• Membrane Journal
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• v.6 no.3
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• pp.141-156
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• 1996

For ultra-pure water, the removal of various impirities is required, and the requirement level is rising year by year. To cope with this problem, various removing technologies and system technologies have been developed and the introduction of new materials for the piping, etc. to form the system have been positively made. For the element technologies to be used for ultra-pure water production, their range will be expanded from the technological and economic viewpoints. Therefore, it is absolutely necessary to develop trace analysis evaluation technologies for ultra-pure water. Especially to raise the analytical level of heavy metals and organic substances is important. It is also important to establish individual analysis methods of organic substances. It is expected that the analytical methods will be established and new treating methods will be put to practical use in the near future.

• Steel and Composite Structures
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• v.8 no.5
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• pp.361-388
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• 2008

The Eurocode 4 presents some negative aspects in the design of composite slabs by the m-k Method or the Partial Connection Method. On one hand, the component chemical adherence is not accounted for in the connection between the profiled steel sheet and the concrete. On the other hand, the application of these methods requires some fitting parameters that must be determined by full scale tests. In this paper, the Eurocode 4 methods are compared with a method developed at the Federal Polytechnic School of Lausanne, based on pullout tests, which can be a valid alternative. Hence, in order to calculate the necessary parameters for the three methods, several tests have been performed such as the full scale test described in Eurocode 4 and pull-out tests. This last type of tests is of small dimensions and implicates lower costs. Finally, a full-scale test of a steel-concrete composite slab with a generic loading is presented, with the goal of verifying the analytical formulation.

• Food Science of Animal Resources
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• v.35 no.4
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• pp.466-472
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• 2015

A rapid and simple analytical method, using liquid chromatography tandem mass spectrometry (LC-MS/MS), was developed to detect myo-inositol (MI) in infant formulas. For protein removal: acid hydrolysis and lipid removal through organic solvent extraction. The operating conditions for instrumental analysis were determined based on previously reported analogous methods that used LC-MS/MS. Quantitative analysis was used for the detection limit test, infant formula recovery test, and standard reference material (SRM) 1849a to verify the validity of our LC-MS/MS analytical method, which was developed to quantify MI. For validation, the results of our method were compared with the results of quantitative analyses of certified values. The test results showed that the limit of detection was 0.05 mg/L, the limit of quantitation was 0.17 mg/L, and the method detection limit was 17 mg/kg. The recovery test exhibited a recovery between 98.07-98.43% and a relative standard deviation between 1.93-2.74%. Therefore, the result values were good. Additionally, SRM 1849a was measured to have an MI content of 401.84 mg/kg and recovery of 98.25%, which is comparable to the median certified value of 409 mg/kg. From the aforementioned results, we judged that the instrumental analysis conditions and preparation method used in this study were valid. The rapid analytical method developed herein could be implemented in many laboratories that seek to save time and labor.

• Steel and Composite Structures
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• v.16 no.1
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• pp.21-44
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• 2014

The aim of this study is to determine the dynamic characteristics of long reinforced concrete highway bridges with post-tension tendons using analytical and experimental methods. It is known that the deck length and height of bridges are affected the dynamic characteristics considerably. For this purpose, Berta Bridge constructed in deep valley, in Artvin, Turkey, is selected as an application. The Bridge has two piers with height of 109.245 m and 85.193 m, and the total length of deck is 340.0 m. Analytical and experimental studies are carried out on Berta Bridge which was built in accordance with the balanced cantilever method. Finite Element Method (FEM) and Operational Modal Analysis (OMA) which considers ambient vibration data were used in analytical and experimental studies, respectively. Finite element model of the bridge is created by using SAP2000 program to obtain analytical dynamic characteristics such as the natural frequencies and mode shapes. The ambient vibration tests are performed using Operational Modal Analysis under wind and human loads. Enhanced Frequency Domain Decomposition (EFDD) and Stochastic Subspace Identification (SSI) methods are used to obtain experimental dynamic characteristics like natural frequencies, mode shapes and damping ratios. At the end of the study, analytical and experimental dynamic characteristic are compared with each other and the finite element model of the bridge was updated considering the material properties and boundary conditions. It is emphasized that Operational Modal Analysis method based on the ambient vibrations can be used safely to determine the dynamic characteristics, to update the finite element models, and to monitor the structural health of long reinforced concrete highway bridges constructed with the balanced cantilever method.

• Analytical Science and Technology
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• v.15 no.4
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• pp.346-359
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• 2002

The brominated flame retardants (BFRs) are one of the unregulated pollutants in Korea, which is recently highlighted the new pollutants of environmental contamination. In this study, the previous research papers related the BFRs were surveyed, and the analytical methods of BFRs were established. The results are followed; The 40 kinds of PBDEs standards were used to establish the analytical methods to perform the experiments of recoveries and detection limits in water and soil. The detection limits of PBDEs using GC/MS represented 5.0~10.0 pg/L for water and 0.5~2.0 ng/g for soil samples. The average recoveries of water samples were 89~98% with ethylacetate, n-hexane and dichloromethane, and 89~103% in combined solvent with n-hexane and acetone. In soxhlet extraction, the higher recoveries obtained the acetone:n-hexane(1:1) comparing with acetone:dichloromethane(1:1).

