• 제목/요약/키워드: XRD analysis

검색결과 2,604건 처리시간 0.038초

펄스 레이저 증착법에 의해 제작된 ZnO-Si-ZnO 다층 박막의 특성 분석 (Characteristics analysis of ZnO-Si-ZnO multi-layer thin films by pulsed laser deposition)

  • 강홍성;강정석;심은섭;방성식;이상렬
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2002년도 하계학술대회 논문집 Vol.3 No.2
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    • pp.1057-1059
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    • 2002
  • ZnO-Si-ZnO multi-layer thin films have been deposited by pulsed laser deposition (PLD). And then, the films have been annealed at $300^{\circ}C$ in oxygen ambient pressure. Electrical properties of the films were improved slightly than ZnO thin film without Si layer. Also, the optical and structural properties changed by Si layer in ZnO thin film. The optical and structural properties of Si-doped ZnO thin films were characterized by PL(Photoluminescence) and XRD(X-ray diffraction method) respectively. Electrical properties were measured by van der Pauw Hall measurements.

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전기로 더스트의 고체탄소에 의한 환원반응속도 (Reduction Rate of Electric Arc Furnace Dust with Solid Carbon)

  • 박병구;이광학;김영홍;신형기
    • 자원리싸이클링
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    • 제7권1호
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    • pp.34-40
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    • 1998
  • 본 연구에서는 고체탄소 첨가량에 의한 전기로 더스트의 환원반응속도에 관하여 조사하였다. $930~1080^{\circ}C$의 반응온도에서 환원 반응 속도식을 얻었으며, 반응시간에 따른 전기로 더스트의 아연제거율과 산화철의 금속화율을 구하였다. 또한 XRD 분석결과, 슬래그 잔재는 Akermanite[${Ca}_{2}{MgSi}_{2}{O}_{7}$]의 혼합물과 $SiO_2$가 잔존함을 알 수 있었다.

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Self-Cleaning and Photocatalytic Performance of TiO2 Coating Films Prepared by Peroxo Titanic Acid

  • Yadav, Hemraj M.;Kim, Jung-Sik
    • 한국재료학회지
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    • 제27권11호
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    • pp.577-582
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    • 2017
  • Self-cleaning and photocatalytic $TiO_2$ thin films were prepared by a facile sol-gel method followed by spin coating using peroxo titanic acid as a precursor. The as-prepared thin films were heated at low temperature($110^{\circ}C$) and high temperature ($400^{\circ}C$). Thin films were characterized by X-ray diffraction(XRD), Field-emission scanning electron microscopy(FESEM), UV-Visible spectroscopy and water contact angle measurement. XRD analysis confirms the low crystallinity of thin films prepared at low temperature, while crystalline anatase phase was found the for high temperature thin film. The photocatalytic activity of thin films was studied by the photocatalytic degradation of methylene blue dye solution. Self-cleaning and photocatalytic performance of both low and high temperature thin films were compared.

경남 창녕군 영산지역에서 산출하는 팔리고르스카이트의 광물학적 연구 (Mineralogy of Palygorskite from the Yeongsan Area in Kyeongnam, Korea)

  • 황진연
    • 한국광물학회지
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    • 제9권1호
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    • pp.26-34
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    • 1996
  • The white leather-like playgorskite occurs as a vein in the Cretaceous sedimentary rocks in the Yeongsan area, Kyeongnam, Korea. It has been investigate by means of XRD, TEM, DTA-TG, IR and chemical analysis. The palygorskite vein is composed mostly of well-crystallized palygorskite. The wall rock of the vein is altered to smectite along both sides of the vein. According to TEM observation the palygorskite shows a fibrous habit. The sizes offibers are quite variable, ranging from 0.1 to 3.0 micron in length. From XRD data, the palygorskite has orthorhombic unit cell with a=12.726$\AA$, b=17.796$\AA$, c=5.1666$\AA$. The chemical formula of the palygorskite was calculated as [Si7.93Al0.07](Al1.91Fe+30.11Mg1.96)Ca0.01O20(OH)4(OH2)2.

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Dip-coating법에 의한 ${alpha}-Fe_2O_3$막 제조에 관한 연구 (A study on the preparation of ${alpha}-Fe_2O_3$films by dip-coating method)

  • 강경원;정용선;현부성;오근호
    • 한국결정성장학회지
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    • 제8권2호
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    • pp.292-298
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    • 1998
  • 출발원료로 ferric nitrate, ethylene glycol, acethyl acetone 혼합용액을 사용하여 dip-coating된 ${\alpha}-Fe_2O_3$ 막을 제조하였다. coating을 위한 혼합용액의 시간 경과에 따른 용액내의 가교(polymerization) 효과를 관찰하기 위해서 적외선 분광기(FT-IR)를 사용하였고, 막 형성시 유기물 분해 및 결정화 시작온도를 확인하기 위하여 FT-IR, XRD, DSC 등을 이용하여 분석을 행하였다. 또한 AFM과 SEM을 통하여 각 조건에서 제조된 막의 표면상태 및 두께 변화에 대하여 관찰되었다.

