• Journal of Magnetics
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• v.10 no.4
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• pp.142-144
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• 2005

The Magnetization behaviour has been measured for amorphous $Fe_{80-x}Mn_xZr_{10}$ (x = 4,6,8,10) alloys. The Curie temperature decreased from 236 K to 195 K with increasing Mn concentration (x = 4 to x = 10). The magnetization measurements were conducted at temperatures above the Curie temperature in the paramagnetic region. In all samples, the magnetic properties showed superparamagnetic behavior above $T_c$ where the mean magnetic moment of the superparamagnetic spin clusters decreased with increasing temperature. A large magnetic entropy change, ${\Delta}S_M$, which is calculated from H vs M curves associated with the ferromagnetic-paramagnetic transitions in amorphous, has been observed. With Mn concentration increasing, ${\Delta}S_M$ decreases 1.04, 0.95, 0.87 J/kg K at 222, 210, 195 K (the Curie temperature), respectively.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 1997.11a
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• pp.136-139
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• 1997

In this paper, we inveatigate frequency dependance of inductance effects of FeCoB amorphous magnetic films. First, amorphous magnetic film having near zero magnetostriction is the basic composition of (Fe$_{1-x}$ / $Co_{x}$)$_{79}$Si$_2$B$_{19}$ with x=0.94, 0.95 and in order to decrease magnetio . anisotropy, the film was annealed in 28$0^{\circ}C$/30min, 40$0^{\circ}C$/30min, 40$0^{\circ}C$/1hr with near crystallization temperature under non-magnetic field. As result of investigation, in case of x=7.95 than x=0.94, we could have obtained high values, which inductance ratios in the low frequency was 488%. And Quality factor Q was under 0.7 in all sample, in case of annealed in 28$0^{\circ}C$/30min, we could have obtained highest value, which x=0.9fl is about 0.62 in 400[kHz], and in case of x=0.95 was about 0.35 in 1[MHz].z].].

• Journal of the Korean Magnetics Society
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• v.5 no.5
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• pp.487-490
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• 1995

With the object of developing a new magnetic core materials for high frequency use, the crystallization behaviors and the soft magnetic properties of amorphous $F_{86-x}Al_{4}B_{10}Zr_{x}\;(5{\leq}x{\leq}10\;at%)$ alloys subjected to annealing treatment at wide temperature range were investigated. For optimally annealed $Fe_{86-x}Al_{4}B_{10}Zr_{x}$ alloys in amorphous state, rather good soft magnetic properties of ${\mu}_{e}=17000~25000,\;H_{c}=20~30$ mOe and $B_{10}{\geq}0.6$ T are obtained. However, as the alloys crystallize, the soft magnetic properties are largely dergely deteriorated, which is attributed principally to the narrow temperature gap between $T_{x1}$ and $T_{x2}$, which allows the nearly co-precipitation of bcc phase and Fe-B compounds in incipient crystallization stage.

• Journal of the Korean Magnetics Society
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• v.19 no.1
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• pp.17-21
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• 2009

In this study, we have investigated that the excitation current and operation frequency dependences of the output properties of the orthogonal fluxgate sensor which was fabricated with a Co base amorphous wire and a pick-up coil. The output signal increased linearly with increase of the excitation current below 0.3 A, and decreased with increase of the excitation current over 0.6 A. It was also found that the output increased sensitively with increase of operation frequency below 1.3MHz. The output was 3.8 V at the frequency of 1.3MHz while 1.32 V at 1MHz.

• Journal of Powder Materials
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• v.28 no.3
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• pp.233-238
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• 2021

Iron-based amorphous powder attracts increasing attention because of its excellent soft magnetic properties and low iron loss at high frequencies. The development of an insulating layer on the surface of the amorphous soft magnetic powder is important for minimizing the eddy current loss and enhancing the energy efficiency of high-frequency devices by further increasing the electrical resistivity of the cores. In this study, a hybrid insulating coating layer is investigated to compensate for the limitations of monolithic organic or inorganic coating layers. Fe₂O₃ nanoparticles are added to the flexible silicon-based epoxy layer to prevent magnetic dilution; in addition TiO₂ nanoparticles are added to enhance the mechanical durability of the coating layer. In the hybrid coating layer with optimal composition, the decrease in magnetic permeability and saturation magnetization is suppressed.

• Journal of the Korean Magnetics Society
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• v.11 no.3
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• pp.85-96
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• 2001

