• Title/Summary/Keyword: YBCO films

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Optimization of process variables in batch-type MOD process (일괄처리방식을 이용한 MOD 공정의 변수 최적화)

  • Chung, Kook-Chae;Yoo, Jai-Moo;Ko, Jae-Woong;Kim, Young-Kuk;Wang, X.L.;Dou, S.X.
    • Progress in Superconductivity and Cryogenics
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    • v.8 no.1
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    • pp.23-25
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    • 2006
  • Optimization of process variables, including oxygen and water partial pressure and also an nesting temperature, was performed in batch-type process to fabricate YBCO films on LaAlO3 single crystal. In this work, YBCO oxide powder was used as a starting precursor for metal-organic deposition(MOD)method. The precursor films were fabricated in batch furnace and they were converted to the epitaxial YBCO films at the same furnace with varying the process variables. The oxygen partial pressure was varied from 100ppm to 2000ppm and the water partial pressure from 1.2% to 12.2%. The window for optimal P(O2) was narrow about 700ppm for batch-type process. YBCO films in bathc-thype MOD process were optimized at 740-770oC and P(H2O) of 2.3%-7.3%.

Development of new current path pattern of YBCO thin films for Superconducting fault current limiters (초전도 한류기용 YBCO 박막 전류 Path Pattern 개발)

  • Lee B. W.;Kang J. S.;Park K. B.;Oh I. S.
    • Progress in Superconductivity
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    • v.6 no.2
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    • pp.113-117
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    • 2005
  • In this study, electromagnetic analysis of current paths including meander pattern, spiral pattern, and bi-spiral pattern were performed and in order to verity the analysis results, experiments tests including quench test, and insulation tests were performed. In addition, bubble corner concepts were introduced to enhance insulation reliability. From our study, bi-spiral pattern of YBCO thin films were rather effective for quench and insulation than the other patterns. So this current path pattern was adopted for YBCO thin films in order to develop 6.6 kV resistive fault current limiters. Finally YBCO thin films were connected in series and parallel to enhance capacity, and the test results of current limiting characteristics of 6.6kV resistive SFCL were successful. The Progress in Superconductivity is published every six month and serves as a channel for publications on superconductivity and related topics. The author(s) are required to submit THREE copies of the manuscripts along with original figures directly to the Editor.

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Structural and Electrical Properties of Semiconducting YBCO Thin Film Annealed at Various Temperatures for Uncooled Infrared Sensor Application (비냉각형 적외선 센서로 응용하기 위한 반도성 YBa2Cu3O6+x 박막의 열처리 온도에 따른 구조적 전기적 특성)

  • Lee, Tae-Ho;Lee, Sung-Gap;Yeo, Jin-Ho;Jung, Hye-Rin
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.26 no.10
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    • pp.731-735
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    • 2013
  • YBCO thin films on $SiO_2$/Si substrate were fabricated by spin-coaing of an alkoxide-derived precursor and heat treatment. The structural and electrical properties of the YBCO films were investigated as functions of annealing temperature at $600{\sim}800^{\circ}C$. Although YBCO single phase was not synthesized, dense films of YBCO matrix phase and minor second phases have been successfully fabricated at the annealing temperatures of $650{\sim}800^{\circ}C$. Thickness and temperature coefficient of resistance (TCR) of YBCO thin films with annealing temperature of $750^{\circ}C$ were 0.31 ${\mu}m$ and $-2.92%/^{\circ}C$, respectively.

Quench Behaviors of Superconducting YBCO Films for Fault Current Limiter Using Magnetic Fields (자기장이 인가된 YBCO 박막형 한류기의 ?치 특성)

  • 박권배;이방욱;강종성;오일성;최효상;현옥배
    • Proceedings of the Korea Institute of Applied Superconductivity and Cryogenics Conference
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    • 2002.02a
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    • pp.365-367
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    • 2002
  • A serious problem in using YBCO films for fault current limiter is inhomogeneities caused by imperpect manufacturing. So simultaneous quenches are a difficult problem which elements for current limiting are connected in series for increasing voltage ratings. We investigated extended electric field - current characteristics for current limiting element of YBCO film when 0-130mT magnetic field is applied. And quench characteristics were investigated in over all element and between elements of YBCO films. From the experiments, it was shown that applied magnetic fields using solenoid coil induced uniform quench distribution for over all stripes and simultaneous quench in all elements for current limiting of YBCO film was realized.

