• Journal of Mechanical Science and Technology
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• v.18 no.9
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• pp.1604-1613
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• 2004

This paper presents an effective and reliable evaluation method for fracture strength and material degradation of the micro-structure of high temperature service steel weldment using advanced small punch (ASP) test developed from conventional small punch (CSP) test. For the purpose of the ASP test, a lower die with a minimized ${\Phi}$1.5 mm diameter loading ball and an optimized deformation guide hole of ${\Phi}$3 mm diameter were designed. The behaviors of fracture energy (E$\_$sp/), ductile-brittle transition temperature (DBTT) and material degradation from the ASP test showed a definite dependency on the micro-structure of weldment. Results obtained from ASP test were compared and reviewed with results from CSP test, Charpy impact test, and hardness test. The utility and reliability of the proposed ASP test were verified by investigating fracture strength, behavior of DBTT, and fracture location of each micro-structure of steel weldment for test specimen in ASP test. It was observed that the fracture toughness in the micro-structure of FL＋CGHAZ and ICHAZ decreased remarkably with increasing aging time. From studies of all micro-structures, it was observed that FGHAZ microstructure has the most excellent fracture toughness, and it showed absence of material degradation.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2005.11a
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• pp.340-341
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• 2005

Lithium titanium oxide as anode material for energy storage prepared by novel synthesis method. $Li_4Ti_5O_{12}$ based spinel-framework structures are of great interest material for lithium-ion batteries. We describe here $Li_4Ti_5O_{12}$ a zero-strain insertion material was prepared by novel sol-gel method and by high energy ball milling (HEBM) of precursor to from nanocrystalline phases. According to the X-ray diffraction and scanning electron microscopy analysis, uniformly distributed $Li_4Ti_5O_{12}$ particles with grain sizes of 100nm were synthesized. Lithium cells, consisting of $Li_4Ti_5O_{12}$ anode and lithium cathode showed the 173 mAh/g in the range of 1.0 $\sim$ 3.0 V. Furthermore, the crystalline structure of $Li_4Ti_5O_{12}$ didn't transfer during the lithium intercalation and deintercalation process.

• Journal of the Korean Society of Industry Convergence
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• v.17 no.1
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• pp.7-14
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• 2014

In this study, characteristic of elastic paving materials in bicycle road using polyurethane were studied experimentally. As a results, following their good result was obtained. Bicycle road packaging materials are flexural strength g test, ratio of mass change after freezing and thawing, repulsion elasticity test, water Permeation coefficient test and slip resistance test results showed good performance.

• Proceedings of the Korean Society of Machine Tool Engineers Conference
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• 1997.04a
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• pp.1-5
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• 1997

The plane surface rolling, one of the plastic working process, good surface condition due to increase of surface roughness and hardness. It is well known that mechanism of surface rolling depends upon rolling conditions such as rolling speed, contact pressure, step length of rolling, the shape of roller and mechanical properties of material. In this study, the optimal value of the above parameter on the surface roughness were investigated by using the rolling tool with NACHI 6000ZZ ball bearing outer races on machine structure carbon steel[SM45C]

• Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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• 2001.05a
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• pp.1130-1135
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• 2001

This paper investigated the dynamic performance of HDD disk-spindle system to reduce disk fluttering. Rocking frequencies of the disk-spindle system and radial NRRO are measured to escape the ball defect frequencies and to determine the relative optimal position of the disk in the motor. It was found that disk fluttering was reduced by increasing disk thickness, inserting viscoelastic material between the disk and the spacer and decreasing the gap between the disk and the base.

• Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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• 1999.11a
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• pp.84-93
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• 1999

Sliding friction and wear tests for silicon nitride(Si$_3$N$_4$) was carried out with a ball-on-disk specimen configuration. The material used in this study was HIPed silicon nitride. The tests was carried out from room temperature to 1000"I with self mated couples of slicon nitride in laboratory air. Worn surfaces were observed by SEM and debris particles from worn surfaces were analyzed degree of oxidation by XPS. XPS.