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VGF법을 이용한 $Bi_2Te_{2.55}Se_{0.45}$의 일방향 응고에 관한 연구 (Unidirectional Solidification of $Bi_2Te_{2.55}Se_{0.45}$ using a VGF Method)

  • 김영희;김기수;김수룡;정상진;이윤주;박동선
    • 한국결정학회지
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    • 제14권2호
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    • pp.62-66
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    • 2003
  • VGF법을 사용하여 CuBr₂ dopant가 첨가된 Bi₂Te/sub 2.55/Se/sub 0.45/ 열전재료를 제조하였다. 이 방법을 사용하여 일방향으로 성장된 Bi₂Te/sub 2.55/Se/sub 0.45/ 잉곳의 제조가 가능하였으며 XRD 분석 결과 우선성장 방향이 (0 1 5)면임이 밝혀졌다. 본 실험을 통하여 제조한 열전재료의 Seebeck 계수와 전기전도도를 373∼523 K 범위에서 측정하였다.

Synthesis and Characterization of CdSe/graphene Nanocomposites and their Catalytic Reusability Studies under Visible Light Radiation

  • Ali, Asghar;Oh, Won-Chun
    • 한국세라믹학회지
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    • 제52권6호
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    • pp.502-507
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    • 2015
  • We examined the photo catalytic activity and catalytic recyclability of CdSe/graphene nanocomposites fabricated via modified hydrothermal technique. The prepared composites were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) with energy dispersive X-ray (EDX), transmission electron microscopy (TEM), Raman spectroscopic analysis, and X-ray photoelectron spectroscopy (XPS). The photocatalytic behavior was investigated through decomposition of RBB as a standard dye under visible light radiation. Our results indicate that there is significant potential for graphene based semiconductor hybrids materials to be used as photocatalysts under visible light irradiation for the degradation of organic dyes from industry effluents.

Bi 첨가량에 따른 BLT 박막의 유전특성 (Dielectric properties of $Bi_{3.25}La_{0.75}Ti_3O_{12}$ thin films with Bi contents)

  • 김경태;김창일;강동희;심일운
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2002년도 하계학술대회 논문집
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    • pp.371-374
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    • 2002
  • Bismuth lanthanum titanate thin films with excess Bi contents were prepared onto Pt/Ti/$SiO_2$/Si substrate by metalorganic decomposition (MOD) technique. The structure and morphology of the films were analyzed using X-ray diffraction (XRD) and atomic force microscopy (AFM), respectively. From the XRD analysis, BLT thin films show polycrystalline structure and the layered-perovskite phase was obtained over 10% excess of Bi contents. As a result of ferroelectric characteristics related to the Bi content of the BLT thin film, the remanent polarization and dielectric constant decreased with increasing over Bi content of 10 % excess. The BLT film with Bi content of 10% excess was measured to have a dielectric constant of n9 and dielectric loss of 1.85[%]. The BLT thin films showed little polarization fatigue test up to 3.5 x $10^{9}$ bipolar switching cycling.

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카복실산으로 표면개질된 다중층 탄소나노튜브의 구조분석 (Structural Analysis of Carboxylic Acid-functionalized Multi-walled Carbon Nanotubes)

  • 김정수;이건웅;오원태
    • 한국전기전자재료학회논문지
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    • 제20권10호
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    • pp.878-882
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    • 2007
  • Carboxylated multi-walled carbon nanotubes (MWNTs) were in detail characterized by XRD, XPS, FTIR, and thermogravimetric measurements. Carboxylic acid groups were functionalized to MWNTs under aqueous acid condition. The changes of sonication and reflux conditions rarely influenced the degree of carboxylation on MWNTs, but decreased the thermal stability of the resultant carboxylated MWNTs. XRD results showed that the diffraction peaks (100), (101), and (102) of pristine MWNTs disappeared after acid treatment, but the diffraction peak (002) was Preserved in the carboxylated MWNTs. The introduction of carboxylic acid groups on MWNTs caused to improve the dispersibility of the resultant carboxylated MWNTs in water.

$50{\mu}m$ 켑톤 기판에 성막된 Polymer/MWCNT 투명 전도막의 미세구조 (Microstructural Properties of the Polymer/MWCNT Transparent Conduction Film Fabricated on the $50{\mu}m$ Kepton Substrate)

  • 장경욱
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2010년도 하계학술대회 논문집
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    • pp.253-253
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    • 2010
  • The Polymer/MWCNT composite films were fabricated by air-spray method under the 2 kg/$cm^2$ pressure using the multi-walled CNTs solution and the polymer on a $50{\mu}m$ kepton film substrates. We obtained the composite films which were sprayed with the MWCNT dispersion. In order to analysis the microstructure for the fabricated Polymer/MWCNT film, we used the X-ray diffraction (XRD) and SEM.

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