• Title/Summary/Keyword: ablative materials

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Evaluation of Structural Performance for Filament Wound Composite Ablative Tubes (필라멘트와인딩된 복합재 내열튜브의 구조 성능 평가)

  • 윤성호;황태경;윤남균;문순일
    • Composites Research
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    • v.15 no.1
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    • pp.53-60
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    • 2002
  • Composite ablative tubes required capabilities of ablative and structural characteristics were fabricated through filament winding technique and several experiments were conducted to evaluate the structural performance of composite ablative tubes. For this purpose, manufacturing procedures were briefly described and then resin digestion method was applied to measure the fiber volume fraction and the void content of composite ablative tubes. The configuration of tensile specimen fur composite ablative tubes with not losing the continuity of reinforced fibers was suggested by evaluating mechanical properties of several types of the specimen with different widths. Also, suitable processing variables for composite ablative tubes were determined by evaluating mechanical properties of several types of the specimen with different processing variables. In addition, acoustic emission signals were obtained during the proof test and could be applicable to study the crack initiation and the damage mode of composite ablative tubes. Finally, the structural reliability of composite ablative tubes could be verified to satisfy design requirements through the proof and burst tests.

Prediction of Local Tumor Progression after Radiofrequency Ablation (RFA) of Hepatocellular Carcinoma by Assessment of Ablative Margin Using Pre-RFA MRI and Post-RFA CT Registration

  • Yoon, Jeong Hee;Lee, Jeong Min;Klotz, Ernst;Woo, Hyunsik;Yu, Mi Hye;Joo, Ijin;Lee, Eun Sun;Han, Joon Koo
    • Korean Journal of Radiology
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    • v.19 no.6
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    • pp.1053-1065
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    • 2018
  • Objective: To evaluate the clinical impact of using registration software for ablative margin assessment on pre-radiofrequency ablation (RFA) magnetic resonance imaging (MRI) and post-RFA computed tomography (CT) compared with the conventional side-by-side MR-CT visual comparison. Materials and Methods: In this Institutional Review Board-approved prospective study, 68 patients with 88 hepatocellulcar carcinomas (HCCs) who had undergone pre-RFA MRI were enrolled. Informed consent was obtained from all patients. Pre-RFA MRI and post-RFA CT images were analyzed to evaluate the presence of a sufficient safety margin (${\geq}3mm$) in two separate sessions using either side-by-side visual comparison or non-rigid registration software. Patients with an insufficient ablative margin on either one or both methods underwent additional treatment depending on the technical feasibility and patient's condition. Then, ablative margins were re-assessed using both methods. Local tumor progression (LTP) rates were compared between the sufficient and insufficient margin groups in each method. Results: The two methods showed 14.8% (13/88) discordance in estimating sufficient ablative margins. On registration software-assisted inspection, patients with insufficient ablative margins showed a significantly higher 5-year LTP rate than those with sufficient ablative margins (66.7% vs. 27.0%, p = 0.004). However, classification by visual inspection alone did not reveal a significant difference in 5-year LTP between the two groups (28.6% vs. 30.5%, p = 0.79). Conclusion: Registration software provided better ablative margin assessment than did visual inspection in patients with HCCs who had undergone pre-RFA MRI and post-RFA CT for prediction of LTP after RFA and may provide more precise risk stratification of those who are treated with RFA.

Ablative Characteristics of Carbon/Carbon Composites by Liquid Rocket

  • Joo, Hyeok-Jong;Min, Kyung-Dae;Lee, Nam-Joo
    • Carbon letters
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    • v.2 no.3_4
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    • pp.192-201
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    • 2001
  • The Carbon/Carbon composite was prepared from 3D carbon fiber preform and coal tar pitch as matrix precursor. In order to evaluate of ablative characteristics of the composite, liquid rocket system was employed Kerosene and liquid oxygen was used as propellants, operating at a nominal chamber pressure of 330 psi and a nominal mixture ratio (O/F) of 2.0. The results of an experimental evaluation were that high density composite exhibited high, while low density composites showed low erosion resistance. The erosion rate against heat flux was highly depended on the density of the materials. The morphology of eroded fiber showed differently according to collision angle with heat flux on the composite. The granular matrix which derived from carbonization pressure of 900 bar was more resistance to heat flux than well-developed flow type matrix.