• Journal of the Korean Geosynthetics Society
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• v.9 no.1
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• pp.47-57
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• 2010

Granular soils having a large particle size have been used as a filling material in the construction of foundation, harbor, dam, and so on. Consequently, the shear behavior of this granular soil plays a key role in respect of stability of structures. For example, soil particle crushing occurring at the interface between structure and soil and/or within soil mass can cause a disturbance of ground characteristics and consequently induce issues in respect of stability of structures. In order to investigate the shear behavior according to an existence and nonexistence of particle crushing, numerical analyses were conducted by using the DEM (Discrete Element Method)-based software program PFC2D (Particle Flow Code). By dividing soil particle bonding model into crushing model and noncrushing model, total four particle bonding models were simulated and their results were compared. Noncrushing model included one ball model and clump model, and crushing model included cluster model and Lobo-crushing model. The combinations of soil particle followed the research results of Lobo-Guerrero and Vallejo (2005) which were composed of eight circles. The results showed that the friction angle was in order of clump model > cluster model > one ball model. The particle bonding model compared to one ball model and noncrushing model compared to crushing model showed higher shear strength. It was also concluded that the model suggested by Lobo-Guerrero and Vallejo (2005) is not appropriate to simulate the soil particle crushing.

• Carbon letters
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• v.8 no.4
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• pp.326-334
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• 2007

In this study, graphite composites were fabricated by warm press molding method to realize commercialization of PEM fuel cells. Graphite composites have been considered as alternative economic materials for bipolar plate of PEM fuel cells. Graphite powder that enables to provide electrical conductivity was selected as the main substance. The graphite powder was mixed with phenolic resin and the mixture was pressed using a warm press method. First of all, the graphite powder was pulverized with a ball mill for the dense packing of composite. As the ball milling time increases, the average size of particles decreases and the size distribution becomes narrow. This allows for improvement of the uniformity of graphite composite. However, the surface electrical resistivity of graphite composite increases as the ball milling time increases. It is due to that graphite particles with amorphous phase are generated on the surface due to the friction and collision of particles during pulverizing. We found that the contact electrical resistivity of graphite particles increases as the particle size decreases. The contact electrical resistivity of graphite powders was reduced due to high molding pressure by warm press molding. This leads to improvement of the mechanical properties of graphite composite. Hydrogen gas impermeability was measured with the graphite composite, showing a possibility of the application for bipolar plate in fuel cell. And, I-V curves of the graphite composite bipolar plate exhibit a similar performance to the graphite bipolar plate.

• Tribology and Lubricants
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• v.38 no.1
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• pp.15-21
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• 2022

Diamond reinforced Cr-based coating has been proposed as wear-resistant materials. In this study, the friction and wear characteristics of diamond reinforced Cr-based coating are experimentally assessed. The experiments are performed using a pin-on-reciprocating plate tribo-tester under various normal forces with boundary lubrication. The stainless-steel ball is used as a counter material. Prior to the experiments, mechanical properties such as elastic modulus and hardness are determined using nanoscale instrumented indentation. The hardness of the specimen is further determined using a Vickers hardness tester. The specimens before and after the experiments are carefully observed using a confocal microscope to understand the wear characteristics. In addition, the wear volume and wear rate of the specimens are determined based on the confocal microscope data. The results show that the friction coefficients are 0.096-0.100 under 20-40 N normal forces. Furthermore, the wear rates of the diamond reinforced Cr-based coating and the stainless steel ball under 20-40 N normal forces are found to be 12.8 × 10^-8 mm³/(Nm)-15.5 × 10^-8 mm³/(Nm) and 1.9 × 10^-8 mm³/(Nm)-3.9 × 10^-8 mm³/(Nm), respectively. However, the effect of the normal force on wear rates is not clearly observed, which may be associated with the flattening of the ball. The results of the study may be useful for the tribological applicability of diamond reinforced Cr-based coating as wear-resistant materials.

• Journal of the Korean Society for Precision Engineering
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• v.11 no.1
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• pp.89-96
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• 1994

This study is to develop a new composite material, a mixture of epoxy resin and granite aggergates which is called Expoxy-Granite, to overcome the inherent disadvantages of conventional materials commonly used as a bed structure material of long-term dimensional/ thermal stability. Under the various manufacturing conditions which could be formulated through experimental investigation, we have constructed 6 kinds of Epoxy-Granite structure models having one fifth the size of the ultra-precision machine tool bed structure. They are compared with cast iron and pure granite models through the dynamic test and the thermal deformation test. Both in the steel ball dropping test and in the forced vibration test, three types of epoxy-granite models made in this study have shown much better dynamic characteristics than the cast iron model and almost the same characteristics as compared with the pure granite model. In the thermal deformation test the above composite materials have also represented lower thermal displacements in the vertical direction of each model as compared with other specimens. It is therefore seen that the epoxy-granite complsite material can be applied to the construction of high-precision machine tool bed, instead of cast iron or pure granite.