• Title/Summary/Keyword: amorphous powder

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Fabrication and Magnetic Properties of A New Fe-based Amorphous Compound Powder Cores

  • Xiangyue, Wang;Feng, Guo;Caowei, Lu;Zhichao, Lu;Deren, Li;Shaoxiong, Zhou
    • Journal of Magnetics
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    • v.16 no.3
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    • pp.318-321
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    • 2011
  • A new Fe-based amorphous compound powder was prepared from Fe-Si-B amorphous powder by crushing amorphous ribbons as the first magnetic component and Fe-Cr-Mo metallic glassy powder by water atomization as the second magnetic component. Subsequently by adding organic and inorganic binders to the compound powder and cold pressing, the new Fe-based amorphous compound powder cores were fabricated. This new Fe-based amorphous compound powder cores combine the superior DC-Bias properties and the excellent core loss. The core loss of 500 kW/$m^3$ at $B_m$ = 0.1T and f = 100 kHz was obtained When the mass ratio of FeSiB/FeCrMo equals 3:2, and meanwhile the DC-bias properties of the new Fe-based amorphous compound powder cores just decreased by 10% compared with that of the FeSiB powder cores. In addition, with the increasing of the content of the FeCrMo metallic glassy powder, the core loss tends to decrease.

Soft-magnetic Characteristics of Co-based Amorphous Powder Produced by Spinning Water Atomization Process (SWAP)

  • Otsuka, I.;Wada, K.;Watanabe, A.;Kadomura, T.;Yagi, M.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.784-785
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    • 2006
  • Co-based amorphous powder was produced by a new atomization process "Spinning Water Atomization Process (SWAP)", having rapid super-cooling rate. The composition of the alloys was ($(Co_{0.95}Fe_{0.05})_{1-x}Cr_x$)$_{75}Si_{15}B_{10}$ (x=0, 0.025, 0.05, 0.075). The powders became the amorphous state even if particle size was up to about $500{\mu}m$. The coercive force of powders was about 0.35 - 0.7 Oe. Furthermore, Co-based amorphous powder cores with glass binders were made by cold-pressing and sintering methods. The initial permeability of the core in the frequency range up to 100 kHz was about 110, and the core loss at 100 kHz for Bm = 0.1 T was $350kW/m^3$.

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Deformation Behavior of $CU_{54}Ni_6Zr_{22}Ti_{18}$ Bulk Amorphous Alloy during Multi-Pass Warm Rolling (동계 벌크 아몰퍼스의 다단 온간 압연시 변형 거동)

  • Park E. S.;Kim H. J.;Bae J. C.;Huh M. Y.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2005.10a
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    • pp.139-142
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    • 2005
  • Cu-Ni-Zr-Ti bulk amorphous thin strips were produced by multi-pass warm rolling of the amorphous powder at temperatures in the supercooled liquid region. Process variables for rolling of the bulk amorphous strips were properly controlled to prevent onset of crystallization and failure during rolling up to three passes. During rolling of the amorphous powder, both the deformation and densification took place and the newly developed surface on the deformed amorphous particles enhances the consolidation leading to an increase in the strength. The strain state during rolling was analyzed by FEM.

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Development of EM Wave Absorber for Hi-pass System Using Amorphous Metal Powder

  • Kim, Dong-Il;Yoo, Gun-Suk;Choi, Dong-Soo
    • Journal of Navigation and Port Research
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    • v.35 no.9
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    • pp.717-720
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    • 2011
  • In this paper, we designed and fabricated the Electromagnetic(EM) wave absorber for an Electronic Toll Collection(ETC or Hi-pass) system by using Amorphous metal powder and CPE. The material properties and the absorption properties of the samples containing 50 wt.%, 60 wt.%, 70 wt.%, and 80 wt.% of Amorphous. Moreover, the EM wave absorption abilities were simulated for the different thicknesses of the EM absorbers by adopting the measured permittivity and permeability, and then the EM wave absorber was fabricated based on the simulated design values. As a result, the EM wave absorber with the composition of Amorphous metal powder : CPE = 50 : 50 wt.% with the thickness of 2.6 mm has excellent absorption ability more than 40 dB at 5.8 GHz.

Production of Fe Amorphous Powders by Gas-Atomization Process and Subsequent Spark Plasma Sintering of Fe amorphous-ductile Cu Composite Powder Produced by Ball-milling Process (II) - II. SPS Behaviors of Composite Powders and their Characteristics - (가스분무법에 의한 Fe계 비정질 분말의 제조와 볼밀링공정에 의한 연질 Cu분말과의 복합화 및 SPS 거동 (II) - II. 복합분말의 SPS와 특성 -)

  • Kim, Jin-Chun;Kim, Ji-Soon;Kim, H.J.;Kim, Jeong-Gon
    • Journal of Powder Materials
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    • v.16 no.5
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    • pp.326-335
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    • 2009
  • Fe based (Fe$_{68.2}$C$_{5.9}$Si$_{3.5}$B$_{6.7}$P$_{9.6}$Cr$_{2.1}$Mo$_{2.0}$Al$_{2.0}$) amorphous powder, which is a composition of iron blast cast slag, were produced by a gas atomization process, and sequently mixed with ductile Cu powder by a mechanical ball milling process. The Fe-based amorphous powders and the Fe-Cu composite powders were compacted by a spark plasma sintering (SPS) process. Densification of the Fe amorphous-Cu composited powders by spark plasma sintering of was occurred through a plastic deformation of the each amorphous powder and Cu phase. The SPS samples milled by AGO-2 under 500 rpm had the best homogeneity of Cu phase and showed the smallest Cu pool size. Micro-Vickers hardness of the as-SPSed specimens was changed with the milling processes.