• Journal of the Korean School Mathematics Society
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• v.21 no.4
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• pp.401-418
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• 2018

The current geometric and vector textbooks focus on the mechanical activities of finding focus, corner, etc. through elliptic equations. In this paper, we propose a process in which analogy and analytical methods are used in reversible activities of focusing from a given elliptic graph without a coordinate plane. The exploratory tool was used as Geogebra. At first, students tried to find the focus of the ellipse by randomly constructing the major a is and the minor a is in the given ellipse. However, we have experienced a method of constructing the circle of symmetry and analyzed this principle and deduced it to the ellipse. As a result, we could construct the center, long a is and short a is of the ellipse. Then, using the analytical method, the focus formula was recognized as the Pythagorean theorem, and the ellipse's focus was constructed by using the original drawing. Therefore, it is confirmed that analogy and analytical method can positively affect the elliptical focus.

• Analytical Science and Technology
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• v.19 no.2
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• pp.172-180
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• 2006

This study was performed to establish new methods for hazardous substances and to develop an analytical method in specified wastes for preventing the environmental pollution caused by hazardous wastes. Therefore, the trends of international management, regulatory criteria, and items of hazardous wastes in various countries were investigated. Based on this study, target priority of new hazardous substances in specified wastes was established. An analytical method was developed using the waste standard reference materials of sludge, oil, bottom ash, etc., which contain the new hazardous substances (Ba, Be, Cr(VI), F, Ni, Sb, Se, and V). A total of 37 waste samples from the representative facilities, which are emitting new hazardous substances, were analyzed.

• Analytical Science and Technology
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• v.21 no.4
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• pp.296-303
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• 2008

This study was performed to establish an analytical method of PAHs in oil contaminated soil of these methods by evaluating the PAHs test methods from US EPA and ISO etc. The application to domestic contaminated soil leads to a conclusion that alumina column is a more effective clean-up procedure for oil contaminated soil rather than the others. It is proposed with the new analytical method of 12 PAHs except for more volatile compounds (naphthalene, acenaphthylene, acenaphthene, fluorene). The recovery of PAHs in this method ranged 67~107%. The oil contaminated soil samples were analyzed using GC/MSD. The concentration of PAHs ranged $78.68{\sim}275.57{\mu}g/kg$. The predominated compounds were fluoranthene, pyrene and chrysene attributing about 70% of total concentration. The level of Benzo[a]pyrene ranged $1.76{\sim}24.65{\mu}g/kg$.

• Journal of Environmental Science International
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• v.4 no.1
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• pp.91-103
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• 1995

The reaction rate, equilibrium, and flow injection analysis methods were fundamentally evaluated for the determination of aqueous ammonia. The selected indophenol blue method was based on the formation of indophenol blue in which ammonium ion reacted with hypochlorite and phenol in alkaline solution. In the optimized reaction condition, the reaction followed 1st order reaction kinetics and the final product was stable. The absorbance measurements before and after the equilibrium were utilized for the reaction rate and equilibrium methods. The reaction rate methods, based on the relative analytical signals for the possibility of eliminating interferents, were shown to have good linear calibration curves but the detection limit and the calibration sensitivity were poorer than those in the equilibrium method. The detection limits were 32-49 pub and 24 pub for the reaction rate and equilibrium methods, respectively In the flow injection analysis, the absorbance was measured before the equilibrium reached and thus resulted in 30% reduction of calibration sensitivity. However, the detection limit was 11 ppb, indicating that the peak-to-peak noise for the blank was remarkably improved. Compared to the manual methods, the optimized experimental condition in a closed reaction system reduced the blank absorbance and the inclusion of ammonia from the atmosphere was prevented. In addition, highly reproducible mixing of sample and reagents and analytical data extracted from continuous recording showed excellent reproducibility.

• Journal of the Korean Society for Industrial and Applied Mathematics
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• v.26 no.4
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• pp.185-223
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• 2022

The classical equation of Jonathan Homer Lane and Robert Emden, a nonlinear second-order ordinary differential equation, models the isothermal spherical clouded gases under the influence of the mutual attractive interaction between the gases' molecules. In this paper, the Adomian decomposition method (ADM) is presented to obtain highly accurate and reliable analytical solutions of a class of generalised Lane-Emden equations with strong nonlinearities. The nonlinear term f(y(x)) of the proposed problem is given by the integer powers of a continuous real-valued function h(y(x)), that is, f(y(x)) = h^m(y(x)), for integer m ≥ 0, real x > 0. In the end, numerical comparisons are presented between the analytical results obtained using the ADM and numerical solutions using the eighth-order nested second derivative two-step Runge-Kutta method (NSDTSRKM) to illustrate the reliability, accuracy, effectiveness and convenience of the proposed methods. The special cases h(y) = sin y(x), cos y(x); h(y) = sinh y(x), cosh y(x) are considered explicitly using both methods. Interestingly, in each of these methods, a unified result is presented for an integer power of any continuous real-valued function - compared with the case by case computations for the nonlinear functions f(y). The results presented in this paper are a generalisation of several published results. Several examples are given to illustrate the proposed methods. Tables of expansion coefficients of the series solutions of some special Lane-Emden type equations are presented. Comparisons of the two results indicate that both methods are reliably and accurately efficient in solving a class of singular strongly nonlinear ordinary differential equations.