• Title/Summary/Keyword: advanced Measurement technique

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Interfacial and Surface Energies Evaluation of Modified Jute and Hemp Fibers/Polypropylene (PP)-Maleic Anhydride Polypropylene Copolymers (PP-MAPP) Composites using Micromechanical Technique and Contact Angle Measurement (미세역학시험법과 접촉각 측정을 통한 변형된 Jute와 Hemp섬유 강화 Polypropylene (PP)-Maleic Anhydride Polypropylene Copolymers (PP-MAPP) 복합재료의 계면 및 표면에너지 평가)

  • Park, Joung-Man;Son, Tran Quang;Jung, Jin-Gyu;Kim, Sung-Ju;Hwang, Byung-Sun
    • Journal of Adhesion and Interface
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    • v.7 no.2
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    • pp.1-11
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    • 2006
  • Interfacial evaluation of the untreated and treated Jute and Hemp fibers reinforced different matrix polypropylene-maleic anhydride polypropylene copolymer (PP-MAPP) composites were investigated by micromechanical technique and dynamic contact angle measurement. For the statistical tensile strength of Jute and Hemp fibers, bimodal Weibull distribution was fitted better than the unimodal distribution. The acid-base parameter on the interfacial shear strength (IFSS) of the natural fiber composites was characterized by calculating the work adhesion, $W_a$. The effect of alkaline, silane coupling agent on natural fibers were obtained with changing MAPP content in PP-MAPP matrices. Alkaline treated fibers made the surface energy to be higher due to removing the weak boundary layers and thus increasing surface area, whereas surface energy of silane treated Jute and Hemp fibers decreased due to blocked high energy sites. MAPP in the PP-MAPP matrix caused the surface energy to increase due to introduced acid-base sites. Microfailure modes of two natural fiber composites were observed clearly differently due to different tensile strength of natural fibers.

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Measurement of Adsorption Characteristic Using a Quartz Crystal Resonator (수정진동자를 이용한 흡착특성의 측정)

  • Kim, Byoung Chul;Sung, Ick Gi;Yamamoto, Takuji;Kim, Young Han
    • Korean Chemical Engineering Research
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    • v.47 no.3
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    • pp.368-372
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    • 2009
  • A technique to measure the adsorption characteristic of surface area and pore size distribution is proposed and its performance is examined. While the existing equipment utilizes liquid nitrogen, the proposed uses carbon dioxide at the room temperature leading to the small measuring device with easy operation and short measurement time. The performance of the device has been examined with micro-particle carbon cryogel and bamboo activated carbon. The results from the proposed device compared with those of the adsorption apparatus indicate that the measurement of meso-porous material is comparable but micro-porous material gives some error.

Direct Strength Evaluation of the CVD SiC Coating of TRISO Coated Fuel Particle with Micro Hemi Spherical Shell Configuration (마이크로 반구 쉘 형상의 화학증착 탄화규소 TRISO 코팅층의 파괴강도 직접평가)

  • Lee, Hyeon-Keun;Kim, Do-Kyung
    • Journal of the Korean Ceramic Society
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    • v.44 no.7
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    • pp.368-374
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    • 2007
  • CVD-SiC coating has been introduced as a protective layer in TRISO nuclear fuel particle of high temperature gas cooled reactor (HTGR) due to its excellent mechanical stability at high temperature. In order to prevent the failure of the TRISO particles, it is important to evaluate the fracture strength of the SiC coating layer. It is needed to develop a new simple characterization technique to evaluate the mechanical properties of the coating layer as a pre-irradiation step. In present work, direct strength measurement method with the specimen of hem i-spherical shell configuration was suggested. The indentation experiment on a hemisphere shell with a plate indenter was conducted. The fracture strength of the coating layer is related with the critical load for radial cracking of the shell. The finite element analysis was used to drive the semi-empirical equation for the strength measurement. The SiC hemispherical shells were successfully recovered from the section-grinding of TRISO coated particle and successive heat treatment in air. The strength of CVD-SiC coating layer was evaluated from the experimentally measured critical load during the indentation on SiC hemisphere shell. Weibull diagram of fracture strength was also constructed. This study suggested a new strength equation and experimental method to measure the fracture strength of CVD-SiC coating of TRISO coated fuel particles.