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A Study on Surface Properties of Ablative Materials from 0.4MW Arc-Heated Wind Tunnel Test (0.4MW 아크 가열 풍동 시험을 통한 삭마 재료의 표면 특성 연구)

  • Kim, Nam Jo;Oh, Philyong;Shin, Eui Sup
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.43 no.12
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    • pp.1048-1053
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    • 2015
  • Ablative materials in a thermal protection system for atmospheric re-entry suffers from the most severe heat fluxes and temperatures, which induces surface recession in the thickness direction. In this paper, a 0.4MW arc-heated wind tunnel is operated to test for ablative materials, and a non-contact three-dimensional surface measuring system is used to evaluate the different surface characteristics of them. In particular, by postprocessing the three-dimensional image data, the surface roughness and recession of ablative materials can be calculated before and after the wind tunnel test. Moreover, the surface properties are analyzed quantitatively by comparing volume and mass losses of the test specimens.

Quantitative Assessment of Variation in Poroelastic Properties of Composite Materials Using Micromechanical RVE Models

  • Han, Su Yeon;Kim, Sung Jun;Shin, Eui Sup
    • International Journal of Aeronautical and Space Sciences
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    • v.17 no.2
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    • pp.175-183
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    • 2016
  • A poroelastic composite material, containing different material phases and filled with fluids, serves as a model to formulate the overall ablative behaviors of such materials. This article deals with the assessment of variation in nondeterministic poroelastic properties of two-phase composite materials using micromechanical representative volume element (RVE) models. Considering the configuration and arrangement of pores in a matrix phase, various RVEs are modeled and analyzed according to their porosity. In order to quantitatively investigate the effects of microstructure, changes in effective elastic moduli and poroelastic parameters are measured via finite element (FE) analysis. The poroelastic parameters are calculated from the effective elastic moduli and the pore-pressure-induced strains. The reliability of the numerical results is verified through image-based FE models with the actual shape of pores in carbon-phenolic ablative materials. Additionally, the variation of strain energy density is measured, which can possibly be used to evaluate microstress concentrations.

Ablative Outcomes of Various Energy Modes for No-Touch and Peripheral Tumor-Puncturing Radiofrequency Ablation: An Ex Vivo Simulation Study

  • Dong Ik Cha;Min Woo Lee;Kyoung Doo Song;Seong Eun Ko;Hyunchul Rhim
    • Korean Journal of Radiology
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    • v.23 no.2
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    • pp.189-201
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    • 2022
  • Objective: To compare the outcomes of radiofrequency ablation (RFA) using dual switching monopolar (DSM), switching bipolar (SB), and combined DSM + SB modes at two different interelectrode distances (25 and 20 mm) in an ex vivo study, which simulated ablation of a 2.5-cm virtual hepatic tumor. Materials and Methods: A total of 132 ablation zones were created (22 ablation zones for each protocol) using three separable clustered electrodes. The performances of the DSM, SB, and combined DSM + SB ablation modes were compared by evaluating the following parameters of the RFA zones at two interelectrode distances: shape (circularity), size (diameter and volume), peritumoral ablative margins, and percentages of the white zone at the midpoint of the two electrodes (ablative margin at midpoint, AMm) and in the electrode path (ablative margin at electrode path, AMe). Results: At both distances, circularity was the highest in the SB mode, followed by the DSM + SB mode, and was the lowest in the DSM mode. The circularity of the ablation zone showed a significant difference among the three energy groups (p < 0.001 and p = 0.002 for 25-mm and 20-mm, respectively). All size measurements, AMm, and AMe were the greatest in the DSM mode, followed by the DSM + SB mode, and the lowest were with the SB mode (all statistically significant). The white zone proportion in AMm and AMe were the greatest in the SB mode, followed by the DSM + SB mode and DSM in general. Conclusion: DSM and SB appear to be complementary in creating an ideal ablation zone. RFA with the SB mode can efficiently eradicate tumors and create a circular ablation zone, while DSM is required to create a sufficient ablative margin and a large ablation zone.

