• 한국분말재료학회지
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• 제12권5호
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• pp.332-335
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• 2005

Porous and porous surfaced Ti-6Al-4V implant compacts were fabricated by electro-discharge-sintering (EDS) of atomized spherical Ti-6Al-4V powders with a diameter of $100-150\;{\mu}m$, The solid core formed in the center of the compact after discharge was composed of acicular ${\alpha}+{\beta}$ Widmanstatten grains, The hardness value at the solid core was much higher than that at the particle interface or particles in the porous layer, which can be attributed to both heat treatment and work hardening effects induced from EDS, The compressive yield strength was in a range of 19 to 436 MPa which significantly depends on both input energy and capacitance, Selected porous-surfaced Ti-6Al-4V implant compacts with a solid core have much higher compressive strengths compared to the human teeth and sintered Ti dental implants.

• 한국주조공학회지
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• 제13권2호
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• pp.187-193
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• 1993

In this study, it was examined the relationship between the microstructure, fatigue properties, mechanical properties and retained austenite volume of Mo-Ni ADI corresponding to various austempering temperatures. When the austempering temperature is increased to $370^{\circ}C$, acicular bainite structure was found to be transformed to feathery bainite structure. But at the austempering temperature of $420^{\circ}C$, the dissolved bainite lath was showned. Up to the austempering temperature of $370^{\circ}C$, the volume of retained austenite was increased. However at the austempering temperature of $420^{\circ}C$ a large amount of retained austenite was decreased. In this study, the retained austenite volume was determined by XRD(X-ray diffraction). It was observed that the optimum fatigue properties can be obtained at the condition of austempering temperature $370^{\circ}C$. Under the such conditions, fatigue limit determined as the value of 290 MPa, tensile strength 877MPa elongation 6%, hardness 285(BHN), impact values(CVN) 9.2J and retained austenite volume 30.3%, respectively.

• Journal of Welding and Joining
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• 제27권6호
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• pp.25-30
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• 2009

SBD (Strain-based design) of pipe lines have gained world-wide attention in recent years. The present research aims to evaluate the fracture characteristics of API (America Petroleum Institute) SBD X100 girth weldment that typically applied for cold climate and deep water offshore, with the focus on the influence of heat input changing with 6kJ/cm and 10kJ/cm from GMAW (Gas Metal Arc Welding). At a low heat input at 6kJ/cm, the weld metal had Multi-phase matrix (Acicular ferrite + Banite + Martensite) that could fill up both fracture toughness and strength as reported previously. Also, the weld metal exhibited 859MPa YS (Yield strength), 108J impact toughness at $-40^{\circ}C$ and 0.52mm CTOD (Crack Tip Open Displacement) at $-10^{\circ}C$. These results can be satisfied with the requirement of API SBD X100 girth weldment and Alaska pipe line project.

• 한국산업융합학회 논문집
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• 제24권5호
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• pp.525-530
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• 2021

The purpose of this study was to investigate the effect of spherodizing heat treatment holding time on the microstructure and mechanical properties of the accelerated cooling-treated API X70 steel, which is mainly used as a structural material for line pipe steel for natural gas pipes. The accelerated cooling-treated API X70 steel was spherodizing treated at 700℃ for 12~48 h. The microstructure was observed using an OM and a FEG-SEM, and mechanical properties were obtained by tensile test. The microstructure of the API X70 steel was banded in the hot rolling direction, and the polygonal ferrite(PF) adjacent to pearlite(P) has mainly a fine size, and coarse PF and fine acicular ferrite were formed in the middle of P and P. As the spherodizing treatment time increased, the number of carbide particles decreased and its distribution interval increased, and the ferrite grain size was coarsened. The tensile strength decreased and the ductility increased with spherodizing treatment time, and the yield point elongation was disappeared in a stress-strain curve after the spherodizing treatment.

• Corrosion Science and Technology
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• 제20권1호
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• pp.37-43
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• 2021

Additively manufactured (AM) Ti-6Al-4V alloys exhibit a dominant acicular martensite phase (α'), which is characterized by an unstable energy state and highly localized corrosion susceptibility. Electrochemical critical localized corrosion temperature (E-CLCT, ISO 22910: 2020) and electrochemical critical localized corrosion potential (E-CLCP, ISO AWI 4631: 2021) were measured to analyze the localized corrosion resistance of the AM Ti-6Al-4V alloy. Although E-CLCP was measured under mild corrosive conditions such as human body, the validity of evaluating localized corrosion resistance of AM titanium alloys was demonstrated by comparison with E-CLCT. However, the mechanisms of resistance to localized corrosion on the as-received and heat-treated AM Ti-6Al-4V alloys under E-CLCT and E-CLCP differ at various temperatures because of differences in properties under localized corrosion and repassivation. The E-CLCT is mainly measured for initiation of localized corrosion on the AM titanium alloys based on temperature, whereas the E-CLCP yields repassivation potential of re-generated passive films of AM titanium alloys after breaking down.