Experimental magnetization-temperature curves for melt-spun ribbons of amorphous alloys (Dy$\_$0.33/Fe$\_$0.67/)$\_$1-x/B$\_$x/(x=0 ,0.05, 0.1, and 0.15) and (Sm$\_$0.33/Fe$\_$0.67/)$\_$1-x/B$\_$x/(x=0, 0.01, 0.02, and 0.03) (in atomic fraction) are fitted with theoretical equations based on the mean field theory in order to calculate exchange couplings between constituent elements as a function of the B content. In the case of the DyFe$_2$-B system, the sign of the exchange coupling between Dy and Fe is negative, indicating that the magnetization direction of Dy is antiparallel to that of Fe. The sign of the other two couplings are positive indicating a parallel alignment. The exchange coupling between Fe ions are greatest, while that between Dy ions is negligible. In the case of the SmFe$_2$B alloys, the sign of all the couplings are positive, indicating ferromagnetic coupling between the spins. The exchange couplings between Fe ions, and Fe and Sm are comparable to each other, but they are much greater than that between Sm ions. The high exchange coupling between Fe and Sm, which is considered to occur indirectly, is rather unexpected, but it is considered to be unique characteristics of amorphous Sm-Fe alloys. In both alloy systems, the exchange coupling between Fe ions increases with increasing B content. and this may be explained by the increase of the Fe-Fe separation with increasing B content. The exchange coupling between Fe and RE also increases with increasing B content. As the B content increases, the magnetization decreases over the whole temperature range, and the Curie temperature also decreases.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 1988.10a
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• pp.5-7
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• 1988

Effect of isothermal aging on the crystallization of $Fe_{78}B_{13}Si_{9}$ metallic glass has been investigated by electrical resistivity, X-ray measurements, bending test, thermal analysis and transmission electron microscopy. Amorphous $Fe_{78}B_{13}Si_{9}$ alloy was annealed isothermally for 5 to 1200 mon. between 300 C and 540 C. It has been found that close relation between relative resistivity and X-ray diffraction pattern showed. The crystalline peak of $\alpha$-(Fe, Si) and Fe$_2$B are detected by X-ray experiment. The crystalline phases observed by TEM show $\alpha$-(Fe, Si) and Fe$_3$B with dendritic and cylindrical morphology, respectively. It has been also found that the embrittleness of aged samples rapidly increased with the crystallization and was shown before the crystallization.th the crystallization and was shown before the crystallization.

• Journal of the Korean Magnetics Society
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• v.7 no.4
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• pp.173-179
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• 1997

Change in phases, microstructures, and magnetic properties by the variation of quench rate and heat treatment were investigated for melt-spun $Fe_{77}Pr_{15}C_8$ ribbons. The amorphization of as-spun ribbons increased as the quench rate increased. As a result, the ribbon quenched at 40 m/s was almost entirely amorphous. Similarly to cast alloys, the primary phase in crystalline ribbons quenched at 10 m/s was $\alpha$-Fe followed by the secondary $Fe_{17}Pr_2C_x$. Crystalline phases were still dominant in the ribbon spun at 20 m/s, but in this case crystallization of $Fe_{17}Pr_2C_x$ was remarkable with a little suppression of $\alpha$-Fe. At 30 m/s an amorphous phase obviously dominated in the as-spun ribbons with small fraction of crystals. Therefore, substantial amount of hard magnetic $Fe_{14}Pr_2C$ was not obtained from the as-spun state but, as in cast alloys, produced only by a solid-state transformation. Within a few minutes fine grains of $Fe_{14}Pr_2C$ were easily obtained at relatively low temperature when the degree of amorphization of as-spun ribbons was higher. The grain size of $Fe_{14}Pr_2C$ was well less than 1${\mu}{\textrm}{m}$. The ribbons quenched at 20 or 30 m/s yielded higher coercivities after heat treatment.

• Journal of the Korean Magnetics Society
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• v.7 no.5
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• pp.250-257
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• 1997

The microstructure and magnetic properties of Fe-Nb-B-N thin film alloys, which produced by rf magnetron sputtering method in $Ar+N_2$ mixed gas atmosphere, were investigated. The $Fe_{70}Nb_{14}B_{11}N_5$ films, annealed at 59$0^{\circ}C$, exhibit soft magnetic properties: $4{\pi}M_s=16.5kG$ , $H_c=0.13Oe$ and ${\mu}_{eff}$ (1~10 MHz)=5, 000. The frequency stability of the Fe-Nb-B-N films has also been found to be good up to 10 MHz. The Fe-Nb-B-N thin film alloys annealed at 59$0^{\circ}C$ consist of three phase; fine crystalline $\alpha$-Fe phase with grain size of about 5~10 nm, Nb-B rich amorphous phase and Nb-nitride precipitates with the size of less than 3 nm. Annealed Fe-Nb-B films have two phases; $\alpha$-Fe grains with the size of about 10 nm and Nb-B rich amorphous phase. The addition of N decreased $\alpha$-Fe grain size due to the precipitation of NbN. The good magnetic properties of the Fe-Nb-B-N film alloys are due to fine $\alpha$-Fe grains resulting from the precipitation of NbN.

• Journal of the Korean Magnetics Society
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• v.6 no.1
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• pp.36-39
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• 1996

We have constructed a disp1acerrent sensor for measuring dynamic magnetostriction of an arrvrphous ribbon under alternating magnetic field using fiber optic Fabry-Perot interferorreter. The signal of the sensor was depen¬dent on the index matching oil and the optical isolator. The resolution of the sensor was $30{\AA}$ and the measured peak to peak magnetostriction of the amorphous ribbon $Fe_{81}B_{13.5}Si_{3.5}C_{2}$ was $28{\times}10^{-6}$.