Study of microstructure of carbon-based materials in plasma wind tunnel testing

  • Kang, Bo-Ram;Lim, Hyeon-Mi;Oh, Phil-Yong;Hong, Bong Guen
    • Proceedings of the Korean Vacuum Society Conference
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    • 2016.02a
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    • pp.200.2-200.2
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    • 2016
  • Carbon-based materials have been known as ablative material and have been used for thermal protection systems. Ablation is an erosive phenomenon that results in thermochemical and thermomechanical changes on materials. Ablation resistance is one of the key properties that determines performance and life-time of the thermal protection material under ablative conditions. In this study, ablation properties of graphite, 3-dimensional (C/C) composites (needle-punched type and rod type) were investigated byusing a plasma wind tunnel which produce a supersonic plasma flow from a segmented arc heater with the power level of 0.4 MW. The mass losses and surface roughness changes which contain main result of the ablation are measured. A morphological analysis ofthe carbon-based materials, before and after the ablation test, are performed through field emission scanning electron microscopy (FE-SEM) and non-contact 3D surface measuring system. Electronic balance and a portable surface roughness tester were used for evaluation of the recession and mass loss of the test samples.

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Microstructure and Ablation Performance of CNT-phenolic Nanocomposites (삭마 효과에 대한 CNT-페놀 나노복합재료의 미세구조 분석)

  • Wang, Zuo-Jia;Kwon, Dong-Jun;Park, Jong-Kyoo;Lee, Woo-Il;Park, Joung-Man
    • Composites Research
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    • v.26 no.5
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    • pp.309-314
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    • 2013
  • Highly ablation resistant carbon nanotube (CNT)-phenolic composites were fabricated by the addition of low concentrations of CNT nanofiller. Tensile and compressive properties as well as ablative resistance were significantly improved by the addition of only 0.1 and 0.3 wt% of uniformly dispersed CNTs. An oxygen-kerosene-flame torch and a field emission scanning electron microscope (FE-SEM) were used to evaluate the ablative properties and microstructures of these CNT-phenolic composites. Thermal gravimetric analysis (TGA) revealed that the ablation rate was lower for the 0.3 wt% CNT-phenolic composites than for neat phenolic or the composite with 0.1 wt% CNT. Ablative mechanisms for all three materials were investigated using this TGA in conjunction with microstructural studies using a FE-SEM. The microstructural studies revealed that CNT acted as an ablation resistant phase at high temperatures, and that the uniformity of dispersion of the CNT played an important role in this resistance to ablation.

Mechanical Properties of Carbon/Phenolic Ablative Composites (Carbon/Phenolic 내열 복합재료의 기계적 특성)

  • Kim, P.W.;Hong, S.H.;Kim, Y.C.;Yeh, B.H.;Jung, B.
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 1999.11a
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    • pp.160-163
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    • 1999
  • The mechanical properties and failure behaviour of carbon/phenolic composites were inverstigated by tension and compression. Carbon/phenolic composites were fabricated by infiltration of matrix into 8 harness satin woven fabric of PAN-based carbon fibers. The tensile and compressive tests were performed at 25℃ under air atmosphere and, at 400℃ and 700℃ under N₂ atmosphere. The tensile strengths of carbon/phenolic composites in with-laminar/0° warp direction were about 10 times higher than those in with-laminar/45° warp direction, which was analyzed due to a change of fracture mode from fiber pull-out by shear to tensile fracture of fibers. The fracture of carbon/phenolic composites in with-laminar/45° direction was analyzed due to delamination by buckling. Tensile and compressive strength of carbon/phenolic composites decreased to about 50% at 400℃, and to about 10% at 700℃ compared to that at room temperature. The main reason for the decrease of tensile or compressive strength with increasing temperature was analyzed due to a reduction of bond strength between fibers and matrix resulting from thermal degradation of phenolic resin.

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Fabrication of Full-Scale Combustion Chamber of Liquid Rocket Engine for Ground Hot Firing Tests (실물형 고압 연소기의 연소시험 검증용 제작)

  • Kim Jonggyu;Seo Seonghyeon;Kim Seunghan;Han Yeoungmin;Ryu Chulsung;Seol Wooseok
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • v.y2005m4
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    • pp.305-308
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    • 2005
  • This paper presents a fabrication of a full-stale combustion chamber of a liquid rocket engine for a ground hot firing test. Engine drawings for manufacturing were prepared after conceptual and detail designs. The combustor is composed of a head and a chamber. SUS316L is used for materials of the head because of the good quality in low temperature. Inner materials of the ablative cooling chamber is silica/phenolic and outer case materials is the SUS316L. Materials of the regenerative cooling chamber are C18200 and SUS316L. After lathe, general milling and MCT machinings, components were finished by electrolytic polishing. A brazing method was applied for bonding the injectors and the injector plate, the regenerative cooling chamber because of structure configurations.

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