• 대한약학회:학술대회논문집
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• 대한약학회 2003년도 Proceedings of the Convention of the Pharmaceutical Society of Korea Vol.2-2
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• pp.213.2-213.2
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• 2003

A simple analytical procedure using FT-NIR for the rapid determination of individual ingredients was evaluated. Direct measurements were made by reflection using a reflectance accessory, by transmittance using tablet accessory and turn table. FT-NIR spectral data were transformed to the first derivative. Partial Least Square Regression(PLSR) was applied to quantify near-infrared (NIR) spectra of 2 ingredients. These calibration models were cross-validated (leave-one-out approach). The prediction ability of the models was evaluated on ambroxol tablets and compared with the real values in manufacturing procedure. (omitted)

• Industrial Engineering and Management Systems
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• 제4권2호
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• pp.165-175
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• 2005

Two extreme and one mixed procedures for designing a noise hazard prevention program are discussed in this paper. The two extreme design procedures (engineering-based and HPD-based) yield upper and lower bounds of the total noise control cost, respectively; while the mixed design procedure provides an optimal noise hazard prevention program within a given total budget. The upper bound of the workforce size for job rotation is approximated using a heuristic procedure. Six optimization models are developed and utilized by the mixed procedure to eliminate or reduce excessive noise levels (or noise exposures) in an industrial workplace. The mixed procedure also follows the OSHA’s hierarchy of noise control. A numerical example is given to demonstrate the application of the proposed design procedures.

• 대한전자공학회논문지SD
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• 제41권2호
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• pp.9-15
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• 2004

본 논문에서는 부분공핍(partially-depleted : PD) 영역과 완전공핍(fully-depleted : FD) 영역을 나누는 임계 전면 게이트 전압 V/sub c/의 해석적 표현을 이용해서 PD 영역과 FD 영역의 천이를 정확히 설명하는 해석적 표면전위 모델(analytical surface potential model)을 소개한다. 이 모델은 모든 동작영역(subthreshold에서 strong inversion까지)에서 유효하고 반복 계산 절차 (iteration procedure)인 수치 해석적 방법보다 훨씬 짧은 계산시간이 걸린다. 이 모델에 기초한 charge sheet 모델이 모는 동작영역에 유효한 드레인 전류의 단일 공식을 유도하는데 사용된다. 대부분의 secondary 효과들이 charge sheet 모델에 쉽게 포함되고 그 모델의 결과들은 수치해석 결과와 실험 결과를 비교적 정확히 일치한다. 세 가지의 smoothing 함수가 사용될지 라도 표면전위 미분 값은 연속이다 더욱 중요한 점은 smoothing 함수에 사용된 파라미터들은 공정 파라미터들에 크게 의존하지 않는다.

• Structural Engineering and Mechanics
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• 제35권1호
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• pp.99-117
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• 2010

Beam-column joints are the key structural elements, which dictate the behavior of structures subjected to earthquake loading. Though large experimental work has been conducted in the past, still various issues regarding the post-yield behavior, ductility and failure modes of the joints make it a highly important research topic. This paper presents experimental results obtained for eight beam-column joints of different sizes and configuration under cyclic loads along with the analytical evaluation of their response using a simple and effective analytical procedure based on nonlinear static pushover analysis. It is shown that even the simplified analysis can predict, to a good extent, the behavior of the joints by giving the important information on both strength and ductility of the joints and can even be used for prediction of failure modes. The results for four interior and four exterior joints are presented. One confined and one unconfined joint for each configuration were tested and analyzed. The experimental and analytical results are presented in the form of load-deflection. Analytical plots are compared with envelope of experimentally obtained hysteretic loops for the joints. The behavior of various joints under cyclic loads is carefully examined and presented. It is also shown that the procedure described can be effectively utilized to analytically gather the information on behavior of joints.

• 분석과학
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• 제23권6호
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• pp.551-559
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• 2010

본 연구는 칼럼 전 유도체화와 HPLC-형광검출을 이용해 염소 소독 음용수 중 7가지 nitrosamine 화합물을 분석하는 방법을 추출 과정(액-액 추출 vs. 고상 추출)과 형광 유도체화 과정(denitrosation 및 dansylation)으로 나누어 평가하여 확립하였다. 최적화된 유도체화 방법으로 두 가지의 추출법을 비교하였을 때, Ambersorb 572를 이용한 고상 추출에 대한 회수율과 재현성(상대표준편차, RSD)이 각각 54.4-88.7%와 1.9-19.4%로 액-액 추출의 51.4-87.7%와 4.2-33.3%에 비해 더 좋게 나타났다. 확립된 방법은 기존의 HPLC를 이용한 분석 방법에 비해 회수율과 재현성 모두 개선되었으며, 방법검출한계(method detection limits, MDLs)는 0.5-4.4 ng/L이었다. 이 방법으로 춘천의 염소로 소독하는 두 곳의 정수장과 10 곳의 수도꼭지에서 채취한 물 시료 중 nitrosamine 화합물을 분석한 결과, N-nitrosodimethylamine (NDMA)이 주요 화합물이었으며, 농도 범위는 26.1-112 ng/L이었다.

