• 제목/요약/키워드: Z.-M. method

검색결과 629건 처리시간 0.021초

Phyto-Sociological Study of Resource Plant in Mt. Daedun

  • Lee, Yoon-Won
    • Plant Resources
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    • 제2권2호
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    • pp.113-126
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    • 1999
  • Through the research of tracheophytes type around Mt. Daedun, we are aiming at figuring out the habitat condition of useful resource plants by the classification of vegetation units and communities using the Z-M phyto-sociological method in the basis of the traits of species composition and by the analysis of vegetation and environment by way of coincidence method. Tracheophytes in our research sites was classifid into 117 family, 475 genus 797, species 102 variety,18 breed, in total to 917 kinds. The forest around Mt. Daedun district was classified into 6 communities, 12 groups, 2 sub-groups according to feature species group, differential species group and differential. Judging the result from the examination of community classification factors by the coincidence method, vegetation unit was decided by altitude and topography.

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Predicting Scour at Bridge Piers

  • Briaud, Jean-Louis
    • 한국지반공학회:학술대회논문집
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    • 한국지반공학회 1999년도 봄 학술발표회 논문집
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    • pp.3-46
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    • 1999
  • A new method called SRICOS is proposed to predict the scour depth z versus time t around a cylindrical bridge pier of diameter D founded in clay. The steps involved are ; 1. taking samples at the bridge pier site, 2. testing them in an Erosion Function Apparatus called the EFA to obtain the scour rate z versus the hydraulic shear stress applied $\tau$, 3. predicting the maximum shear stress r max which will be induced around the pier by the water flowing at ν Ο before the scour hole starts to develop, 4. using the measured z versus r curve to obtain the initial scour rate zi corresponding to r max , 5. predicting the maximum depth of scour zmax for the pier, 6. using zi and zmarx to develop the hyperbolic function describing the scour depth z versus time t curve, and 7. reading the z vs. t curve at a time corresponding to the duration of the flood to find the scour depth which will develop around the pier. A new apparatus is developed to measure the z vs t curve of step 2, a series of advanced numerical simulations are performed to develop an equation for the $\tau$ max value of step 3, and a series of flume tests are performed to develop an equation for the zmax value of step 5. The method is evaluated by comparing predictions and measurements in 42 flume experiments.

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알콕사이드로부터 Si-Al-O-N계 분말합성 II. 알콕사이드로부터 합성한 Si3N4 및 $\beta$-Sialon의 분말 및 소결체의 특성 (Synthesis of Powder of the System Si-Al-O-N from Alkoxides II. Properties of Powders and Sintered Ceramics of Si3N4 and $\beta$-Sialon Prepared from Alkoxides)

  • 이홍림;전명철
    • 한국세라믹학회지
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    • 제26권2호
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    • pp.201-209
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    • 1989
  • Fine Si-Al-OH coprecipitate powders were prepared from Si- and Al-alkoxides by the hydrolysis method. $\beta$-Sialon powder was obtained from prepared Si-Al-OH coprecipitate by the simultaneous reduction and nitridation method. The syntehsized Sialon powder was pressureless sintered at 175$0^{\circ}C$ for 90 min in N2 atmosphere. The characterization of the Sialon powder was performed with XRD, BET, SEM, TEM and particle size analysis. The sinterability and mechanical properties of sintered bodies were investigated in terms of relative density, M.O.R., fracture toughness, hardness and the morphology of microstructure. The highest values of their mechanical properties were obtained for the $\beta$-Sialon ceramics at Z=1 and those values are as follows : M.O.R., KIC and HV of $\beta$-Sialon ceramics(Z=1) are 499.1 MPa, 5.9MN/m3/2 and 18.7GPa, respectively.

