• Restorative Dentistry and Endodontics
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• v.40 no.3
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• pp.202-208
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• 2015

Objectives: This study determined the effect of the air-stream application time and the bonding technique on the dentin bond strength of adhesives with different solvents. Furthermore, the content and volatilization rate of the solvents contained in the adhesives were also evaluated. Materials and Methods:Three adhesive systems with different solvents (Stae, SDI, acetone; XP Bond, Dentsply De Trey, butanol; Ambar, FGM, ethanol) were evaluated. The concentrations and evaporation rates of each adhesive were measured using an analytical balance. After acid-etching and rinsing, medium occlusal dentin surfaces of human molars were kept moist (conventional) or were treated with 10% sodium hypochlorite for deproteinization. After applying adhesives over the dentin, slight air-stream was applied for 10, 30 or 60 sec. Composite cylinders were built up and submitted to shear testing. The data were submitted to ANOVA and Tukey's test (${\alpha}=0.05$). Results: Stae showed the highest solvent content and Ambar the lowest. Acetone presented the highest evaporation rate, followed by butanol. Shear bond strengths were significantly affected only by the factors of 'adhesive' and 'bonding technique' (p < 0.05), while the factor 'duration of air-stream' was not significant. Deproteinization of dentin increased the bond strength (p < 0.05). Stae showed the lowest bond strength values (p < 0.05), while no significant difference was observed between XP Bond and Ambar. Conclusions: Despite the differences in content and evaporation rate of the solvents, the duration of air-stream application did not affect the bond strength to dentin irrespective of the bonding technique.

• Restorative Dentistry and Endodontics
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• v.42 no.2
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• pp.95-104
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• 2017

Objectives: This study evaluated the influence of a multi-mode universal adhesive (MUA) containing silane (Single Bond Universal, 3M EPSE) on the bonding of resin cement to lithium disilicate. Materials and Methods: Thirty IPS e.max CAD specimens (Ivoclar Vivadent) were fabricated. The surfaces were treated as follows: Group A, adhesive that did not contain silane (ANS, Porcelain Bonding Resin, Bisco); Group B, silane (S) and ANS; Group C, hydrofluoric acid (HF), S, and ANS; Group D, MUA; Group E, HF and MUA. Dual-cure resin cement (NX3, Kerr) was applied and composite resin cylinders of 0.8 mm in diameter were placed on it before light polymerization. Bonded specimens were stored in water for 24 hours or underwent a 10,000 thermocycling process prior to microshear bond strength testing. The data were analyzed using multivariate analysis of variance (p < 0.05). Results: Bond strength varied significantly among the groups (p < 0.05), except for Groups A and D. Group C showed the highest initial bond strength ($27.1{\pm}6.9MPa$), followed by Group E, Group B, Group D, and Group A. Thermocycling significantly reduced bond strength in Groups B, C, and E (p < 0.05). Bond strength in Group C was the highest regardless of the storage conditions (p < 0.05). Conclusions: Surface treatment of lithium disilicate using HF and silane increased the bond strength of resin cement. However, after thermocycling, the silane in MUA did not help achieve durable bond strength between lithium disilicate and resin cement, even when HF was applied.

• Restorative Dentistry and Endodontics
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• v.40 no.1
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• pp.30-36
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• 2015

Objectives: This study was performed to determine whether the combined use of one-bottle self-etch adhesives and composite resins from same manufacturers have better bond strengths than combinations of adhesive and resins from different manufacturers. Materials and Methods: 25 experimental micro-shear bond test groups were made from combinations of five dentin adhesives and five composite resins with extracted human molars stored in saline for 24 hr. Testing was performed using the wire-loop method and a universal testing machine. Bond strength data was statistically analyzed using two way analysis of variance (ANOVA) and Tukey's post hoc test. Results: Two way ANOVA revealed significant differences for the factors of dentin adhesives and composite resins, and significant interaction effect (p < 0.001). All combinations with Xeno V (Dentsply De Trey) and Clearfil $S^3$ Bond (Kuraray Dental) adhesives showed no significant differences in micro-shear bond strength, but other adhesives showed significant differences depending on the composite resin (p < 0.05). Contrary to the other adhesives, Xeno V and BondForce (Tokuyama Dental) had higher bond strengths with the same manufacturer's composite resin than other manufacturer's composite resin. Conclusions: Not all combinations of adhesive and composite resin by same manufacturers failed to show significantly higher bond strengths than mixed manufacturer combinations.

