Xiao;Wang, Pinyi;Al-Dhaifallah, Mujahed;Rawa, Muhyaddin;Khadimallah, Mohamed Amine
    • Advances in nano research
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    • v.12 no.1
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    • pp.81-99
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    • 2022
  • The aim of current work is to evaluate thermo-electrical characteristics of graphene nanoplatelets Reinforced Composite (GNPRC) coupled with magneto-electro-elastic (MEE) face sheet. In this regard, a cylindrical smart nanocomposite made of GNPRC with an external MEE layer is considered. The bonding between the layers are assumed to be perfect. Because of the layer nature of the structure, the material characteristics of the whole structure is regarded as graded. Both mechanical and thermal boundary conditions are applied to this structure. The main objective of this work is to determine critical temperature and critical voltage as a function of thermal condition, support type, GNP weight fraction, and MEE thickness. The governing equation of the multilayer nanocomposites cylindrical shell is derived. The generalized differential quadrature method (GDQM) is employed to numerically solve the differential equations. This method is integrated with Deep Learning Network (DNN) with ADADELTA optimizer to determine the critical conditions of the current sandwich structure. This the first time that effects of several conditions including surrounding temperature, MEE layer thickness, and pattern of the layers of the GNPRC is investigated on two main parameters critical temperature and critical voltage of the nanostructure. Furthermore, Maxwell equation is derived for modeling of the MEE. The outcome reveals that MEE layer, temperature change, GNP weight function, and GNP distribution patterns GNP weight function have significant influence on the critical temperature and voltage of cylindrical shell made from GNP nanocomposites core with MEE face sheet on outer of the shell.

Banana agriculture waste as eco-friendly material in fibre-reinforced concrete: An experimental study

  • Mohammed M., Attia;Abd Al-Kader A., Al Sayed;Bassam A., Tayeh;Shymaa M.M., Shawky
    • Advances in concrete construction
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    • v.14 no.5
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    • pp.355-368
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    • 2022
  • This paper investigates the impact of length and volume fractions (VFs) of banana fibres (BFs) on the mechanical and physical properties of concrete. The mechanical properties were compressive strength, splitting tensile, flexural strength, and bond stress, while the physical properties were unit weight and absorption. The slump test was used to determine workability. The concrete's behaviour with BFs was studied using scanning electron microscopy. Experimental work of concrete mixtures with BFs of various lengths (12 mm, 25 mm, and 35 mm) and VFs (0%, 0.5%, 1.0%, and 1.5%) were carried out. The samples did not indicate any agglomeration of fibres or heterogeneity during mixing. The addition of BFs to concrete with VFs of up to 1.50% for all fibre lengths have a significant impact on mechanical properties, also the longer fibres performed better than shorter ones at all volume fractions of BFs. The mix10, which contain BFs with VFs 1.5% and length 35 mm, demonstrated the highest mechanical properties. The compressive strength, splitting tensile, flexural strength, and bond stress of the mix10 were 37.71 MPa, 4.27 Mpa, 6.12 MPa, and 6.75 MPa, an increase of 7.37%, 20.96%, 24.13%, and 11.2% over the reference concrete, which was 35.12 MPa, 3.53 MPa, 4.93 MPa, and 6.07 MP, respectively. The absorption is increased for all lengths by increasing the VFs up to 1.5%. Longer fibres have lower absorption, while shorter fibres have higher absorption. The mix8 had the highest absorption of 4.52%, compared to 3.12% for the control mix. Furthermore, the microstructure of concrete was improved through improved bonding between the fibres and the matrix, which resulted in improved mechanical properties of the composite.