• Nano
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• 제13권11호
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• pp.1850136.1-1850136.12
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• 2018

Three-dimensional (3D) mixed phases NiSe nanoparticles growing on the nickel foam were synthesized via a simple one-step hydrothermal method. A series of experiments were carried out to control the morphology by adjusting the amount of selenium in the synthetic reaction. Meanwhile, the as-prepared novel column-acicular structure NiSe exist three advantages including ideal electrical conductivity, high specific capacity and high cycling stability. It delivered a high capacitance of $10.8F\;cm^{-2}$ at a current density- of $5mA\;cm^{-2}$. An electrochemical capacitor device operating at 1.6 V was then constructed using NiSe/NF and activated carbon (AC) as positive and negative electrodes. Moreover, the device showed high energy density of $31W\;h\;kg^{-1}$ at a power density of $0.81kW\;kg^{-1}$, as well as good cycling stability (77% retention after 1500 cycles).

• Metals and materials international
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• 제24권6호
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• pp.1221-1231
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• 2018

The effect of strain aging on tensile behavior and properties of API X60, X70, and X80 pipeline steels was investigated in this study. The API X60, X70, and X80 pipeline steels were fabricated by varying alloying elements and thermomechanical processing conditions. Although all the steels exhibited complex microstructure consisting of polygonal ferrite (PF), acicular ferrite, granular bainite (GB), bainitic ferrite (BF), and secondary phases, they had different fractions of microstructures depending on the alloying elements and thermomechanical processing conditions. The tensile test results revealed that yielding behavior steadily changed from continuous-type to discontinuous-type as aging temperature increases after 1% pre-strain. After pre-strain and thermal aging treatment in all the steels, the yield and tensile strengths, and yield ratio were increased, while the uniform elongation and work hardening exponent were decreased. In the case of the X80 steel, particularly, the decrease in uniform elongation was relatively small due to many mobile dislocations in PF, and the increase in yield ratio was the lowest because a large amount of harder microstructures such as GB, BF, and coarse secondary phases effectively enhanced work hardening.

• 대한금속재료학회지
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• 제49권10호
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• pp.766-773
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• 2011

In this study, three kinds of linepipe steels were processed by changing the amount of Mo and Nb to investigate the effects on microstructures, tensile and Charpy impact properties. All the specimens consisted of acicular ferrite, granular bainite and secondary phases such as martensite and austenite constituents (MA). The increase in Mo raised the volume fractions of the granular bainite and MA, and raised the number of fine precipitates, which increased the yield and tensile strengths and decreased the upper self energy and energy transition temperatures. In the steel having less Mo and more Nb, the volume fractions of the granular bainite and MA decreased, and a finer microstructure was observed. This microstructure suppressed the formation of separation during Charpy impact testing and led to a higher upper shelf energy and lower energy transition temperature, while the yield and tensile strengths were lower than those of the steels with more Mo and less Nb.

• 대한금속재료학회지
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• 제47권3호
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• pp.195-201
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• 2009

This paper is concerned with effects of Mn and heat-input on the mechanical properties of EGW welds. Four different kinds of welding consumables were fabricated by varying Mn contents such as 1.3, 1.5, 1.7, 2.0%Mn and each consumable was welded for EGW on four heat-input conditions between 190 and 340 KJ/Cm. Mn contents were decreased as heat-input increases and alloy elements (C, Si, Ti, B, Al) to deoxidize easily also revealed similar tendency to Mn. Their microstructure, Charpy impact property and strength were investigated, and it is found that Charpy impact property and strength exhibit a strong dependence on change of microstructure by Mn contents and heat-input. The increase of Mn contents or the decrease of heat-input made the microstructure fine and increase volume fraction of acicular ferrite, thereby leading to the great improvement of Charpy impact property and strength. In case of single EGW, optimum Mn contents are over 1.7% for the toughness and strength.

• Archives of Metallurgy and Materials
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• 제67권4호
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• pp.1487-1490
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• 2022

In this study, the effect of the coiling temperature on the tensile properties of API X70 linepipe steel plates is investigated in terms of the microstructure and related anisotropy. Two coiling temperatures are selected to control the microstructure and tensile properties. The API X70 linepipe steels consist mostly of ferritic microstructures such as polygonal ferrite, acicular ferrite, granular bainite, and pearlite irrespective of the coiling temperature. In order to evaluate the anisotropy in the tensile properties, tensile tests in various directions, in this case 0° (rolling direction), 30°, 45° (diagonal direction), 60°, and 90° (transverse direction) are conducted. As the higher coiling temperature, the larger amount of pearlite is formed, resulting in higher strength and better deformability. The steel has higher ductility and lower strength in the rolling direction than in the transverse direction due to the development of γ-fiber, particularly the {111}<112> texture.