• Restorative Dentistry and Endodontics
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• v.24 no.4
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• pp.546-553
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• 1999

In Older to evaluate the effectiveness of 'One-bottle dentin adhesive system', the shear bond strengths of two fourth generation dentin adhesive systems and two One-bottle systems to the occlusal dentin of the freshly extracted third molars were measured by the regulation of the ISO TR 11405. The fourth generation dentin adhesive systems used in this study were Scotchbond Multi-Purpose Plus and All-Bond 2, and the One-bottle systems were Single Bond and One-Step. The effects of the thickness of hybrid layer and adhesive layer, the diameter of resin tag and the ratio between the diameter of resin tag and that of dentinal tubule were analyzed as the contributing factors of the shear bond strength of dentin bonding systems from the Scanning Electron Microscopic images. The results were as follows: 1. The shear bond strengths of Scotchbond Multi-Purpose, All-Bond 2, and Single Bond were 16.98${\pm}$3.40 MPa, 15.10${\pm}$2.77 MPa and 15.05${\pm}$3.18 MPa, respectively. There were no statistical differences(p>0.05). 2. But, the shear bond strength of One-Step were significantly lower than those of the other groups (11.81${\pm}$1.95 MPa, p<0.05). 3. The thicknesses of hybrid layer and adhesive layer of One-Step were significantly thinner than those of the other groups(p<0.05). The differences of the diameter of resin tag(p=0.0685) and the ratio between the diameter of resin tag and that of dentinal tubule(p=0.2401) were not significant among all the material groups. 4. The thickness of hybrid layer and adhesive layer might be considered as contributing factors of the she at bond strengths of dentin bonding systems, but the diameter of resin tag and the ratio between the diameter of resin tag and that of dentinal tubule might not.

• Steel and Composite Structures
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• v.20 no.6
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• pp.1275-1303
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• 2016

Steel plates and carbon-fiber-reinforced polymer (CFRP) laminates or plates bonded to concrete substrates have been widely used for concrete strengthening. However, this technique cause plate debonding, which makes the strengthening system inefficient. The main objective of this study is to enhance the bond strength of externally bonded steel plates and CFRP laminates to the concrete surface by proposing new embedded adhesive and steel connectors. The effects of these new embedded connectors were investigated through the tests on 36 prism specimens. Parameters such as interfacial shear stress, fracture energy and the maximum strains in plates were also determined in this study and compared with the maximum value of debonding stresses using a relevant failure criterion by means of pullout test. The study indicates that the interfacial bond strength between the externally bonded plates and concrete can be increased remarkably by using these connectors. The investigation verifies that steel connectors increase the shear bond strength by 48% compared to 38% for the adhesive connectors. Thus, steel connectors are more effective than adhesive connectors in increasing shear bond strength. Results also show that the use of double connectors significantly increases interfacial shear stress and decrease debonding failure. Finally, a new proposed formula is modified to predict the maximum bond strength of steel plates and CFRP laminates adhesively glued to concrete in the presence of the embedded connectors.

• The Journal of Korean Academy of Prosthodontics
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• v.39 no.4
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• pp.351-365
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• 2001

For accurate impression taking, accurate impression material, solid individual tray, and bond strength between impression materials and resin tray are important factors. The purpose of this study was to evaluate tensile bond strength of rubber impression materials to various tray resin materials. This study tested the time dependent tensile bond strength between commercial brands or poly ether, polysulfide, additional silicone impression materials and commercial brands of self curing tray resin. light activited tray resin when applying adhesive Resin specimens were made with 20mm in diameter, 2mm in thickness. 1 made total 360 specimens, 10 per each group and the tensile bond strength was measured by using the Instron($M100EC^{(R)}$, Mecmesin Co., England). The results were as follows ; Comparisons of various impression materials. 1. In case of Impregum $F^{(R)}$, the bond strength of tray resin was decreased in order of SR $Ivolen^{(R)}$, Ostron $100^{(R)}$ Instant tray $mix^{(R)}$, $Lightplast^{(R)}$. All groups excluding Ostron $100^{(R)}$, Instant tray $mix^{(R)}$ are significant difference (p<0.05). Drying time after applying adhesive, the tensile bond strength of tray resin was insignificantly decreased in order of 10 min drying time group. 1 min drying time group. 5 min drying time group. 2. In case of Permlastic $regular^{(R)}$ the bond strength of tray resin was insignificantly decreased in order of Ostron $100^{(R)}$. SR $Ivolen^{(R)}$, Instant tray $mix^{(R)}$ $Lightplast^{(R)}$. About drying time after applying adhesive, the tensile bond strength of tray resin was significantly decreased in order of 5 min drying time group, 10 min drying time group, 1 min drying time group(p<0.05). 3. In case of Exaflex $regular^{(R)}$. the bond strength of tray resin was decreased in order of $Lightplast^{(R)}$, SR $Ivolen^{(R)}$, Instant tray $mix^{(R)}$, Ostron $100^{(R)}$. $Lightplast^{(R)}$ was significant difference(p<0.05). About drying time after applying adhesive, the tensile bond strength of tray resin was decreased in order of 5 min drying time group, 10 min drying time group, 1 min drying time group(p<0.05). Especially 5 min ding time group was significant difference(p<0.05). According to the results of this study, we can see the greatest tensile bond strength when using Impregrm $F^{(R)}$ and Permlastic $regular^{(R)}$ with self curing tray resin, when using Exaflex $regular^{(R)}$ with light activated tray resin In my opinion, adhesive should be dried more than 5 min before impression taking to achieve the greatest tensile bond strength.