Comparison of Acoustic Attenuation Measurement Technique of Polyethylene Matrix Composite Materials (폴리에틸렌기재 복합재료의 음향감쇠 측정방법 비교)

  • Kim Kyongsub;Jung Hyun K.;Lee Zin-Hyoung;Hong Soon H.
    • Proceedings of the Acoustical Society of Korea Conference
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    • autumn
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    • pp.265-268
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    • 1999
  • 감쇠가 큰 고분자 복합재료에서 초음파 다중반사파를 이용한 Pulse Echo법, 공진주파수에서 내부마찰계수 측정법과 Rheometer를 이용한 동적탄성계수 측정법을 사용하여 음향감쇠계수를 측정하고 각각의 측정자료를 비교하는 연구를 수행하였다. Pulse Echo법을 이용하여 0.5, 1.0, 2.25MHz에서 음향감쇠계수를 측정하였고, 이때 폴리에틸렌기지 복합재료의 음향감쇠계수는 강화재의 부피분율에 따라 3-15dB/cm 정도로 큰 값을 나타내었다. 폴리에틸렌기지 복합재료를 600kHz 근처에서 공진주파수를 가지도록 시편을 만든 후에 내부마찰계수를 측정한 결과로 계산된 음향감쇠계수는 Pulse Echo 실험에서 구한 값과 잘 일치하는 결과를 얻을 수 있었다. Rheometer를 이용한 동적탄성계수 측정법은 0.1-100Hz의 주파수에서 측정한 자료를 TTSP 이론을 이용하여 1MHz의 결과와 비교하였는데, 단일 고분자 재료에서는 다른 측정방법과 음향감쇠계수가 일치하였지만 복합재료에서는 음향감쇠계수값이 일치하지 않는 결과를 나타내었다.

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Experimental Study on the Forming Limit Curve of Aluminum Alloy Sheets using Digital Image Correlation (디지털 이미지 상관관계를 이용한 알루미늄 합금 판재의 성형한계도 평가)

  • Kim, Yongbae;Park, Jungsoo;Song, Junghan
    • Journal of Institute of Convergence Technology
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    • v.5 no.1
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    • pp.7-12
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    • 2015
  • Sheet metal formability can be defined as the ability of metal to deform without necking or fracture into desired shape. Every sheet metal can be deformed without failure only up to a certain limit, which is normally known as forming limit curve(FLC). In this paper, the dome stretching tests and tensile tests have been performed to obtain forming limit curve of aluminum alloy. During the experiment, failure strain is measured using digital image correlation(DIC) method. DIC method is a whole-field measurement technique that acquires surface displacements and strains from images information which characterized a random speckle as intensity grey levels. Recently years, this DIC method is being developed and used increasingly in various research. DIC results demonstrated the usefulness and ability to determine a strain.

Real-time Fluorescence Lifetime Imaging Microscopy Implementation by Analog Mean-Delay Method through Parallel Data Processing

  • Kim, Jayul;Ryu, Jiheun;Gweon, Daegab
    • Applied Microscopy
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    • v.46 no.1
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    • pp.6-13
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    • 2016
  • Fluorescence lifetime imaging microscopy (FLIM) has been considered an effective technique to investigate chemical properties of the specimens, especially of biological samples. Despite of this advantageous trait, researchers in this field have had difficulties applying FLIM to their systems because acquiring an image using FLIM consumes too much time. Although analog mean-delay (AMD) method was introduced to enhance the imaging speed of commonly used FLIM based on time-correlated single photon counting (TCSPC), a real-time image reconstruction using AMD method has not been implemented due to its data processing obstacles. In this paper, we introduce a real-time image restoration of AMD-FLIM through fast parallel data processing by using Threading Building Blocks (TBB; Intel) and octa-core processor (i7-5960x; Intel). Frame rate of 3.8 frames per second was achieved in $1,024{\times}1,024$ resolution with over 4 million lifetime determinations per second and measurement error within 10%. This image acquisition speed is 184 times faster than that of single-channel TCSPC and 9.2 times faster than that of 8-channel TCSPC (state-of-art photon counting rate of 80 million counts per second) with the same lifetime accuracy of 10% and the same pixel resolution.

Effect of Delayed Oxygen Evolution in Anodic Polarization on the Passive Film Characteristic and Localized Corrosion Resistance of Titanium Alloys (타이타늄 합금에서 산소발생전위 지연이 부동태 피막 특성과 국부부식 저항성에 미치는 영향)