• 한국자동차공학회논문집
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• 제9권2호
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• pp.107-115
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• 2001

It is required more precise analysis for practical load because of complexities and varieties of vehicle structure. To establish the numerical model, many researchers have been developed designing tools for linking F.E. Analysis results and experimental results. There studies have generally focused on each experimental method or analytical method separately. There are few studies based on both methods. This paper conceives new procedure for the determination of the load direction and magnitude applied on mechanical structures. New procedure is the combination of the analytical and empirical method with analyzed strain by F.E. Analysis under unit load and with measured principal stress by strain gages under driving load, respectively. In this paper, we theorize the procedure of practical load determination and make the validity and the practicality of the procedure with the application to T-shape jointed structure. F.E. Analysis is conducted to get the principal stress on arbitrary points in the F.E. model of T-shape joint under unit load. Then experiment is carried out to get the principal stress on the same points of F.E. model. To demonstrate the actual driving condition, the load conditions are bending and torsion. From these two data sets, the magnitude, the direction and the position of load can be obtained. Theory and practice do not always coincide; since there are some errors such as ill-poseness, measuring error and modeling error in experimental data, we examine the proper method of error minimization.

• 정보처리학회논문지C
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• 제19C권2호
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• pp.153-166
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• 2012

모바일 네트워크에서 멀티캐스트서비스의 이용량 증가로 MN(이동단말)에게 끊김없이 멀티캐스트 서비스를 전송하는 통신이 중요한 통신 형태가 요구될 것이다. 본 논문에서 IETF에서 표준화가 진행중인 PMIPv6(Proxy Mobile IPv6)에서 MLS(Multicast Listener Support)에 대한 현재의 문제점을 지적하고, 네트워크 기반의 이동성관리 기법인 PMIPv6 네트워크에서 도메인간 고속 멀티캐스트 핸드오버 절차를 제안한다. 제안된 도메인간 고속 멀티캐스트 핸드오버 절차에서는 MN의 컨텍스트를 사용하여 멀티캐스트 관리를 최적화한다. 제안된 고속 멀티캐스트 핸드오버 절차를 기본적인 것과 해석 모델링을 통하여 비교분석하고, 도메인간 핸드오버의 경우에 제안된 도메인간 고속 멀티캐스트 핸드오버 절차가 기본적인 것과 비교하여 서비스 단절 시간과 전체 네트워크 오버해드가 상당히 감소한다는 것을 보여준다.

• Mass Spectrometry Letters
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• 제7권2호
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• pp.31-40
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• 2016

The analysis of nuclear materials and environmental samples is an important issue in nuclear safeguards and nuclear forensics. An analysis technique for safeguard samples has been developed for the detection of undeclared nuclear activities and verification of declared nuclear activities, while nuclear forensics has been developed to trace the origins and intended use of illicitly trafficked nuclear or radioactive materials. In these two analytical techniques, mass spectrometry has played an important role in determining the isotope ratio of various nuclides, contents of trace elements, and production dates. These two techniques typically use similar analytical instruments, but the analytical procedure and the interpretation of analytical results differ depending on the analytical purpose. The isotopic ratio of the samples is considered the most important result in an environmental sample analysis, while age dating and impurity analysis may also be important for nuclear forensics. In this review, important aspects of these techniques are compared and the role of mass spectrometry, along with recent progress in related technologies, are discussed.

• Journal of Korean Society for Atmospheric Environment
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• 제20권E1호
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• pp.29-33
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• 2004

In environmental studies, decisions are often made on the analytical data indicating certain contaminants as being 'detected' or 'non-detectible.' Since detection limits are analytical method specific, one has to first review the concepts and definitions associated with analytical method systems and specifications. In this study, the experimental analytical values for a series of low level standards (for an ionic species) were used as an example to estimate two different method detection limits (MDL). The scores of EPA's MDL and Pallesen's MDL determined by real analytical scores are 0.0575 and 0.0561 mg/L, respectively for our nitrate data. These scores determined by two different MDL models are roughly similar, while there are apparent differences between two methods with respect to statistical and systematical procedure. However, determination of MDL for one's laboratory provides some practical applications which helps to assure one's regulating authorities that one's measured scores are accurate.

• JSTS:Journal of Semiconductor Technology and Science
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• 제2권1호
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• pp.59-69
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• 2002

A semi-analytical model based on exact numerical analysis of the 2DEG channel in pseudo-morphic HEMT (PMHEMT) is presented. The exactness of the model stems from solving both Schrodinger's wave equation and Poisson's equation simultaneously and self-consistently. The analytical modeling of the device terminal characteristics in relation to the charge control model has allowed a best fit with the geometrical and structural parameters of the device. The numerically obtained data for the charge control of the channel are best fitted to analytical expressions which render the problem analytical. The obtained good agreement between experimental and modeled current/voltage characteristics and small signal parameters has confirmed the validity of the model over a wide range of biasing voltages. The model has been used to compare both the performance and characteristics of a PMHEMT with a competetive HEMT. The comparison between the two devices has been made in terms of 2DEG density, transfer characteristics, transconductance, gate capacitance and unity current gain cut-off frequency. The results show that PMHEMT outperforms the conventional HEMT in all considered parameters.