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인체 혈장중 라베프라졸의 정량을 위한 LC-MS/MS 분석법 검증 및 단일 용량 투여에 의한 약물동태 연구 (Validation of LC-MS/MS Method for Determination of Rabeprazole in Human Plasma : Application of Pharmacokinetics Study)

  • 탁성권;서지형;류주희;최상준;이명재;강종민;이진성;홍승재;임성빈;이경태
    • Journal of Pharmaceutical Investigation
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    • 제39권1호
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    • pp.73-78
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    • 2009
  • A simple LC-MS/MS method of rabeprazole in human plasma was developed and validated. Rabeprazole and Internal standard (I.S), omeprazole, were extracted from human plasma by liquid liquid extraction, chromatographic separation of rabaprazole in plasma was achieved at $45^{\circ}C$ with a Shiseido UG120 $C_{18}$ column and methanol-10 mM ammonium acetate buffer (pH 9.42 with ammonium water), as mobile phase. Rabeprazole produced a protonated precursor ion [$(M+H)^+$] at m/z 360.10 and corresponding product ion at m/z 242.21. Internal standard produced a protonated precursor ion [$(M+H)^+$] at 346.09 and corresponding product ion at m/z 198.09. This method showed linear response over the concentration range of $1{\sim}500\;ng/mL$ with correalation coefficient greater than 0.99. The lower limit of quantitation (LLOQ) using 0.2 mL plasma was 1 ng/mL, which was sensitive enough for pharmacokinetics studies. The method was specific and validated with a limit of quantitation of 1 ng/mL. The intra-day and inter-day precision and accuracy were acceptable for all samples including the LLOQ. The applicability of the method was demonstrated by analysis of plasma after administration of a single 10 mg dose to 36 healthy subject. From the plasma rabeprazole concentration versus time curves, the mean $AUC_t$ (The area under the plasma concentration-time curve from time 0 to 12 hr ) was $691.36{\pm}321.88\;ng{\cdot}hr/mL$, $C_{max}$ (maximum plasma drug concentration) of $353.21{\pm}131.52\;ng/mL$ reached $3.4{\pm}1.1\;hr$ after adiministration. The mean biological half-life of rabeprazole was $1.37{\pm}0.75\;hr$. Based on the results, this simple method could readily be used in pharmacokinetics studies.

식품 중 플루오로퀴놀론계 항생제의 분석 (Analysis of Fluoroquinolone Antibiotics in Foods)

  • 김희연;신민수;최희주;박세종;송재상;정소영;최선희;이화정;김영선;최재천
    • 한국식품과학회지
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    • 제41권6호
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    • pp.636-643
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    • 2009
  • 총 388건의 시료를 분석한 결과, 닭 143건 중 총 12건의 플루오르퀴놀론계 항생제가 검출되었으며 다른 식품군에서는 모두 불검출 되었다. 항생제 별로 보면 엔로플록사신이 12건으로 가장 많았고 시프로플록사신이 5건, 노르플록사신이 1건 순이었다. 검출농도는 엔로플록사신이 0.01-0.73 mg/kg, 시프로플록사신이 0.01-0.03 mg/kg 및 노르플록사신이 0.12 mg/kg이었다.

THE EVOLUTION OF THE GALACTIC GLOBULAR CLUSTERS.: II. HELIUM ABUNDANCES AND AGES

  • Lee, See-Woo
    • 천문학회지
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    • 제18권2호
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    • pp.41-69
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    • 1985
  • For the well observed 16 globular clusters with known metal abundance (Z), the helium abundances (Y) and ages are determined by various methods, and the relations between Y, Z and age are examined. The luminosity $L_{RR}$ of RR Lyrae stars is known to be dependent of evolutionary models and pulsation theory in the sense that the pulsation theory and horizontal branch (HB) models yield the anticorrelation between $L_{RR}$ and Z whereas main sequence (MS) and red giant branch (RGB) models yield the direct correlation between them. Similarly the anticorrelation between Y and Z is obtained from the HB models and pulsation theory whereas the direct correlation between them is obtained when the RGB model is applied. The current evolutionary models yield the anticorrelation between Z and age of clusters whenever the direct correlation between Y and Z holds. However when the anticorrelation between Y and Z is applied for age determination, the similar age of clusters is obtained as shown by Sandage (1982b). The ages, which are determined by the fitting of C-M diagrams to isochrones in the ($M_v$, B-V)-plane, suggest the two different chemical enrichment processes, which could be accounted for by the disk-halo model for the chemical evolution of the Galaxy (Lee and Ann 1981). Also it is known that the R-method is very useful for Y-determination and the derived Y's show the increasing rate of $\frac{{\Delta}Y}{{\Delta}Z}{\simeq}0.5$ which is comparable to the observed value of $\frac{{\Delta}Y}{{\Delta}Z}{\simeq}0.3$ from HII regions and planetary nebulae by Peimbert and Torres-Peimbert (1976). In this case, the age-metallicity relation of globular clusters could be explained by the disk-halo model.