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MOD-processed YBCO thin films prepared by chemically controlled precursor solution (화학적으로 제어된 전구체용액을 사용하여 MOD법으로 제조된 YBCO 박막)

  • 유재무;김영국;고재웅;허순영;홍계원;이희균;김철진;정경원
    • Proceedings of the Korea Institute of Applied Superconductivity and Cryogenics Conference
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    • 2003.10a
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    • pp.27-29
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    • 2003
  • Solution-based MOD-TFA deposition technology of YBCO layers offers a route to low-cost YBCO coated conductors. Since the structures and properties of grown thin film by MOD process are strongly influenced by chemistry of precursor solution, the chemical modification of precursor solution for MOD process are important for improvement of the electrical properties of YBCO films. In this study, the precursor solution for MOD process are modified by chemical additives and solvents. The microstructure and texture of YBCO films grown by chemically modified precursor solution were characterized with SEM/EDS, XRD.

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Oxide precursor-based MOD processing of YBCO thin films

  • Kim, Young-Kuk;Yoo, Jai-Moo;Ko, Jae-Woong;Chung, Kook-Chae;Heo, Soon-Young
    • Progress in Superconductivity and Cryogenics
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    • v.6 no.4
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    • pp.5-8
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    • 2004
  • A low cost MOD processing using YBCO oxide powder as a starting precursor was employed for fabrication of YBCO thin films. YBCO oxide is advantageous over metal acetates or TFA salts which are popular starting precursors for conventional MOD-TFA process. YBCO thin films were prepared by oxide-precursor-based MOD process and annealing condition was optimized. The YBCO thin film annealed at 78$0^{\circ}C$ shows no transport $I_c$ and poor microstructure. However, the YBCO thin film annealed at higher temperature shows improvement in microstructure and current transport property. In order to improve critical current, YBCO thin film was prepared by double coating method. YBCO thin film prepared with double coating approach shows enhanced superconducting performance ($I_c$>100A/cm-w).

Fabrication of Cu-Sheathed YBCO Thick Films by Screen Printing Method Using $Y_2$BaCu$O_5$ and BaC$O_3$ Powders (Y211 및 BaCO$_3$ 분말로 Screen Printing 법을 이용한 Cu-sheath의 YBCO 후막 제조)

  • 김경진;한상철;한영희;박병삼;정년호;윤희중;오제명;최희락;성태현
    • Progress in Superconductivity
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    • v.5 no.2
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    • pp.132-135
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    • 2004
  • We fabricated YBCO thick films by using a screen printing method with $Y_2$BaCuO$_{5}$(Y211) and BaCO$_3$ powders on Cu-substrate in $N_2$ atmosphere. Cu-sheathed YBCO thick film process is more simple and economic than YBCO coated conductor methods. The heat treatment is performed in the range of 860 - 875 $^{\circ}C$ for 5 min in the tube furnace of $N_2$ atmosphere. The flow rate of $N_2$ gas is fixed 60 $m\ell$/min. Microstructure and phases of thick films were investigated by optical microscope, X-ray diffraction(XRD) and SEM. At heat-treatment temperature, the thick films were partially melted by liquid reaction between CuO of oxidized copper substrate and the powders screen-printed on Cu-sheath. During the heat-treatment procedure, YBCO superconducting grains nucleate.e.

