• Bulletin of the Korean Chemical Society
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• v.34 no.11
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• pp.3451-3455
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• 2013

Single-crystalline silicon nanowires (SiNWs) were fabricated by using an electroless metal-assisted etching of bulk silicon wafers with silver nanoparticles obtained by wet electroless deposition. The etching of SiNWs is based on sequential treatment in aqueous solutions of silver nitrate followed by hydrofluoric acid and hydrogen peroxide. SEM observation shows that well-aligned nanowire arrays perpendicular to the surface of the Si substrate were produced. Free-standing SiNWs were then obtained using ultrasono-method in toluene. Alkyl-derivatized SiNWs were prepared to prevent the aggregation of SiNWs and obtained from the reaction of SiNWs and dodecene via hydrosilylation. Optical characterizations of SiNWs were achieved by FT-IR spectroscopy and indicated that the surface of SiNWs is terminated with hydrogen for fresh SiNWs and with dodecyl group for dodecyl-derivatized SiNWs, respectively. The main structures of dodecyl-derivatized SiNWs are wires and rods and their thicknesses of rods and wire are typically 150-250 and 10-20 nm, respectively. The morphology and chemical state of dodecyl-derivatized SiNWs are characterized by scanning electron microscopy, transmission electron microscopy, and X-ray photoelectron spectroscopy.

• Applied Chemistry for Engineering
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• v.9 no.7
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• pp.1011-1017
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• 1998

$YBa_2Cu_3O_{6+x}(Y123)-Ag$ high-Tc superconducting wires were fabricated by plastic extrusion technique using pyrophoric synthetic and mechanical mixing powder with and without Ag addition(20 wt.%). This method involves powder preparation, plastic paste making, die extrusion, binder burn-out and the sintering process. In order to fabricate a good-quality superconducting body, it is required to use homogeneous and fine-size power as a starting materials. $Y_2O_3-BaCO_3-CuO$ precursor powders with/without Ag addition were prepared both by pyrophoric synthetic(PS) and mechanical mixing(MM) method of raw powders. The formation kinetics of the powder mixtures into Y123 phase was investigated at various temperatures and times in air atmosphere. The powder prepared by PS method was more easily converted into a Y123 phase than the MM powder. The fine size and good chemical homogeneity of the powder prepared by PS method is attributable to the fast formation into a Y123 phase. The critical current density($J_c$) of the Y123-Ag superconducting wires made by plastic extrusion method were in the range of $150A/cm^2{\sim}230A/cm^2$. depending on the charateristics of starting material powders. $J_c$ of the wire prepared by pyrophoric synthetic powder with 20 wt.% Ag addition was $230A/cm^2$.

• Journal of Sensor Science and Technology
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• v.17 no.1
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• pp.9-14
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• 2008

In this paper, the gas responses of tungsten oxide films prepared by anodic reaction was discussed. Sensing electrodes and heating electrodes were patterned by photolithography method on quartz substrate. Porous tungsten oxide was fabricated in electrolyte solutions of 5 % HF (HF :$C_2H_6OH:H_2O$=3 : 2 : 20) by anodic reaction. The anodic reaction with metal (platinum wire) as a cathode and the sensing device as an anode was conducted under the various reaction times (1-10 min) at 10 mA/$cm^2$ The surface structure and morphology of the fabricated sensor have been analysed by X-ray diffraction (XRD) and field-emission scanning electron microscopy (FE-SEM). All the peaks of XRD results were well indexed to the pure phase pattern. The average diameter of the porous tungsten oxide surface were ranged about 100 nm. The fabricaed sensor showed good sensitivity to 200 ppm toluene at operating temperature of $250^{\circ}C$.

• Analytical Science and Technology
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• v.6 no.2
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• pp.157-165
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• 1993

The potentiostatic etching dissolution method, which had been used for the quantification of precipitates in steel, was applied to investigate the origin of cracks occurred in 304 stainless steel during processing. The morphology of crack propagation was observed by SEM. EDS and EPMA were used for the analysis of chemical composition of large precipitates on the grain boundary. The crystal structure of these large precipitates was determined by X-ray diffraction and electron diffraction. In both a stainless steel plate and a wire, the crack propagated along the grain boundary. Large precipitates on the grain boundary were identified to be $M_2C$ and $M_{23}C_6$. Potentiostatic etching dissolution method was found to be appropriate to the sample preparation for the analysis of precipitates in stainless steel.