• The Journal of Korean Academy of Prosthodontics
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• v.44 no.4
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• pp.383-393
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• 2006

Statement of problem : Limited research on flowable resin has been undertaken on its application directly on dentin associated with the adhesive systems. Purpose : This study was to evaluate the shear bond strengh and fracture aspect of flowable resin on human dentin with various types of dentin bonding adhesives with thermo cycling effect. Materials and methods: Filtek-Flow(3M ESPE, USA) was used as flowable resin and Eighty human molars were randomly divided into 4 groups : three dentin bonding adhesives (Scotchbond-Multipurpose : 3-step contentional system, One-Step : One-bottle system. Prompt L-Pop : All-in-one, self-etching primer) and 32% etching treatment without bonding adhesive as a control group. For evaluating their durability of bonding, each group was subdivided : storaging in the water at 37$^{\circ}C$(24 hours) and thermocycling (0$^{\circ}C$-55$^{\circ}C$, 30 seconds intervals, 1000 cycle). Shear bond strength tests were performed and resin-dentin interface and fracture mode were observed. Results were analysed by one-way ANOVA and Scheffe's multiple range test. Results and Conclusion : 1. At 0 cycle, the mean shear bond strength of One-Step exhibited the highest value of all groups(p<0.05), and there were no significant differences between Prompt L-Pop and Scotchbond-Multipurpose, Scotchbond-Multipurpose and control(p>0.05). After 1000 thermocycling, One-Step exhibited higher value than other groups(p<0.05), and there were no significant differences among other groups (p>0.05). 2. The shear bond strength of each group was significantly decreased after thermocycling except Scotchbond-Multipurpose (p>0.05). 3. The most common failure mode was adhesive type and mixed type, next in order.

• Proceedings of the KWS Conference
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• 2006.10a
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• pp.45-47
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• 2006

Lightweight design, safety, vibration, energy absorption capability can no longer achieve without adhesive bond joint. Base on those concepts and cost reduction, adhesive bond FEM model development has been done. The FEM analysis and experiments were conducted in this study. Crash condition is 143 Kg Hammer weight and unit meter Height. and then These test results were used to develop resonable FEM model. To estimate which FEM model is resonable, compare hybrid joint specimen experiment results with FEM analysis results. Conclusively this study achieves optimization bonding model related crash and adhesive bond jointed hat profile crash characters.

• Proceedings of the Korea Concrete Institute Conference
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• 2003.11a
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• pp.219-222
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• 2003

Substantial experimental and theoretical work exists on the bond characteristics of FRP-concrete adhesive joints. Experimental studies show that the bond strength cannot always increase with an increase in the bond length, and that the ultimate strength is strongly influenced by the concrete strength. To solve this feature, analytic solutions based on fracture mechanics are widely used, and the local shear stress-slip curve with a softening branch is known as more rational model. The analytic solution, however, cannot describe various shapes of model curve. In this study, numerical method using interface element is introduced to express various shapes of model curve. Characteristics of adhesive joint is investigated for the shapes of the model curve and their parameters. And the numerical solutions are compared with the test results of CFRP sheet adhesive joints.

• Journal of Adhesion and Interface
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• v.21 no.1
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• pp.6-13
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• 2020

The objective of the current study is to characterize the long-term stability and efficacy of a structural adhesive assembly under static load. An apparatus was designed to be used in the Instron tensile test machine that would allow for real time modeling of the failure characteristics of an assembly utilizing a moisture- cure adhesive which was bonded to concrete. A regression model was developed that followed a linear - natural log function which was used to predict the expected life of the assembly. Evaluations at different curing times confirmed the structure was more robust with longer cure durations prior to loading. Finally, the results show that under the conditions the assembly was tested, there was only a small amount of inelastic creep and the regression models demonstrated the potential for a stable structure lasting several decades.