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육방정 페라이트의 결정과 Block 구조 (Crystal and Block Structures of Hexagonal Ferrites)

  • 신형섭
    • 한국세라믹학회지
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    • 제49권3호
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    • pp.205-215
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    • 2012
  • It has been studied the crystal and block structures of the hexagonal ferrites with M, W, Y and Z types prepared by various coprecipitation-oxidation method. The structures have been refined with a Rietveld analysis of the powder X-ray diffraction pattern with high precision ($R_{WP}$ <0.09, $R_I$ <0.03). The density difference between the S-blocks was proportioned to the cobalt contents in hexagonal ferrites, but that between the R or T-blocks was relatively small. Compared with the blocks and cation-oxygen polyhedra in BaM ($BaFe_{12}O_{19}$), those were bulky to the normal direction for the c-axis in $Co_2W$ ($BaCo_2Fe_{16}O_{27}$) and to the parallel direction for the c-axis in $Co_2Y$ ($Ba_2Co_2Fe_{12}O_{22}$) and $Co_2Z$ ($Ba_3Co_2Fe_{24}O_{41}$). The S-blocks of $Co_2W$, $Co_2Y$, and $Co_2Z$ were unstable and distorted. Because the T-block of $Co_2Z$ was unstable, the T-block was decomposed into the Ba-rich phase and $Co_2W$ at high temperatures above $1200^{\circ}C$. A standard powder X-ray diffraction pattern for $Co_2Z$ was proposed as well.

실습선 아라호(M.S. A-RA)의 조종성능에 관한 연구 (A Study on the Maneuverabilities of the Training ship M.S. A-RA)

  • 안영화;박명호;최환문;정용진
    • 수산해양기술연구
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    • 제37권4호
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    • pp.275-284
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    • 2001
  • 본 연구에서는 제주대학교 실습선 아라호(G/T : 990tons)의 조종 성능을 파악하기 위하여 2000년 8월과 2001년 5월에 2회에 걸쳐 제주항 북방 3마일 해상에서 조타에 의한 선회성과 추종성 등의 조종성능을 실시한 결과는 다음과 같다. 1. 부표 방위반법으로 측정한 선회권의 크기에서 선회종거는 우현선회시가 198m, 좌현선회시가 192m로서 좌현선회시가 우현선회시보다 6m 작았으며, 또한, 선회경의 크기는 우현선회시가 194m, 좌현선회시가 188m로서 좌현선회시가 우현선회시 보다 6m 작았다. 2. DGPS 측위에 의한 선회권의 크기에서 선회종거는 우현선회시가 196m, 좌현선회시가 194m로서 좌현선회시가 우현선회시보다 2m 작았다. 또한, 선회경의 크기는 우현선회시가 194m, 좌현선회시 190m로서 좌현선회시가 우현선회시보다 4m 작았다. 3. 신조 시운전시 부표 방위반법에 의해 측정한 선회권의 크기와 2001년 5월에 DGPS 측위에 의하여 측정한 선회권의 크기를 비교해 본 결과, 선회종거는 DGPS 측위에 의한 선회권이 신조시운전시 선회종거보다 우현선회시가 1m 컸으며, 좌현선회시가 21m 작았다. 또한, 선회경의 크기는 우현선회시 16m, 좌현선회시 23m 작았다. 4. 선속 13k't로 전속 전진중 타각 $35^\circ$로 좌현 또는 우현으로 전타 했을 때 선회각 $180^\circ$에서 선속이 7.8k't이고 $360^\circ$선회시는 6.0k't가 되었으며, 소요 시간은 좌현선회시가 150초, 우현선회시가 156sec로 좌현선회시가 우현선회시보다 6초 짧았으며, 선회평균 각속도는 좌현선회시가 $2.4^\circ$/sec, 우현선회시가 $2.3^\circ$/sec였다. 5. 타각 $10^\circ$, $20^\circ$, $30^\circ$ Z시험에서 선회성지수 K와 추종성지수 T는 각 각 선회성지수는 1.24, 1.45, 1.65였으며, 추종성지수는 각 각 0.33, 0.20, 0.14가 되어 $30^\circ$인 경우가 $10^\circ$, $20^\circ$ Z시험에서 보다 선회성지수 K는 크고, 추종성지수 T는 작아서 대각도 조타일 때가 소각도 조타일 때 보다 조종성능이 양호하였다.