Synthesis of Cu-coated Ni-based Bulk Metallic Glass Powders by Gas Atomization and Spray Drying Process

  • Kim, Byoung-Kee;Kim, Yong-Jin;Kim, Jin-Chun
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.936-936
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    • 2006
  • Bulk amorphous materials have been intensively studied to apply for various advanced industry fields due to their high mechanical, chemical and electrical properties. These materials have been produced by several techniques such as mechanical alloying, melt spinning and gas atomization, etc. Among them, the atomization is the most potential technique for commercialization due to high cooling rate during solidification of the melt and mass productivity. However, the amorphous powders still have some limitations because of their low ductility and toughness. Therefore, intensive efforts have to be carried out to increase the ductility and toughness. In this study, the Ni-based amorphous powder was produced by the gas atomization process. And in order to increase the ductile toughness, ductile Cu phase was coated on the Ni amorphous powder by spray drying process. The characteristics of the as-synthesis powders have been examined and briefly mentioned. The master alloy with $Ni_{57}Zr_{20}Ti_{16}Si_2Sn_3$ was prepared by vacuum induction melting furnace with graphite crucible and mold. The atomization was conducted at $1450^{\circ}C$ under the vacuum of $10^{-2}$ torr. The gas pressure during atomization was varied from 35 to 50 bars. After making the Ni amorphous powders, the spray drying was processed to produce the Cu -coated Ni amorphous composite powder. The amorphous powder and Cu nitrate solution were mixed together with a small amount of binder and then it was sprayed at temperature of $130^{\circ}C$ and rotating speed of 15,000 R.P.M.

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Synthesis and Properties of Amorphous Matrix Composites using Cu-based/Ni-based Amorphous Powders (Cu계 및 Ni계 비정질 합금 분말을 이용한 비정질기지 복합재의 제조 및 특성)

  • Kim Taek-Soo;Lee Jin-Kyu;Kim Hwi-Jun;Bae Jung-Chan
    • Journal of Powder Materials
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    • v.12 no.6 s.53
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    • pp.406-412
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    • 2005
  • This work is to present a new synthesis of metallic glass (MG)/metallic glass (MG) composites using gas atomization and spark plasma sintering (SPS) processes. The MG powders of $Cu_{54}Ni_6Zr_{22}Ti_{18}$ (CuA) and $Ni_{59}Zr_{15}Ti_{13}Nb_7Si_3Sn_2Al_1$(NiA) as atomized consist of fully amorphous phases and present a different thermal behavior; $T_g$ (glass transition temperature) and $T_x$ (crystallization temperature) are 716K and 765K for the Cu base powder, but 836K and 890K for the Ni base ones, respectively. SPS process was used to consolidate the mixture of each amorphous powder, being $CuA/10\%NiA\;and\;NiA/10\%CuA$ in weight. The resultant phases were Cu crystalline dispersed NiA matrix composites as well as NiA phase dispersed CuA matrix composites, depending on the SPS temperatures. Effect of the second phases embedded in the MG matrix was discussed on the micro-structure and mechanical properties.

Fabrication and consolidation of amorphous Cu55Ti45 powders by mechanical alloying (기계적 합금화에 의한 비정질 Cu55Ti45 분말의 제조 및 성형)

  • 김도용
    • Journal of Powder Materials
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    • v.7 no.2
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    • pp.85-92
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    • 2000
  • The Cu55Ti45 system was effectively mechanically-alloyed using a pulverizer. Noncrystallinities of the powders were characterized by TEM, X-ray and DSC. The amorphous powders were consolidated without losing their noncrystallinities. The consolidating conditions keeping a non-crystalline were obtained by building a TTT diagram of the amorphous powders. The microhardness of the crystallite and bulk amorphous alloys are also compared.

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Amorphous Diamond for Generating Cold Cathode Fluorescence Light

  • Sung, James-C.;Kan, Ming-Chi;Hu, Shao-Chung
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.913-914
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    • 2006
  • Amorphous diamond has a very low work function (1 eV) at modest temperature ($150^{\circ}C$). It has been coat coated on electron emitting electrodes. Such electrodes are used for cold cathode fluorescence lamps (CCFL) that illuminate liquid crystal displays (LCD) for rnote books and television sets. Amorphous diamond can dramatically reduce the turn-on voltage to lit CCFL so the lamp life can be greatly extended. Moreover, the electrical current can be increased to enhance the brightness of the light.

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