• Journal of the Korean Society for Aeronautical & Space Sciences
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• v.37 no.11
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• pp.1080-1088
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• 2009

An actuator using piezoceramic material was designed in order to perform a flow control for flat plate flow. Boundary layer measurements were carried out to explore the flow disturbances by the designed actuator that was activated at low excitation frequency(15Hz). The mean velocity and fluctuation in the boundary layers were measured at $x/{\delta}^*=31.9$ downstream from the actuator tip by a one-dimensional hot-wire probe(55P14). Results reveal that low- and high-velocity regions were observed in the vicinity of the actuator center and in the outer area of the actuator respectively, and the formation of counter-rotating streamwise vortices was predicted. The fluctuations were persistently found in the outer part of the actuator and an inflection point in the spanwise gradient of the streamwise velocity was observed. Boundary layer instability was amplified at both the actuator excitation frequency and the T-S wave frequency when the actuator was excited at low frequency.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.11 no.11
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• pp.1014-1021
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• 1998

We evaluated the effect of processing variables on microstructural evolution interface irregularity between Ag sheath and superconductor core and resultant critical current density(J$_{c}$) of (Bi,Pb)$_2$Sr$_2$Ca$_2$Cu$_3$O$_{x}$(2223) superconductor tape. The value of J$_{c}$ was significantly influenced by the interface irregularity, degree of texturing and relative 2223 content. The interface became more irregular(sausage effect), while the degree of texturing gradually improved as the dimension of tape decreased during forming process. As the dimension of wire/tape were changed from diameter of 3.25 mm to thickness of 0.20 mm, J$_{c}$ value was observed to be increased by 10 times. In addition, optimum sintering temperature for improved J$_{c}$ was observed to be 835$^{\circ}C$ in a ambient atmosphere probably due to combined effect of both improved texturing and high 2223 content. Microstructural investigation showed the degree of texturing was degraded by the existence of both second phases and interface irregularity. It was observed that larger grain size and better texturing was developed near relatively flat interface compared to those inside superconducting core.ting core.

• Journal of the Korean Institute of Telematics and Electronics
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• v.27 no.12
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• pp.1878-1888
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• 1990

In this paper, the input-output interconnection method of the multi-valued signal processing circuit using perfect Shuffle technique and Kronecker product is discussed. Using this method, the design method of circuit of the multi-valued Reed-Muller expansions(MRME) to be used the multi-valued signal processing on finite field GF(p**m) is presented. The proposed input-output interconnection method is shown that the matrix transform is efficient and that the module structure is easy. The circuit design of MRME on FG(p**m) is realized following as` 1) contructing the baisc gates on GF(3) by CMOS T gate, 2) designing the basic cells to be implemented the transform and inverse transform matrix of MRME using these basic gates, 3) interconnecting these cells by the input-output interconnecting method of the multivalued signal processing circuits. Also, the circuit design of the multi-valued signal processing function on GF(3\ulcorner similar to Winograd algorithm of 3x3 array of DFT (discrete fourier transform) is realized by interconnection of Perfect Shuffle technique and Kronecker product. The presented multi-valued signal processing circuits that are simple and regular for wire routing and posses the properties of concurrency and modularity are suitable for VLSI.

• The korean journal of orthodontics
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• v.4 no.1
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• pp.57-61
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• 1974

The patient, a girl of 19 years in good health, had a class I malocclusion. The maxillary left centra1 incisors and both lateral incisors had already erupted. But the space for the right central incisor was partially closed by the mesial drifting of the neighboring teeth. The caused a shift in the midline and a cross-bite relation on the incisors. X-ray examination revealed the presence of the right central incisor in the alveolar bone and odontoma just above the crown of the right central incisor. After enough space for the impacted incisor was created in the dental arch with a open-coil spring the rectangular incision was made. Removing the odontoma uncovered the flat surface of the labial aspect of the incisor. During the tooth had erupted of its own accord, any unnecessary force had been imposed on the tooth. When it was decided that the tooth should be brought out by the mechanical device, the gold cast onlay with hook was used and run a light elastic between this hook and the main arch wire. Finally the tooth was brought down to the arch level. The result was excellent. Fortunately the esthetic problem and any detrimental effects on the psychological make-up could be avoided.

• Journal of Mechanical Science and Technology
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• v.15 no.12
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• pp.1860-1868
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• 2001

An experimental investigation was carried out to clarify unsteady flow fields with rotating stall cell, especially behavior of stall cell, in a high specific-speed diagonal flow fan. As its specific-speed is vary high for a diagonal flow fan, its pressure-flow rate curve tends to indicate unstable characteristics caused by rotating stall similar to axial flow fan. Although for an axial flow fan many researchers have investigated such the flow field, for a diagonal flow fan tittle study has been done. In this study, velocity fields at rotor Inlet in a high specific-speed diagonal flow fan were measured by use of a single slant hot-wire probe. These data were processed by using the "Double Phase-Locked Averaging"(DPLA) technique, i. e. phases of both the rotor blade and the stall cell were taken into account. The behaviors of stall cell at rotor inlet were visualized for the meridional, tangential and radial velocity.

• Transactions of the Korean Society of Mechanical Engineers B
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• v.20 no.1
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• pp.244-254
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• 1996

Flow velocity was measured by, use of hot wire anemometer. Turbulence intensity was in proportion to mean flow velocity regardless of swirl velocity. And integral length scale has proportional relation with swirl velocity regardless of measurement position. Turbulent burning speed during flame propagation which was determined by flame photograph and gas pressure of combustion chamber was increased with the lapse of time from spark and was decreased a little at later combustion period. Because of combustion promotion effect, turbulent burning speed was increased according to increase of turbulence intensity. Burning speed ratio i.e. ratio of turbulent burning speed ($S_BT$) to laminar burning speed ($S_BL$) was found out by use of turbulence intensity u' and integral length scale $l_x$ , $\delta_L$ is width of preheat zone in laminar flame.