• Korean Journal of Pharmacognosy
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• v.41 no.1
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• pp.67-72
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• 2010

In the recent version of the Korea Pharmacopoeia(KP) and the Korean Herbal Pharmacopoeia(KHP), there are 563 items(181 in KP, 381 in KHP) of herbal medicines including finished drugs. Also, approximately 507 items including herbal extracts and herbal medicinal products was published in the 3th edition of Korea Pharmaceutical Codex (KPC). These items help the persons working in the pharmaceutical manufacturing field to register the drug and in research fields to develop the new drug considering as a standard specifications. This study was carried out to establish standard analytical methods for 'Compound Hawthorn Berry 60% Ethanol Extract, Ginkgo Biloba Leaf Extract and Garlic Oil Capsules' in the 3th edition of Korea Pharmaceutical Codex. Ginkgo flavonoid and terpene lactone were employed as reference compounds for analytical method. Analytical methods established in this study could be applied to a reasonable and unified quality control of G. biloba leaf extract and hawthorn berry extract.

• Analytical Science and Technology
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• v.15 no.3
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• pp.300-316
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• 2002

The extraction methods of PBBs from environmental samples by soxhlet extraction for solid phase and liquid-liquid extraction for liquid phase were compared. After extraction, silicagel and florisil as column clean up methods were used for the comparison of cleanup efficiency with different solvent system. Also, the analytical instruments were used GC/MSD. The 22 kinds of PBBs standards were used to establish the analytical methods to perform the experiments of recoveries and detection limits in water and soil. The detection limits of PBBs represented 5~10 ng/L for water and 0.5~3.5 ng/g for soil samples, respectively. The recoveries of water samples represented 96~107% in n-hexane, dichloromethane and toluene for water, and 60~80% in combined solvent with n-hexane and acetone. The recoveries of soil sample were surveyed 67~97% in soxhlet extraction and 64~76% in ultrasonic extraction with selected solvents.

• Analytical Science and Technology
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• v.20 no.2
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• pp.91-108
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• 2007

This study was investigated both the Korean official soil test method and the international various methods for PCBs in soil sample. The analytical guideline of PCBs in contaminated soil were proposed based on the official soil test methods by discussing the extraction, column cleanup, instrumental conditions, quantification methods of peak matching and individual isomers. The total 28 soil samples were selected by consideration of PCBs-contamination, land use etc., and then analyzed using gas chromatography/electron capture detection (GC/ECD) and gas chromatography/mass spectrometry(GC/MS). In this study, the PCBs were not detected as peak matching method using GC/ECD, but PCBs detected $0.002{\sim}0.487{\mu}g/kg$ using GC/MS in background concentrations.

• Journal of the Korean Chemical Society
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• v.38 no.11
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• pp.800-807
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• 1994

A method to determine the iron and steels employing a Direct Reading Atomic Emission Spectrometer was investigated. Matrix effect was removed by two correction methods which utilize linear and curvilinear functions. Although two methods gave different sets of matrix correction coefficients, the analytical results by the two methods gave the same results. The analytical results obtained by the present work were well agreed with those obtained by inductively coupled plasma spectrometry.

• Journal of Astronomy and Space Sciences
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• v.15 no.2
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• pp.485-497
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• 1998

To estimate the availability of the MCE for KOMPSAT I, mathematical models of H/W and S/W availability, the availability estimating methods for parallel and redundant system were presented. Furthermore, to improve and estimate the MCE system availability, we analyzed the computational procedure of redundant methods, and we also included effective switch choosing methods in this paper. The analytical results of the MCE system availability were estimated as follows: - 0.995216 not considering system redundancy, - 0.9955165 considering system redundancy, and -0.9963991 for the time of system real time operation.

• Proceedings of the Korea Air Pollution Research Association Conference
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• 2010.04a
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• pp.41-44
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• 2010

Hazardous air pollutants such as benzo[a]pyrene (BaP), benzene, formaldehyde have been concerned about the adverse health effect of long-term exposure. Contour map is useful for finding high-concentration region, emission source, and distributions of HAPs in the ambient air. To make a contour map, we have developed simple analytical method for selected HAPs; polycyclic aromatic hydrocarbons such as BaP, benzene and its derivatives such as toluene and xylene, and aldehydes and ketones. We have applied these methods to investigate air pollution by HAPs in some cities in Japan. The results show that these methods reveal actual emission sources if the PRTR emission report was not submitted.

• Selected Papers of The Society of Naval Architects of Korea
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• v.2 no.1
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• pp.1-17
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• 1994

For a planar curve-sided panel with constant or linear density distributions of source or doublet in the singularity methods, Cantaloube and Rehbach show that the surface integral can be transformed into contour integral by using Stokes'formulas. As an extension of their formulations, this paper deals with a planar polygonal panel for which we derive the closed-forms of the potentials and the velocities induced by the singularity distributions. Test calculations show that the analytical evaluation of the closed-forms is superior to numerical integration (suggested by Cantaloube and Rehbach) of the contour integral. The compact and explicit expressions may produce accurate values of matrix elements of simultaneous linear equations in the singularity methods with much reduced computer time.

• Proceedings of the Korean Environmental Sciences Society Conference
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• 2003.11a
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• pp.135-138
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• 2003

Based on solid phase extraction, gas chromatography and mass spectrometry procedure for determining phenol and its derivatives in natural water was presented. In solid phase extraction, three types of techniques using solid phase adsorption material were treated with acid and salt, and converted second portion of acetyl derivatives. Under the these condition, extraction efficiency and detection ability dependent on extraction methods were discussed. Obtained results using optimized solid phase extraction techniques showed more convenience, simplifier and lower cost than the conventional analytical methods with holding wide dynamic range and lower detection limits.

• Journal of the Korean Society of Manufacturing Technology Engineers
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• v.26 no.2
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• pp.199-204
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• 2017

In this study, analytical methods for designing a torque arm pin and elastomeric bushings of a conventional-type three-point-suspension gearbox of a wind turbine are investigated. The design loads for the torque arm were derived by considering the effects of the transmitted torque and self-weight of the gearbox. Based on the design loads, design methods for the torque arm pin and elastomeric bushings were introduced in the terms of material and size selection. Finally, a small-scale conventional-type gearbox was designed by applying the derived design methods. This study is an elementary and analytical study for the design of the torque arm pin and elastomeric bushings. It is necessary to verify and supplement the results further through extensive experimentation.

• Food Science and Biotechnology
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• v.18 no.6
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• pp.1515-1518
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• 2009

The objective of this study was to compare 3 extraction methods including, solid phase extraction (SPE), acetonitrile extraction, and methanol extraction, for their usefulness as extraction methods to determine capsaicinoids. The determination of capsaicinoids in the extracts was carried out on a reverse-phased high performance liquid chromatography (HPLC) using a fluorescence detector. Three extraction methods, i.e., SPE, acetonitrile extraction, and methanol extraction were compared for the quantification of capsaicinoids using raw peppers and pepper powder. The highest analytical values were observed using methanol extraction and the lowest values using SPE. Also, the analytical method validation parameters such as accuracy, precision, limit of detection, limit of quantitation, and specificity were calculated to ensure the method's validity. This method provides a fast and accurate approach for the determination of capsaicinoids in peppers.