  • Oh, Yu Soo;Seo, Dong-Il;Lee, Jae-Bong
    • Corrosion Science and Technology
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    • v.19 no.3
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    • pp.156-162
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    • 2020
  • The objective of this study was to investigate delayed oxygen evolution and localized corrosion resistance of titanium alloys by performing potentiodynamic polarization, potentiostatic polarization, and Mott-Schottky measurements. Delayed oxygen evolution was compared among titanium alloys, 316 stainless steel, and platinum. Difference in delayed oxygen evolution between titanium alloys and other metals was attributed to specific surface characteristic of each metal. Delayed oxygen evolution of titanium alloys resulted from the predominant process of ionic conduction over electronic conduction. The effect of oxygen evolution on localized corrosion of titanium alloys was investigated using electrochemical critical localized corrosion temperature (E-CLCT) technique. Mott-Schottky measurement was performed to clarify the difference in film properties between titanium alloys and stainless steels. Titanium alloys were found to have much lower donor density than stainless steels by 1/28. These results indicate that delayed oxygen evolution has little influence on the concreteness of passive film and the resistance to localized corrosion of titanium alloys.

Circumferential steady-state creep test and analysis of Zircaloy-4 fuel cladding

  • Choi, Gyeong-Ha;Shin, Chang-Hwan;Kim, Jae Yong;Kim, Byoung Jae
    • Nuclear Engineering and Technology
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    • v.53 no.7
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    • pp.2312-2322
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    • 2021
  • In recent studies, the creep rate of Zircaloy-4, one of the basic property parameters of the nuclear fuel code, has been commonly used with the axial creep model proposed by Rosinger et al. However, in order to calculate the circumferential deformation of the fuel cladding, there is a limitation that a difference occurs depending on the anisotropic coefficients used in deriving the circumferential creep equation by using the axial creep equation. Therefore, in this study, the existing axial creep law and the derived circumferential creep results were analyzed through a circumferential creep test by the internal pressurization method in the isothermal conditions. The circumferential creep deformation was measured through the optical image analysis method, and the results of the experiment were investigated through constructed IDECA (In-situ DEformation Calculation Algorithm based on creep) code. First, preliminary tests were performed in the isotropic β-phase. Subsequently in the anisotropic α-phase, the correlations obtained from a series of circumferential creep tests were compared with the axial creep equation, and optimized anisotropic coefficients were proposed based on the performed circumferential creep results. Finally, the IDECA prediction results using optimized anisotropic coefficients based on creep tests were validated through tube burst tests in transient conditions.

A Study for the Border line Extraction technique of City Spatial Building by LiDAR Data (LiDAR 데이터와 항공사진의 통합을 위한 사각 빌딩의 경계점 설정)

  • Yeon, Sang-Ho;Lee, Young-Wook
    • Proceedings of the Korea Contents Association Conference
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    • 2007.11a
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    • pp.27-29
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    • 2007
  • The visual implementation of 3-dimensional national environment is focused by the requirement and importance in the fields such as, national development plan, telecommunication facility deployment plan, railway construction, construction engineering, spatial city development, safety and disaster prevention engineering. The currently used DEM system using contour lines, which embodies national geographic information based on the 2-D digital maps and facility information has limitation in implementation in reproducing the 3-D spatial city. Moreover, this method often neglects the altitude of the rail way infrastructure which has narrow width and long length. There it is needed to apply laser measurement technique in the spatial target object to obtain accuracy. Currently, the LiDAR data which combines the laser measurement skill and GPS has been introduced to obtain high resolution accuracy in the altitude measurement. In this paper, we first investigate the LiDAR based researches in advanced foreign countries, then we propose data a generation scheme and an algorithm for the optimal manage and synthesis of railway facility system in our 3-D spatial terrain information. For this object, LiDAR based height data transformed to DEM, and the realtime unification of the vector via digital image mapping and raster via exactness evaluation is transformed to make it possible to trace the model of generated 3-dimensional railway model with long distance for 3D tract model generation.

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Experimental Study on Corrosion Detection of Aluminum Alloy Using Lamb Wave Mixing Technique (램파 혼합 기법을 이용한 알루미늄 합금의 부식 결함 검출에 대한 실험 연구)

  • Choi, Heeung;Lee, Jaesun;Cho, Younho
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.40 no.11
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    • pp.919-925
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    • 2016
  • In this study, the Lamb wave mixing technique, which is basised on advanced research on the nonlinear bulk wave mixing technique, is applied for corrosion detection. To demonstrate the validity of the Lamb wave mixing technique, an experiment was performed with normal and corroded specimens. Comparison group in an experimentation are selected to mode and frequency with dominant in-plane displacement and out-of-plane displacement of Lamb waves. The results showed that the Lamb wave mixing technique can monitor corrosion defects, and it has a trend similar to that of the conventional Lamb wave technique. It was confirmed that the dominant displacement and mode matching the theory were generated. Flaw detectability is determined depending on displacement ratio instead of using the measurement method and mode selection.