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Filter Hybridization 방법에 의한 Surfactant Protein B mRNA의 정량측정 (Quantitative Measurement of Surfactant Protein B mRNA by Filter Hybridization)

  • 박성수;이동후;신동호;이정희
    • Tuberculosis and Respiratory Diseases
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    • 제39권3호
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    • pp.242-247
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    • 1992
  • 연구배경 : Surfactant 단백은 surfactant의 물리학적 성상의 결정 및 대사를 조절하는데 있어서 중요한 역할을 한다. 유전자 발현의 조절을 연구하기 위하여서는 cDNA의 탐지자에 의한 mRNA의 정량측정이 중요하다. 방법 : 쥐의 surfactant 단백 B의 cDNA에 대한 coding 부위를 PGem 3Z 또는 4Z에 subclone하여 SP6 RNA polymerase 효소를 이용하여 antisense와 sense을 얻었다. Sense을 이용한 filter hybridization올 시행하여 정상곡선을 얻었다. Antisense는 $^{32}P$를 표지시켜 탐지자로 이용하였다. 결과 : SP-B에 대한 sense 복사체의 정상곡선은 Y=2034.9X+159.1(X=SP-BmRNA 복사체, Y=CPM)이고, 상관계수는 1.0이었다. 결론 : 이상의 결과로 filter hybridization 방법은 mRNA을 정량측정 하는데 있어서 빠르고, 재현성이 높으며, 많은 시료를 한꺼번에 시행할 수 있는 유용한 방법이다.

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참당귀(Angelica gigas Nakai) 중 Decursin 및 Decursinol Angelate의 분리 및 정제 (Isolation and Purification of Decursin and Decursinol Angelate in Angelica gigas Nakai)

  • 김강민;정재연;황성우;김묘정;강재선
    • 한국식품영양과학회지
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    • 제38권5호
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    • pp.653-656
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    • 2009
  • 생약재로 사용 중인 Angelica gigas Nakai의 decursin 및 decursinol angelate를 60% ethanol로 최종적으로 추출 후 recycling HPLC 및 HPLC/MS에 의해 각각을 분리하였다. 60% ethanol로 $-20^{\circ}C$에서 추출하였을 경우 95% 순도의 decursin 및 decursinol angelate를 얻을 수 있었고 10번 이상의 recycle를 통해서 순수한 decursin 및 decursinol angelate를 분리할 수 있었다. 분리한 decursin 및 decursinol angelate를 HPLC/MS를 통해 분자량을 확인하였을 경우 m/z=329($[M+H]^+$) 및 m/z=351($[M+Na]^+$)과 같은 결과를 얻을 수 있었다. 이 분리 방법을 통해 decursin 및 decursinol angelate를 통한 의약품 및 식품 등에 관한 여러 연구에 있어 두 물질 각각에 대한 약리학적 효과를 도출하는데 기여할 것이며, 물질표준화에 기여할 것으로 사료된다.