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Characteristics of $YBa_2Cu_3O_{7-x}$ Thin Films on $SrTiO_3$ substrate with surface modification by Au nanoparticles (STO기판에 금 나노입자가 분산된 YBCO 박막의 특성)

  • Oh, Se-Kweon;Jang, Gun-Eik;Tran, Hai Duc;Kang, Byoung-Won;Lee, Cho-Yeon;Hyun, Ok-Bae
    • Progress in Superconductivity and Cryogenics
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    • v.12 no.3
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    • pp.7-11
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    • 2010
  • For many large-scale applications of high-temperature superconducting materials, large critical current density($J_c$) in high applied magnetic fields are required. A number of methods have been reported to introduce artificial pinning centers(APCs) in $YBa_2Cu_3O_{7-\delta}$(YBCO) films for enhancement of their $J_c$. In this work, we investigated electric characteristic of YBCO films on $SrTiO_3$ (100) substrates whose surfaces were modified by the introduction of Au nanoparticles (AuNPs). Au nanoparticles were uniformly dispersed on STO substrates with one of typical solution techniques, self assembled monolayer. After heating the STO substrates with Au nanoparticles, the size of Au nanoparticles was around 29~32 nm in height and 41~49 nm in diameter. XRD diffraction patterns taken on the YBCO film with Au nanoparticles show the c-axis orientation. The measured $T_c$ of YBCO /AuNPs films was around 89K and the $J_c$ was 0.75 MA/$cm^2$ at 65 K and 1 T.

Influence of PEG addition on the surface properties of YBCO Thick Films (PEG 첨가에 의한 YBCO 후막 표면 변화)

  • Soh, Dea-Wha;Jeon, Yong-Woo;Cho, Yong-Joon;Korobova, Natalya
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2003.05c
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    • pp.53-56
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    • 2003
  • The properties of YBCO thick film coated on Ag wire with YBCO powder is deeply affected by cracking on its surface which was deposited in organic solution by electrophoretic method. YBCO superconducting thick films were prepared on Ag wire$({\Psi}0.8mm)$ by electrophoresis in acetone with added PEG (Poly-Ethylene Glycol, 3% in Acetone), 1ml for being crack-free. The surface properties of YBCO superconducting wire was evidently improved with adding PEG. Added PEG which molecular weight is 600, 1000, 3400 was affected with variation of deposition voltages to the surface properties of samples. As a result, with adding PEG (its molecular weight is 3400), YBCO superconducting wire was better on its surface properties.

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The Effect of the Addition of BZO Nanopowder in the YBCO PLD Targets on the Flux Pinning Properties of BZO-YBCO Thin Film (YBCO PLD 타겟에 BZO 나노분말 첨가에 따른 PLD-YBCO 박막의 자속고정 효과)

  • Song, K.J.;Ko, R.K.;Lee, Y.S.;Park, Y.M.;Yang, J.S.;Kim, H.S.;Ha, H.S.;Ha, D.W.;Kim, S.W.;Oh, S.S.;Kim, D.J.;Park, C.;Yoo, S.I.
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2005.11a
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    • pp.20-21
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    • 2005
  • [ $BaZrO_3$ ], nanopowder was added to YBCO powder to make ($BazrO_3)_x(YBCO)_{(100-x)mol.-%}$ ($BZO_x$-YBCO) ($0{\leq}x{\leq}10$) composite targets fur pulsed laser deposition of superconducting layer in order to investigate the effect of the addition of BZO nanopowder in the YBCO target on the flux pinning properties of $BZO_x$-YBCO thin films. All the $BZO_x$-YBCO thin films were grown on single crystal STO substrate under similar conditions in the PLD chamber. The effect of YBCO targets doped with BZO on the flux pinning properties of $BZO_x$-YBCO thin films has been investigated comparatively. The isothermal magnetizations M(H) of the films were measured at temperatures between 5 and 80 K in fields up to 5 T, employing a PPMS. The optimal amount of BZO nanopowders in $BZO_x$-YBCO thin films to obtain the strongest flux pinning effects at high magnetic fields is about 6 mol.-%.

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